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Single Crystalline Commensurate Metallic Assemblages of π-slabs and CdI2-Type Layers: Synthesis and Properties of β-(EDT-TTF-I2)2[Pb5/61/6I2]3 and β-(EDT-TTF-I2)2[Pb2/3+xAg1/3-2xxI2]3, x = 0.05

Thomas Devic、M. Evain、Yves Moëlo 等 7 位作者2003-02-14Journal of the American Chemical Society

The ability of I...I van der Waals interactions to direct the self-assembly of slabs of the radical cation of ethylenedithio-1,2-diiodo-tetrathiafulvalene, EDT-TTF-I(2), and polymeric lead iodide covalent anionic layers is demonstrated by the synthesis of single crystals of beta-(EDT-TTF-I(2))(2)(.+)[(Pb(5/6) square (…

Perovskite Materials and ApplicationsMolecular Junctions and NanostructuresOrganic and Molecular Conductors Research

Crystalline Structure and Morphology in Nylon-12: A Small- and Wide-Angle X-ray Scattering Study

Li、Michel H. J. Koch、Wim H. de Jeu2003-02-14Macromolecules

Simultaneous small- and wide-angle X-ray scattering has been employed to monitor the temperature dependence of the crystalline structure and morphology of nylon-12. Wide-angle measurements reveal that the α‘-phase is a stable high-temperature crystalline phase. Upon cooling, a crystalline transition takes place from t…

Polymer crystallization and propertiesPolymer Nanocomposites and PropertiesFiber-reinforced polymer composites

Arrays of ZnO nanowires fabricated by a simple chemical solution route

Hui Zhang、Xiangyang Ma、Jin Xu 等 5 位作者2003-02-14Nanotechnology

A sol–gel process and a nanochannel aluminium template were employed to fabricate an orderly array of ZnO nanowires. The ZnO nanowires, with a hexagonal structure, were identified by means of x-ray diffraction and selected-area electron diffraction. The arrays of ZnO nanowires were characterized by scanning electron m…

ZnO doping and propertiesAnodic Oxide Films and NanostructuresGa2O3 and related materials

Water uptake and mechanical characteristics of natural filler–polypropylene composites

Mehdi Tajvidi、Ghanbar Ebrahimi2003-02-14Journal of Applied Polymer Science

Abstract Water uptake characteristics and some mechanical properties of polypropylene composites containing three types of natural fillers, purified α‐cellulose, wastepaper fibers, and wood flour were studied. The fiber contents were 15, 25, and 35% by weight. Two percent maleic anhydride polypropylene (MAPP) was also…

Mechanical Behavior of CompositesPolymer Nanocomposites and PropertiesNatural Fiber Reinforced Composites

Colloid-Polymer Mixtures in the Protein Limit

Peter G. Bolhuis、Evert Jan Meijer、Ard A. Louis2003-02-14Physical Review Letters

We computed the phase-separation behavior and effective interactions of colloid-polymer mixtures in the "protein limit," where the polymer radius of gyration is much larger than the colloid radius. For ideal polymers, the critical colloidal packing fraction tends to zero, whereas for interacting polymers in a good sol…

Phase Equilibria and ThermodynamicsProteins in Food SystemsMaterial Dynamics and Properties

σ Aromaticity of the Bimetallic Au5Zn+ Cluster

Hiromasa Tanaka、Sven Neukermans、Ewald Janssens 等 5 位作者2003-02-14Journal of the American Chemical Society

Experimental and theoretical evidence for a "sigma aromatic" bimetallic cluster is presented. A mass spectrometric analysis of AuNZn+ (N = 2-44) photofragments shows Au5Zn+ to be very abundant, proving its high stability. Calculations predict that Au5Zn+ has a planar geometry and six valence s electrons occupying delo…

Organometallic Complex Synthesis and CatalysisSynthesis and Properties of Aromatic CompoundsNanocluster Synthesis and Applications

Layer-by-Layer Self-Assembled Pyrrole-Based Donor−Acceptor Chromophores as Electro-Optic Materials

Antonio Facchetti、Alessandro Abbotto、Luca Beverina 等 8 位作者2003-02-14Chemistry of Materials

