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An Unorthodox Conformation of [18]porphyrin-(1.1.1.1) Heteroanalogue—21,23-Ditelluraporphyrin with a Flipped Tellurophene Ring Financial support from the State Committee for Scientific Research KBN of Poland (Grant: 3 T09A 155 15) and the Foundation for Polish Science is gratefully acknowledged.

Ewa Pacholska、Lechosław Latos‐Grażyński、Z. Ciunik2001-12-03Angewandte Chemie International Edition

The flexible partially inverted structure of an 18-π-electron porphyrin-(1.1.1.1)-like framework is found for 21,23-ditelluraporphyrin (see structure). The dihedral angle between the plane of meso-carbon atoms and the inverted tellurophene plane in the solid state is 123.0(2)°, while in solution the porphyrin molecule…

Advanced Chemical Physics StudiesSupramolecular Chemistry and ComplexesPorphyrin and Phthalocyanine Chemistry

Control of Liquid Crystallinity of Diazadibenzoperylene Dyes by Covalent and Hydrogen-Bonded Attachment of Mesogens We thank P. Zell for his assistance in the practical work, Frau G. Dörfner and Prof. U. Thewalt (Sektion Röntgenbeugung, Universität Ulm) and Dr. B. Heise (Abteilung Experimentelle Physik, Universität Ulm) for X-ray diffraction studies. Financial support from the Deutsche Forschungsgemeinschaft (Habilitandenstipendium for F.W.), the Fonds der Chemischen Industrie (Liebig-Stipendium for F.W.), and the Dr. Otto Röhm Gedächtnisstiftung is gratefully acknowledged.

Armin Sautter、Christoph Thalacker、Frank Würthner2001-12-03Angewandte Chemie International Edition

Fluorescent liquid crystals: Hydrogen bonding of benzoic acids to azaaromatic receptor groups of diazadibenzoperylene fluorophores induces columnar liquid crystalline mesophases which are highly fluorescent. The structure of a mesogenic supermolecule generated in this way is shown on a background of a polarizing micro…

Liquid Crystal Research AdvancementsNonlinear Dynamics and Pattern FormationMolecular spectroscopy and chirality

Creation of nanodiamonds by single impacts of highly charged ions upon graphite

T. Meguro、Akira Hida、Mitsutoshi Suzuki 等 8 位作者2001-12-03Applied Physics Letters

The local modification of the electronic states of highly oriented pyrolytic graphite (HOPG) surfaces using highly charged ion (HCI) irradiation has been demonstrated as a promising technique in the design of nanoscale materials. The high potential energy of HCI and subsequent surface treatment by either electron inje…

Diamond and Carbon-based Materials ResearchIon-surface interactions and analysisIntegrated Circuits and Semiconductor Failure Analysis

Temperature-induced change from p to n conduction in metallofullerene nanotube peapods

Po‐Wen Chiu、Grace X. Gu、Guntae Kim 等 7 位作者2001-12-03Applied Physics Letters

Metallofullerene nanotube peapods were prepared by introducing Dy@C82 into the interior space of single-walled carbon nanotubes. Transport measurements show that the Dy@C82 molecules function as electron donors and transfer charge to the carbon nanotube host. The amount of charge transferred varies with the temperatur…

Carbon Nanotubes in CompositesGraphene research and applicationsFullerene Chemistry and Applications

Towards Rational Design of Fast Water-Exchanging Gd(dota-Like) Contrast Agents? Importance of the M/m Ratio

Frank A. Dunand、Rachel S. Dickins、David Parker 等 4 位作者2001-12-03Chemistry - A European Journal

1H NMR line-shape analysis and magnetisation-transfer experiments at variable temperature and pressure have been used to elucidate the solution dynamics of both M and m isomers of three [Eu(dota-tetraamide)(H2O)]3+ complexes. The direct 1H NMR observation of the bound water signal allows the water-exchange rates on ea…

Advanced MRI Techniques and ApplicationsMagnetism in coordination complexesLanthanide and Transition Metal Complexes

Figure-Eight Tetrathiaoctaphyrin and Dihydrotetrathiaoctaphyrin

Natasza Sprutta、Lechosław Latos‐Grażyński2001-12-03Chemistry - A European Journal

The acid-catalyzed condensation of pyrrole and 2,5-bis(p-tolylhydroxymethyl)thiophene yields two novel giant heteroporphyrins: 5,10,15,20,25,30, 35,40-octa(p-tolyl)-41,43,45,47-tetrathia[36]octaphyrin(1.1.1.1.1.1.1.1) (S4OP) and 5,10,15,20,25,30,35,40-octa(p-tolyl)-dihydro-41,43,45,47-tetrathia[38]octaphyrin(1.1.1.1.1…

Molecular Sensors and Ion DetectionSupramolecular Chemistry and ComplexesPorphyrin and Phthalocyanine Chemistry

Material Characterization of High Dielectric Constant Polymer–CeramicComposite for Embedded Capacitor to RF Application

