Materials Literature
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Abstract A butyl methacrylate oligomer with furan end‐groups was synthesized by ozonolysing a poly(butyl methacrylate‐ co ‐butadiene) latex. The end‐groups of this oligomer were amidated with aminomethylfuran to give a coagulated mass of derivatized oligomers. This furan functional oligomer was then mixed with poly(et…
An applications of the molecular orbital (MO) calculation and Maeir-Meier theory to liquid crystal compounds are investigated for estimating dielectric anisotropy (δϵ). The method involves calculating the parameters on MO calculation and substituting these values into Maeir-Meier theory. These calculations are repeate…
Compounds based on 4,4'-substituted phenylbenzoate \[R O-C6H4COO-C6H4- X] (I), where X is a cyano group and R is a terminal alkyl chain ranging from 12 to 30 carbon atoms, and alternatively where R is held at 16 carbons and X is CN, COOH, OH, COOCH2C6H4, OCH2C6H4 and OC16H33, were prepared and their mesophase stabilit…
Measurements of the thermal expansion of a single crystal of ${\mathrm{La}}_{0.835}{\mathrm{Sr}}_{0.165}{\mathrm{MnO}}_{3}$ were performed under hydrostatic pressure of up to 9 kbar. The $P$-$T$ phase diagram is established for the structural and magnetic phase transitions. Pressure is found to enhance the ferromagnet…
Alumina–glass composites that contain oxidized aluminum were investigated to make shrinkage‐free, all‐ceramic dental porcelain. This was achieved by control of the volume expansion and shrinkage that occur during the aluminum oxidation and densification processes. The dimensional change and strength of the alumina‐gla…
ortant for the materials mentioned above, it may be very relevant for transition metals and other materials with a stress exponent different from m = 1. To investigate the implications of a stress exponent m?1 we study a simple two-dimensional model of the dislocation activity close to a semi-infinite crack in an infi…
Blends from poly(trimethylene carbonate) (PTMC) and poly(adipic anhydride) (PAA) with different compositions and different molecular weights were prepared by a solution blending method. Comparing blends with copolymers generally, the original degradation properties of the used components were changed through physical…
We report for the first time the results of theoretical study on the optical properties of single layer non-absorptive broadband cholesteric liquid crystals (BBCLC) polarizers. The objective of this study is to understand the effect of material parameters and sample configuration on the performake of BBCLC films and t…
Abstract It has long been the bane of analytical electron microscopy (AEM) that the use of focused probes during microanalysis of specimens increases the local rate of hydrocarbon contamination. This is most succinctly observed by the formation of contamination deposits (fig.l) during focused probe work typical of AEM…
Pure and doped (Benzophenone and Urea) triglycine sulphate (TGS) crystals have been grown from aqueous solution by slow cooling method. The influence of doping of benzophenone and urea on the growth and electrical properties have been investigated. The pyroelectric coefficient increases with the addition of benzopheno…
Ba 6 CoNb 9 O 30 and Ba 6 FeNb 9 O 30 in space group P 4 bm are shown to satisfy the structural criteria for ferroelectricity. Ba 6 CoNb 9 O 30 undergoes a diffuse phase transition at 660 (11) K, as observed calorimetrically, in addition to a dielectric permittivity anomaly with an onset temperature of 685 (10) K. The…
Abstract Treatment of a C222‐vanadyl‐AMP complex (C222 = cryptand‐222, AMP = adenosine monophosphate) with Me 2 NH in the presence of air yielded centrosymmetric dihydrogen‐decavanadate H 2 V 10 O 4 28 , sandwiched by two diprotonated C222 molecules. An X‐ray crystal‐structure analysis was performed of this compound w…
The desorption processes of adsorbed impurity ions on various alignment layers in nematic liquid crystal cells have been studied by measuring ac conductivity of the cells. The liquid crystal used here is 4-cyano-4′-pentyl biphenyl. The adsorption of the ions is induced by the application of dc voltage to the cells. It…
Four major cardenolide glycosides of Xysmalobium undulatum (L.) R. Br. roots (Uzara) have been isolated for the first time in pure form. The structures were elucidated by spectral analyses and determined as sophorosides and their 17-epimers, respectively. Thus, the structural elucidation of uzarin and xysmalorin, the…
A thermal conductivity augmentation technology for zeolite beds has been studied in this paper. To enhance the effective thermal conductivity of zeolite, the zeolite particle was coated with a thermal polymer material in a new synthesis process. It was found that the effective thermal conductivity of the polymerzeolit…
Statistical properties of well-defined fully conjugated poly(3-octylthiophene) (POT) gels are explored above glass transition and fusion temperatures by varying the cross-link functionality, f, and the cross-link concentration, R i . Four series of gels are prepared using four different cross-linking agents. The state…
The article deals with ionic crystals of the type A+B− where the cations are alkali, NH+ 4 or TI+ ions and the anions are the triatomic linear entities SCN−, OCN−, N− 3 and HF− 2. These crystals show a large variety of crystallographic phases which are based on the orientational degrees of freedom of the linear anions…
The grain size distribution of copper and nickel processed by severe plastic deformation was studied by transmission electron microscopy. The temperature dependence of electrical resistivity in the temperature range from 20 to 300 K is presented. The tunnel model of electrical resistivity of grain boundaries is discus…
The analytical models already developed by Smith and Roylance for impact in yarns and impact in textiles have been used, together with a new failure criterion based on the energy that crosses each yarn, to build a simple analytical model of impact in textiles. This model has been checked with Dyneema armours and predi…
The room-temperature phases of sodium potassium molybdates K 3 Na(MoO 4 ) 2 and K 2.5 Na 1.5 (MoO 4 ) 2 are isostructural with the monoclinic low-temperature phases of KaNa(SeO 4 ) 2 and K 3 Na(CrO 4 ) 2 , which are twinned distorted glaserite structures. In the molybdates there are two crystallographically independen…