Materials Literature
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There is a need for a method to facilitate the development of novel, reproducible colloidal surface-enhanced Raman scattering (SERS) substrates to encourage the use of SERS in applied studies. In this study we show for the first time that by using suitably designed SERS experiments in conjunction with multivariate ana…
Different approaches to the deposition of Mn(12) single molecule magnets on the Au(111) surface and their characterization by a broad variety of techniques are investigated with respect to their suitability for a profound corroboration of the integrity of the Mn(12) core. In this context, the most recent improvements…
Fullerene C 60 , C 70 , single-walled and multi-walled carbon nanotubes and graphene sheets are doped to nematic liquid crystal (LC) host in the same percentage. Planar samples of these mixtures are prepared and our measurements constitute an optimization basis for possible applications. Fullerene balls are found to b…
The effects of cyclic extrusion and compression (CEC) processing on the microstructure and mechanical properties of ZK60 Mg alloy were investigated at room temperature. ZK60 alloy was dramatically refined by CEC processing at 350°C. In addition, the initial fiber texture became disintegrated and changed into a {10\\ba…
We report the co-assembly and adsorption properties of coacervate complexes made from polyelectrolyte-neutral block copolymers and oppositely charged nanocolloids. The nanocolloids put under scrutiny were ionic surfactant micelles and highly charged 7 nm cerium oxide (CeO2) nanoparticles. Static and dynamic light scat…
Composites prepared by infiltration of 50- wt% ceria into porous YSZ were investigated for use as H2–H2O electrodes for solid oxide electrolyzers (SOE) or fuel cells (SOFC). Cells prepared from these composites showed excellent performance, with SOFC power densities as high as 1.1 W cm−2 at 1073 K. Further investigati…
The incoherent approximation for the determination of the vibrational density of states of glasses from inelastic neutron or x-ray scattering data is extended to treat the coherent scattering. The method is applied to new room temperature measurements of vitreous silica and germania on the thermal time-of-flight spect…
A joint initiative of the Woodrow Wilson International Center for Scholars and the Grocery Manufacturers Association, this report provides "an initial roadmap through the regulatory process and insights into industry stewardship efforts for a new generation of nano-enabled food packaging applications."
Abstract An efficient method towards water soluble cellodextrine mixtures is described and detailed information on structure analysis is given. For cellulose degradation in good yield, treatment of cellulose with 85% phosphoric acid for 30 minutes at room temperature and a hydrolysis of 20 hours at 55 °C are suitable.…
Electrochemical properties of redox-active self-assembled molecular films of novel metallo-octacarboxyphthalocyanine (MOCPc, M = Fe, Co and Mn) complexes integrated with cysteamine (Cys) monolayer on gold electrodes via amide bonds were investigated. X-Ray photoelectron spectroscopy confirmed the appearance of the var…
Spatially confined self-assembly of peptide amphiphile nanofibers inside liposomes is triggered by light.
Washed human erythrocytes were incubated with titanium dioxide (TiO2) particles at 37 degrees C for 1 hr and hemolysis was determined by the percentage of hemoglobin released (optical density at 540 nm; OD540) from the cells. Effects of TiO2 on OD540 were corrected and dose-response curves were analyzed by the Hill pl…
Dendrimers up to the fourth generation (G1–G4) were successfully synthesized via the efficient copper catalyzed 1,3-dipolar cycloaddition between primary alkynes and azides (CuAAC), also referred to as a click reaction. The synthetic protocol involved the preparation of presynthesized dendron wedges that subsequently…
Research activities on various supercapacitor materials have grown enormously in recent years. Capacitor studies of over a limited potential window in alkaline electrolytes are reported. A high potential window of a capacitor material is desirable for use in a device. Furthermore, as the specific energy and specific p…
A single phase Mg(BH4)2 was successfully synthesized and its hydrogen storage properties were systematically investigated. Depending on the synthesis conditions, Mg(BH4)2 forms low- and high-temperature phases with different crystal structures. The dehydriding reaction of Mg(BH4)2 starts at approximately 500 K, and 14…
BiMnO3−δ compositions differing in oxygen stoichiometry have been synthesized under high pressure. Orthorhombic BiMnO2.99 and monoclinic BiMnO2.84 exhibit canted antiferromagnetism and ferromagnetism respectively. BiMnO2.94 and BiMnO2.89 are also monoclinic and show ferromagnetism, but it seems possible that they may…
Argon (Ar) plasma beam scanning treatments were applied to modify the surfaces of polyimide (PI) films deposited on indium tin oxide glasses in favor of liquid crystal (LC) alignment. LC cells were filled with twist nematic LC (ZLI-2293) on the PI films (Chisso 5310) treated with Ar plasma beam scanning. LC alignment…
The effect of high pressure on the crystal structure of the intermetallic compounds R2Fe17 − x Six (R = Lu or Y; x = 0 or 1.7) was studied using neutron diffraction. A correlation between changes in structural parameters and magnetic properties under the action of high pressure, as well as under chemical substitution…
In order to obtain high-concentration doped erbium ions in silica-based fiber, we manufactured Er3+-Bi3+-Ga3+ co-doped fiber using MCVD and solution doping technique. The concentration of Er3+ in the fiber was about 5.24×1025/m3. We described a new method to measure the degree of clustering in the Er3+-Bi3+-Ga3+ co-do…
Deburring operations with high efficiency and full automation of the conventional burr removal methods are extremely difficult. A promising solution is provided by Electrochemical Deburring (ECD). Successful utilisation of ECD, in present day manufacturing, demands extensive research for economical manufacturing of en…