The synthesis of the heterocycle-based diethanolaminomethyl-functionalized derivative 1-(pyridin-4-yl)-2-[( N -methylpyrrol-2-yl)-5-methylenediethanolamine]ethene ( 2 ) from (1-pyridin-4-yl)-2-( N -methyl-pyrrol-2-yl)ethene ( 1 ) and their methylpyridinium dyes 1-( N -methylpyridinio)-2-[( N -methylpyrrol-2-yl)-5-meth…

Porphyrin and Phthalocyanine ChemistryMolecular Junctions and NanostructuresNonlinear Optical Materials Research

Hydrogen storage capacity of commercially available carbon materials at room temperature

Hisashi Kajiura、Shigemitsu Tsutsui、Koji Kadono 等 6 位作者2003-02-14Applied Physics Letters

The hydrogen storage capacity of five types of commercially available carbon materials with different nanostructures was measured at up to 8 MPa at room temperature using an apparatus based on a volumetric method with an error of less than 0.04 wt %/gr. The highest storage capacity of 0.43 wt % was obtained for purifi…

Advancements in Battery MaterialsCarbon Nanotubes in CompositesHydrogen Storage and Materials

Mechanical Properties of Artificial Protein Matrices Engineered for Control of Cell and Tissue Behavior

Kathleen Di Zio、David A. Tirrell2003-02-14Macromolecules

Genetic engineering methods were used for the preparation of artificial proteins containing sequences designed to reproduce essential features of the extracellular matrix (ECM). The long-term objective of the work is to develop matrices for use in the engineering of small-diameter vascular grafts. The CS5 domain of fi…

Electrospun Nanofibers in Biomedical ApplicationsConnective tissue disorders researchSilk-based biomaterials and applications

Pressure-Induced Simultaneous Metal-Insulator and Structural-Phase Transitions in LiH: a Quasiparticle Study

S. Lebègue、M. Alouani、B. Arnaud 等 4 位作者2003-02-14arXiv

A pressure-induced simultaneous metal-insulator transition (MIT) and structural-phase transformation in lithium hydride with about 1% volume collapse has been predicted by means of the local density approximation (LDA) in conjunction with an all-electron GW approximation method. The LDA wrongly predicts that the MIT o…

Materials ScienceStrongly Correlated Electrons

The influence of hydrogen adsorption on magnetic properties of Ni/Cu(001) surface

František Máca、Alexander B. Shick、Josef Redinger 等 5 位作者2003-02-14arXiv

Ni/Cu(001) is known as a unique system showing the spin-reorientation transition from an in-plane to out-of-plane magnetization direction when the Ni-overlayer thickness is increased. We investigate different relaxed multilayer structures with a hydrogen adlayer using the full-potential linearized augmented plane-wave…

Materials Science

Exceptionally Slow Rise in Differential Reflectivity Spectra of Excitons in GaN: Effect of Excitation-induced Dephasing

Y. D. Jho、D. S. Kim、A. J. Fischer 等 7 位作者2003-02-14arXiv

Femtosecond pump-probe (PP) differential reflectivity spectroscopy (DRS) and four-wave mixing (FWM) experiments were performed simultaneously to study the initial temporal dynamics of the exciton line-shapes in GaN epilayers. Beats between the A-B excitons were found \textit{only for positive time delay} in both PP an…

Materials Science

Orbital-Order-Induced Metal-Insulator Transition inLa1−xCaxMnO3

Bas B. Van Aken、Oana D. Jurchescu、Auke Meetsma 等 6 位作者2003-02-14Physical Review Letters

We present evidence that the insulator-to-metal transition in ${\mathrm{L}\mathrm{a}}_{1\ensuremath{-}x}{\mathrm{C}\mathrm{a}}_{x}{\mathrm{M}\mathrm{n}\mathrm{O}}_{3}$ near $x\ensuremath{\sim}0.2$ is driven by the suppression of coherent Jahn-Teller distortions, originating from $d$-type orbital ordering. The orbital-…

Magnetic and transport properties of perovskites and related materialsRare-earth and actinide compoundsAdvanced Condensed Matter Physics

