Materials Literature
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The volatility of compounds formed during heating of trace quantities of 238Pu or 239Pu in a stream of helium and oxygen mixture was studied by gas thermochromatography. Under certain conditions plutonium forms four adsorption zones with the centers at 450±25°C, 250±25°C, 130±50°C and -105±25°C in quartz TC columns. F…
Abstract The thermal stability of polymers is of fundamental importance both in processing and in many applications, eg, injection moulding, hot melts. As part of an investigation to determine the suitability of supramolecular polymers for novel applications in materials science, the thermal behaviour of two model com…
Abstract The influence of high electrical fields (above 20 kV mm −1 ) on ageing, polarization and morphology of polyethylene (PE) is discussed. Infrared and positron annihilation spectroscopy measurements together with capacitance measurements tend to indicate that polymer morphology is modified by high fields. We sho…
Abstract Planetary roller extruders (PREs) are currently being employed first and foremost to feed calender/lamination units, for pelleting, for compounding powdered paint and for the reuse of recyclate. In these disciplines it is the most successful multi‐screw extruder. The range of materials that are compounded ext…
The magnetic properties of a LaMn0.46Co0.54O3 single crystal, grown by electrochemical deposition, are studied in a wide range of fields and temperatures. The two-phase magnetic state model of the crystal is used to analyze the results.
The effects of La-doping and external pressure on the crystal structure of layered perovskite-like manganate Ca3Mn2O7 have been investigated by substituting La3+ for Ca2+ in Ca3Mn2O7 and in situ high pressure energy dispersive X-ray diffraction measurements on Ca3Mn2O7, respectively. With the increase of La3+ content…
Abstract 2,2,2-Tris(diphenylphosphinomethyl)ethane (triphos) coordinates to Co(BF4)2·6H2O to synthesis the red-violet cationic complex of [Co(triphos)(solv)2]2+ (solv: solvent) in THF/EtOH at room temperature. Addition of 2-hydroxy-2-d-carboxylic acids (L) into the cationic solution as co-ligands yields the red-brown…
Many relations between the physical, rheological or mechanical properties of linear polymers and their molar mass are well known. For disperse polymers, parameters that express these relations are typically related to (a combination of) the moments of the molar-mass distribution. Properties of branched, nonlinear poly…
There are two fundamental considerations in preparing samples for electron probe microanalysis (EPMA). The first one may seem obvious, but we often find it is overlooked. That is, the sample analyzed should be representative of the population from which it comes. The second is a direct result of the assumptions in the…
This paper presents detailed morphological descriptions of three small Navicula species that occur rather abundantly in the brackish Baltic Sea, and probably also in brackish waters elsewhere. Two of these, N. sjoersii and N. bossvikensis, are described as new taxa. A morphologically similar species, N. perminuta Grun…
Abstract In situ synchrotron radiation structure analyses of a light-induced radical pair from o-Cl-HABI were performed by using an X-ray vacuum camera at 23–70 K at the BL02B1 station of SPring-8. The combined results of X-ray analysis with theoretical calculation, IR, and UV-vis spectroscopy reveal that a slight con…
Cellulose membranes formed by Acetobacter xylinum under known cell density in a culture medium were characterized. A dead end testing unit was used for water flux and filtration of Chlorella sp. and bovine serum albumin (BSA). This study found that the cells formed membranes faster in sucrose supplemented coconut juic…
To study the strong magneto-volume effects observed in CrTe and MnAs with NiAs-type crystal structure, first-principle band calculations are carried out by a self-consistent linear muffin-tin orbital method within the atomic sphere approximation. The equilibrium volume of the unit cell is obtained as a function of the…
When complexed PSS/CTAB is coadsorbed onto silica, a long-range, predominantly electrosteric repulsion is measured which decays exponentially with surface separation. Adsorption is driven by locally hydrophobic, surfactant-rich regions along the PSS chain. These anchor the PSS chain to the surface, resulting in a clas…
The rheological behaviour and mechanical properties of the polycarbonate/high density polyethylene/glass fiber (PC/HDPE/GF) composites have been studied, along with fiber-resin interface behaviour. Maleic anhydride grafted low density polyethylene (LDPE-g-MAH) was used as a compatibilizer in the composites. A study of…
The failure of a viscoelastic material, such as solid propellant, is a complex phenomenon with a requirement to address the following two fundamental and complementary aspects in the failure criteria. First, what is the failure criterion for a solid propellant in stress–strain space, and what are the variations in fai…
This work proposes a new approach, based on the reaction Si 3 N 4 + 2B 2 O 3 + 9C → 3SiC + 4BN + 6CO, to synthesize an SiC–BN composite. The composite was prepared by reactive hot pressing (RHP), at 2000°C for 60 min at 30 MPa under an argon atmosphere, following a 60 min hold at 1700°C without applied pressure before…
Transverse sections of the (11–20) cuts of a 6H-SiC substrate-porous SiC layer-epitaxial 6H-SiC layer structure were studied using electron microscopy. An intermediate layer is revealed between pores and unetched SiC which consists of a damaged region containing two-dimensional defects and a completely amorphous regio…
The determination of nitroxide concentrations and distributions across plaques of polycarbonate/acrylonitrile-butadiene-styrene copolymer blend (PC/ABS) containing a high molecular weight hindered amine stabilizer (HALS) exposed to thermal and photochemical degradation treatments by EPR and EPR imaging (EPRI) is repor…
Ultrasonic irradiation in the presence of ozone was used to efficiently eliminate methyl tert-butyl ether (MTBE) from groundwater. The sonolytic degradation of MTBE was investigated in three different reactor configurations and frequencies: vibrating-plate reactor (VPR, 358 kHz), near-field acoustical processor (NAP 2…