Yang Rao、Jireh Yue、C.P. Wong2001-12-03Active and Passive Electronic Components

Embedded capacitor technology can improve electrical performance and reduce assembly cost compared with traditional discrete capacitor technology. Polymer–ceramic composites have been of great interest as embedded capacitor material because they combine the processability of polymers with the desired electrical proper…

Electromagnetic wave absorption materialsDielectric materials and actuatorsSynthesis and properties of polymers

S-Position Isomers of BEDT-TTF and EDT-TTF: Synthesis and Influence of Outer Sulfur Atoms on the Electrochemical Properties and Crystallographic Network of Related Organic Metals

Piétrick Hudhomme、S. Le Moustarder、Christophe Durand 等 10 位作者2001-12-03Chemistry - A European Journal

The synthesis and characterization of new modified tetrathiafulvalenes (TTF), the S-position isomers of BEDT-TTF and EDT-TTF, are described. The synthetic strategy presented in this work is based on an efficient and unprecedented two-step sequence for the conversion of a vicinal bis(hydroxymethyl) functionality into a…

Magnetism in coordination complexesOrganic and Molecular Conductors ResearchOrganometallic Compounds Synthesis and Characterization

Amorphous carbon nanowires investigated by near-edge-x-ray-absorption-fine-structures

Yu-Hui Tang、Peng Zhang、Peter Kim 等 11 位作者2001-12-03Applied Physics Letters

The structure and bonding of amorphous carbon nanowires and amorphous carbon nanowires-converted multiwalled carbon nanotubes have been investigated with carbon K-edge near-edge x-ray absorption fine structure using surface-sensitive total electron yield, and bulk-sensitive fluorescence yield. The results strongly sup…

Carbon Nanotubes in CompositesDiamond and Carbon-based Materials ResearchFullerene Chemistry and Applications

Synthesis of Highly Magnetic, Air-Stable Iron-Iron Carbide Nanocrystalline Particles by Using Power Ultrasound

Sergei I. Nikitenko、Yuri Koltypin、O. Palchik 等 6 位作者2001-12-03Angewandte Chemie

Durch eine Eisencarbid- und Kohlenstoffhülle gegen Luftoxidation geschützt sind die nanokristallinen Eisenpartikel, die durch Sonolyse von [Fe(CO)5] in Diphenylmethan und Tempern des erhaltenen Materials hergestellt wurden. Die Sättigungsmagnetisierung des Materials (222 emu g−1, siehe Bild) ist fast so hoch wie die v…

Carbon Nanotubes in CompositesDiamond and Carbon-based Materials ResearchLaser-Ablation Synthesis of Nanoparticles

From CO2 to Methanol by Hybrid QM/MM Embedding

Samuel A. French、Alexey A Sokol、Stefan T. Bromley 等 7 位作者2001-12-03Angewandte Chemie

Struktur und Energetik der Schlüsselintermediate bei der katalytischen Umwandlung von CO2 zu Methanol (siehe Bild) wurden untersucht. Die Polarität der für die Katalyse relevanten (000)-Oberfläche von ZnO führt zu unbesetzten Sauerstoffpositionen, die als Elektronenfallen die Reaktion vorantreiben. Die entwickelte Fes…

Advanced Chemical Physics StudiesCatalytic Processes in Materials ScienceCatalysts for Methane Reforming

Host-Guest Interaction of 12-MC-4, 15-MC-5, and Fused 12-MC-4 Metallacrowns with Mononuclear and Binuclear Carboxylato Complexes: Structure and Magnetic Behavior

C. Dendrinou-Samara、George Psomas、Lykourgos Iordanidis 等 5 位作者2001-12-03Chemistry - A European Journal

Interaction of manganese with salicylhydroxamic ligands leads to the formation of the 12-membered metallacrown [Mn(II)(2(2,4-DP)2(HCOO)2]-[12-MC(Mn(III)N(shi)-4](py)6 (2) (H-2,4-DP =2-(2,4-dichlorophenoxy)propionic acid) and the 15-membered metallacrown [Mn(II)(2,4-D)2][15-MC(Mn(III)N(shi)-5](py)6 (1) (H-2,4-D = 2,4-d…

Metal-Organic Frameworks: Synthesis and ApplicationsMagnetism in coordination complexesLanthanide and Transition Metal Complexes

Scaling of hysteresis dispersion in a model spin system

Jun‐Ming Liu、Helen Lai Wah Chan、C. L. Choy 等 4 位作者2001-12-03Physical review. B, Condensed matter

We present a calculation of the magnetic hysteresis and its area for a model continuum spin system based on three-dimensional $({\ensuremath{\Phi}}^{2}{)}^{2}$ model with $O(N)$ symmetry in the limit $N\ensuremath{\rightarrow}\ensuremath{\infty},$ under a time-varying magnetic field. The frequency dependence of the hy…

Magnetic properties of thin filmsTheoretical and Computational PhysicsMagnetic Properties and Applications

Dissipative water intrusion in hydrophobic MCM-41 type materials

Thierry Martin、Benoît Lefèvre、D. Brunel 等 9 位作者2001-12-03Chemical Communications

Texture-related features of water intrusion in hydrophobised MCM-41 silicas render these materials especially suitable for energy dissipation in mechanical dampers.