Nonequilibrium phase transition in surface growth

B. Chakrabarti、C. Dasgupta2003-02-14arXiv

Conserved growth models that exhibit a nonlinear instability in which the height (depth) of isolated pillars (grooves) grows in time are studied by numerical integration and stochastic simulation. When this instability is controlled by the introduction of an infinite series of higher-order nonlinear terms, these model…

cond-mat.dis-nnMaterials Sciencecond-mat.stat-mech

Degenerate p-type conductivity in wide-gap LaCuOS1−xSex (x=0–1) epitaxial films

Hidenori Hiramatsu、Kazushige Ueda、Hiromichi Ohta 等 6 位作者2003-02-14Applied Physics Letters

Epitaxial films of LaCuOS1−xSex (x=0–1) solid solution were grown on MgO (001) substrates and their electrical and optical properties were examined. Sharp emission due to room-temperature exciton with binding energy of ∼50 meV is observed for all x values. Hall mobility becomes large with an increase in the Se content…

ZnO doping and propertiesCopper-based nanomaterials and applicationsElectronic and Structural Properties of Oxides

Light-Induced Coherent Interactions between Silver Nanoparticles in Two-Dimensional Arrays

S. Z. Malynych、George Chumanov2003-02-14Journal of the American Chemical Society

Silver nanoparticles arranged in two-dimensional arrays experience quadrupolar coupling of plasmon resonances when irradiated with visible light. This coupling leads to the formation of the coherent plasmon mode characterized by an intense narrow resonance in the blue spectral range in the extinction spectrum. The cou…

Gold and Silver Nanoparticles Synthesis and ApplicationsPlasmonic and Surface Plasmon ResearchNonlinear Optical Materials Studies

Deposition of Gold Nanoparticles on Silica Spheres: A Sonochemical Approach

Vilas G. Pol、Aharon Gedanken、José Maria Calderón-Moreno2003-02-14Chemistry of Materials

Gold nanoparticles with an average size of ∼5 nm were deposited on the surface of preformed silica submicrospheres with the aid of power ultrasound. The sonochemical reduction was carried out by ultrasonic irradiation in an argon atmosphere at room temperature. Ultrasonic irradiation of a slurry of silica submicrosphe…

Gold and Silver Nanoparticles Synthesis and ApplicationsUltrasound and Cavitation PhenomenaLaser-Ablation Synthesis of Nanoparticles

Oxygen adsorption on Au clusters and a rough Au(111) surface: The role of surface flatness, electron confinement, excess electrons, and band gap

G.A. Mills、Mark S. Gordon、Horia Metiu2003-02-14The Journal of Chemical Physics

It has been shown recently that while bulk gold is chemically inert, small Au clusters are catalytically active. The reasons for this activity and its dramatic dependence on cluster size are not understood. We use density functional theory to study O2 binding to Au clusters and to a Au(111) surface modified by adsorpt…

Advanced Chemical Physics StudiesCatalytic Processes in Materials ScienceMolecular Junctions and Nanostructures

Selective Adsorbents from Ordered Mesoporous Silica

Ka Yee Ho、Gordon McKay、King Lun Yeung2003-02-14OpenAlex

Ordered mesoporous silica adsorbents were prepared by grafting amino- and carboxylic-containing functional groups onto MCM-41 for the removal of Acid blue 25 and Methylene blue dyes from wastewater. The amino-containing OMS−NH 2 adsorbent has a large adsorption capacity and a strong affinity for the Acid blue 25. It c…

Adsorption and biosorption for pollutant removalCatalytic Processes in Materials ScienceMesoporous Materials and Catalysis

Metal and ligand hyperfine couplings in transition metal complexes: The effect of spin–orbit coupling as studied by coupled perturbed Kohn–Sham theory

Frank Neese2003-02-14OpenAlex

The derivation, implementation, and validation of a method to calculate spin–orbit coupling (SOC) contributions to the hyperfine coupling (HFC) is reported. Due to this development it is now possible to calculate the complete ligand and metal nuclei HFCs at a consistent level of theory, i.e., spin unrestricted Hartree…

Advanced Chemical Physics StudiesMagnetism in coordination complexesAdvanced NMR Techniques and Applications