Materials Literature
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This paper describes a systematic investigation on the synthesis of CeO2 supported on SiO2 by two different methods: (i) the in situ incorporation of CeO2 onto MCM-41 and (ii) wet impregnation. We were interested in investigating how the CeO2 preparation could influence their physicochemical properties and catalytic p…
Mesoporous gold sponges were prepared using 4-dimethylaminopyridine (DMAP)-stabilized Au seeds. This is a general process, which involves a simple template-free method, room temperature reduction of HAuCl4·4H2O with hydroxylamine. The formation process of mesoporous gold sponges could be accounted for the electrostati…
As biodegradable scaffolds, protein hydrogels have considerable potential, particularly for bioartificial organs and three-dimensional space-filling materials. However, their low strength and stiffness have been considered to be limitations for enduring physiological stimuli. Therefore, protein hydrogels have been com…
A combination of electron paramagnetic resonance (EPR) spectra and density functional theory (DFT) calculations is used to characterize the paramagnetic species in rutile N-doped SnO 2 samples synthesized by wet chemistry methods. In particular, the nature of paramagnetic N species, substitutional or interstitial, and…
A galvanic test panel design incorporating a painted and scribed Al alloy panel and uncoated through-hole noble fasteners has recently been utilized to compare effects of different surface pretreatments on galvanic attack in laboratory chambers. In this work, corrosion of galvanic panels composed of a coated AA2024-T3…
We report a macrocyclic ligand based on a 3,6,10,13-tetraaza-1,8(2,6)-dipyridinacyclotetradecaphane platform containing four hydroxyethyl pendant arms (L(1)) that forms extraordinary inert complexes with Ln(3+) ions. The [EuL(1)](3+) complex does not undergo dissociation in 1 M HCl over a period of months at room temp…
In this paper, we report polyfluorene-separated ultra-high purity semiconducting carbon nanotube radio frequency transistors with a self-aligned T-shape gate structure. Because of the ultra-high semiconducting tube purity and self-aligned T-shape gate structure, these transistors showed an excellent direct current and…
In this article, carbon nanofiller, in particular graphite, has been reviewed for the preparation of polymer-based composites. The dispersion of graphite relies on fabrication methods employed such as solution mixing, melt blending, and in situ polymerization. The consequences of surface modification on thermal, mecha…
Trianguleniums are fascinating conjugated hexacyclic cations that exhibit interesting electronic and optical properties. Herein, the electrogenerated chemiluminescence (ECL) emission of this family of fluorescent dyes is reported for the first time. Redox behavior and fluorescence properties of eight cationic triangul…
Laterally ordered sub-10 nm features are produced from the directed self-assembly of poly(1,1-dimethyl silacyclo-butane)-block-poly(methyl methacrylate) (PDMSB-b-PMMA) thin films on sinusoidal azobenzene-containing patterns. The use of sinusoidal surface relief grating enables the formation of very large grain areas (…
High-quality epitaxial growth of inter-metallic MnPt films on oxides is achieved, with potential for multiferroic heterostructure applications. Antisite-stabilized spin-flipping induces ferromagnetism in MnPt films, although it is robustly antiferromagnetic in bulk. Moreover, highly ordered antiferromagnetic MnPt film…
We have studied the transformation of carbides in AISI M42 high-speed steels in the temperature window used for forging. The annealing was found to result in the partial transformation of the large, metastable M2C carbides into small, more stable grains of M6C, with an associated change in the crystal orientation. In…
Loss is known to be detrimental for achieving perfect focusing with the passive perfect lens designs suggested thus far, and it is believed to pose a fundamental barrier. We show that perfect lensing can be achieved with actual lossy left-handed metamaterials, without a need for gain or nonlinearity. The proposed loss…
In this work, a series of high-solids crosslinked hybrid networks based on the epoxy-terminated urethane oligomer and the comb-like structure epoxy-functional siloxane cured with diethylenetriamine, were obtained. The structure of the obtained poly(urethane–siloxane) thermosets was confirmed by FTIR spectroscopy. The…
ABSTRACT Microparticles formed by poly(lactic acid) (PLA) and poly(ethylene glycol) (PEG) diblock copolymers containing fluorescein grafted to the polymer chain were synthesized by a Ugi four‐component condensation (UFCC) reaction. To synthesize these copolymers, lactide was first polymerized by a ring‐opening polymer…
In this work, new kinds of magnetic luminescent nanoparticles were synthesized by doping of Dy in CeO2 nanoparticles (DDC) with ratios of 5.2, 11.11 and 17.6 mol% via microwave-induced combustion method. The nanoparticles obtained were characterized by several techniques including X-ray diffraction, specific surface a…
A new type of easily synthesized rhodamine-based chemosensor L(3), with potential NO2 donor atoms, selectively and rapidly recognizes Hg(2+) ions in the presence of all biologically relevant metal ions and toxic heavy metals. A very low detection limit (78 nM) along with cytoplasmic cell imaging applications with no o…
Microcrystalline cellulose (MCC) is an important ingredient in pharmaceutical, food, cosmetic and other industries. Microcrystalline cellulose was synthesized from the alpha cellulose content of pretreated cotton, Bombax ceiba L. by hydrochloric acid hydrolysis. The prepared microcrystalline cellulose was characterize…
Ag and Ag-based pseudo-alloys were evaluated in terms of application as metal brazes for the use in a hybrid direct carbon fuel cell stack. This paper reports on a series of wetting experiments on systems of pure Ag as well as Ag–Cu–Ti and Ag–Cu–Ni pseudo-alloys in contact with the widely used austenitic stainless ste…
Abstract This study facilitates an effective design and development of various high stretch compression products by analyzing fabric size, stretch properties, and clothing pressure for various knit structures. Four types of fabrics were knitted with polyester SCY (Single Covered Yarn). Then fabric size including weigh…