Mesoporous Materials and CatalysisAdvanced Materials and MechanicsAerogels and thermal insulation

Strain-induced diffuse dielectric anomaly and critical point in perovskite ferroelectric thin films

A. K. Tagantsev、N.A. Pertsev、Paul Muralt 等 4 位作者2001-12-03Physical review. B, Condensed matter

It is shown that a strong but diffuse dielectric anomaly, commonly expected only in disordered ferroelectrics, may be inherent in strained and defect-free perovskite ferroelectric thin films. The origin of this unusual anomaly, which was never predicted for a defect-free system, is the overcritical trace of a critical…

Ferroelectric and Piezoelectric MaterialsMultiferroics and related materialsMicrowave Dielectric Ceramics Synthesis

Organische Nanopartikel in wässriger Phase - Theorie, Experiment und Anwendung

Dieter Horn、Jens Rieger2001-12-03Angewandte Chemie

Viele organische Wirk- und Effektstoffe sind in Wasser schwer löslich oder sogar unlöslich. Wässrige Anwendungsformen erfordern daher besondere Formulierungsverfahren, um die physiologische (Pharma, Kosmetik, Pflanzenschutz, Ernährung) oder technologische Wirkung (Lacke, Druckfarben, Toner) nutzen zu können oder zu op…

Quantum Dots Synthesis And PropertiesAlgal biology and biofuel productionPolyoxometalates: Synthesis and Applications

Atomic and electronic structure ofCo/SrTiO3/Comagnetic tunnel junctions

I. I. Oleinik、Evgeny Y. Tsymbal、D. G. Pettifor2001-12-03Physical review. B, Condensed matter

First-principles density-functional calculations of the atomic and electronic structure of ${\mathrm{C}\mathrm{o}/\mathrm{S}\mathrm{r}\mathrm{T}\mathrm{i}\mathrm{O}}_{3}/\mathrm{Co}$ (001) magnetic tunnel junctions (MTJ's) are performed. Different interface terminations are considered and the most stable structure wit…

Magnetic and transport properties of perovskites and related materialsAdvanced Condensed Matter PhysicsElectronic and Structural Properties of Oxides

Synthesis, Structure, Spectroscopic Properties, and Electrochemistry of Rare Earth Sandwich Compounds with Mixed 2,3-Naphthalocyaninato and Octaethylporphyrinato Ligands

Jianzhuang Jiang、Yongzhong Bian、Fumio Furuya 等 10 位作者2001-12-03Chemistry - A European Journal

A series of 14 heteroleptic rare earth sandwich complexes [M(III)-(nc)(oep)] (M=Y, La-Lu except Ce and Pm; nc=2,3-naphthalocyaninate; oep = octaethylporphyrinate) have been prepared by a one-pot procedure from corresponding [M(acac)3] . nH2O (acac = acetylacetonate), metal-free porphyrin H2(oep), and naphthalonitrile…

Magnetism in coordination complexesPorphyrin and Phthalocyanine ChemistryMetal-Catalyzed Oxygenation Mechanisms

Synthesis of Highly Magnetic, Air-Stable Iron–Iron Carbide Nanocrystalline Particles by Using Power Ultrasound A. Gedanken is grateful for the support of the German Ministry of Science through the Deutsche-Israeli DIP program. I. Felner and A. Gedanken thank also the Israeli Ministery of Science, Culture and Sport for an infrastructure grant. S. I. Nikitenko thanks the Bar-Ilan Research Authority for his fellowship. The authors also thank Dr. Shifra Hochberg for editorial assistance.

Sergei I. Nikitenko、Yuri Koltypin、O. Palchik 等 6 位作者2001-12-03Angewandte Chemie International Edition

A coating of iron carbide and carbon confers air-stability on the nanocrystalline iron particles that were prepared by sonolysis of [Fe(CO)5] in diphenylmethane followed by annealing of the as-prepared material. The saturation magnetization of this material (222 emu g−1, see picture) is almost as high as that of bulk…

Diamond and Carbon-based Materials ResearchPower Transformer Diagnostics and InsulationPowder Metallurgy Techniques and Materials

Tetraphenylbenziporphyrin—A Ligand for Organometallic Chemistry

Marcin Stępień、Lechosław Latos‐Grażyński2001-12-03Chemistry - A European Journal

6,11,16,21-Tetraphenylbenziporphyrin (TPBPH)H, an analogue of tetraphenylporphyrin with one of the pyrrole groups replaced by a benzene ring, is formed in good yield in the condensation of the appropriate precursor with pyrrole and benzaldehyde. (TPBPH)H gives organometallic complexes with palladium(II) and platinum(I…

Porphyrin and Phthalocyanine ChemistryLuminescence and Fluorescent MaterialsMetal-Catalyzed Oxygenation Mechanisms