Materials Literature
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Abstract The technique of photo-electron emission microscopy (PEEM) is based on imaging of photo excited electrons from a surface. Typically ultra violet (UV) light above the work function of a metal will cause electrons to be emitted from a surface. Since photo excited electrons originate very near to the surface, th…
Abstract Compositional mapping with energy dispersive x-ray spectrometry (EDS) in the scanning electron microscope (SEM) is one of the most widely used techniques for elemental imaging of microstructures. SEM/EDS maps are usually qualitative presentations of elemental distributions in x-y space. In older implementatio…
V2O5 is a layered semiconducting oxide, which is used as a catalyst for the partial oxidation of hydrocarbons. In view of its catalytic applications, the vibrational properties of the (001) surface were examined by means of HREELS, a technique which is uniquely sensitive to the first layers' characteristics. On a clea…
Abstract Achieving superplasticity in fine-grained ceramics is a potential method to lower energy costs associated with ceramic manufacturing via net shape forming. Superplasticity is intrinsic in 3-mol%- yttria-stabilized tetragonal zirconia polycrystals (3Y-TZP), and can be enhanced by addition of glass to form inte…
Abstract A large number of electroceramics derive their technologically useful and scientifically appealing properties via electrically active (charged) interfaces.[l] These interfaces can be simple grain boundaries in, for example, varistors, to complicated domain configuration in ferroelectric thin films. Several co…
Abstract Interest in electron beam x-ray microanalysis with low incident beam energies, defined arbitrarily as 5 keV and below, has been greatly stimulated in recent years by the development of the high performance field emission gun scanning electron microscope (FEG-SEM), which can produce a nanometer-scale probe wit…
Point-defect formation energies were calculated using a molecular static method in a Mott-Littleton approximation for defects in ionic crystals. Energy barriers for oxygen migration in metal-oxygen planes were determined. The results obtained are compared with the experimental ones and those previously calculated for .
Polycrystalline (ZnSe)x(CdS)1−x (0≤x≤1.0) films were formed on glass substrates kept at a temperature of 197°C by thermal evaporation technique. The dark conductivity and thermoelectric power were measured and were used to calculate the electron density and mobility. The temperature dependences of electrical conductiv…
In this work, the efficiency of starch acetylation to reduce water sensitivity of hydrophilic materials was investigated. Starch acetate was either included in foamed starch trays and/or used to coat these trays, wheat gluten based films or paper sheets. The water sensitivity of these foamed trays (quantity and kineti…
Abstract Phase segregation is important in determining the properties of many complex polymers, including polyurethanes. Achieving a better understanding of the links between formulation, chemical nature of segregated phases, and physical properties, has the potential to aid development of improved polymers. However,…
The phase behavior of blends of poly(isobutylene) (PIB) having different molecular weights and its carbosilane analog poly(dimethylsilylenemethylene) (PDMSM) is studied by optical microscopy, differential scanning calorimetry (DSC) and pressure—volume—temperature (PVT) measurements. DSC and microscopy measurements rev…
Die bewährten Schwefelsäurewerkstoffe Nicrofer 4221 (2.4858) und Nicrofer 3620 Nb (2.4660) besitzen nur eine geringe Lokalkorrosionsbeständigkeit in chloridhaltigen Wässern und sind daher als Werkstoffe für Schwefelsäurekühler ungeeignet. Die neuentwickelte austenitische Cr-Legierung Nicrofer 3033 (X1CrNiMoCuN 33-32-1…
Magnetic studies of graphite-coated nanocrystals of nickel and cobalt (5-50 nm) synthesized in a special fullerene are chamber are reported. Magnetization measurements as a function of temperature in the range 20-900/spl deg/C indicate the ferromagnetic nature of the nanocrystals. Upon heating and recooling of the nan…
The polyester in the base fabrics (PET) and the polyvinyl chloride coating (PVC) along with plasticizers and adhesive/glue were separated from a commercial coated fabric by a scheme of chopping, grinding, and extracting with a selected preferred aqueous MEK solution. A novel recovering method called swelling method is…
Brazing experiments were performed at 830/spl deg/C for Al/sub 2/O/sub 3//Al/sub 2/O/sub 3/ and Al/sub 2/O/sub 3//Fe-Ni-Co alloy joints, which are used in electronic and structural applications. The brazing was done with Ag-Cu and Ag-Cu-Ti and changes in fracture mode and fracture strength of the Al/sub 2/O/sub 3/-Al/…
PMN-PT ceramics with perovskite structure were prepared by powders synthesized in KCl molten salt. Dielectric and piezoelectric properties were studied and compared with those of the ceramics prepared by conventional ceramic processing. The results indicate that the PMN-PT powders with perovskite structure can be synt…
FT-IR Spectroscopy have been used for identifying both the structure of BN and the intensity of the compressive stress in cubic boron nitride (c-BN) film prepared by a unbalanced of (13.56 MHz) magnetron sputtering of a hexagonal boron nitride target in a mixture argon and nitride discharge. A T(temperature) - V(negat…
Molecular modeling and thermal analysis have been integrated into our Polymer Science course in order to encourage multifaceted problem solving and allow students to systematically explore the role of chemical structure in determining the glass transition temperature of a polymer. A variety of case studies, such as th…
The influence of exchange coupling of layers on the propagation of magnetostatic dipole volume waves in normally and tangentially magnetized two-layer epitaxial ferrite structures is investigated. It is shown that the indicated influence is manifested in the form of dynamic spin pinning effects on the interlayer bound…
Abstract The 35 Cl NQR frequencies, spin-lattice relaxation time and 1 H NMR relaxation time were measured on crystalline Na 2 PtCl 6 • 6H 2 O at 77-350 K. The presence of three nonequivalent chlorine sites found by X-ray diffraction measurement is in agreement with the observed three NQR lines, which have different t…