Materials Literature
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Condensation of hydrazine with 1,3,6,8-tetrakis(4-formylphenyl)pyrene under solvothermal conditions yields highly crystalline two-dimensional covalent organic frameworks. The pyrene units occupy the vertices and the diazabutadiene (-C═N-N═C-) linkers locate the edges of rohmbic-shaped polygon sheets, which further sta…
A systematic and detailed study for size-specific antibacterial efficacy of silver nanoparticles (AgNPs) synthesized using a co-reduction approach is presented here. Nucleation and growth kinetics during the synthesis process was precisely controlled and AgNPs of average size 5, 7, 10, 15, 20, 30, 50, 63, 85, and 100…
We report interesting self-assembly structures of nematic liquid-crystal colloid (NLCC) networks, which are arrested during cooling from the isotropic temperature to room temperature. The NLCC is composed of sterically stabilized colloidal particles and a nematic liquid crystal (NLC) with nematic-isotropic transition…
The use of NaBH4 as a hydrogen storage material suffers to some extent from its deficient stability against chemicals and degradation at elevated temperatures. This disadvantage can be overcome by the use of polyelectrolytes as protective layers. Furthermore, the coating of NaBH4 with polyelectrolytes significantly en…
The basic oxygen steelmaking (BOS) process typically produces a dust rich in valuable iron units and often contaminated with zinc. This paper takes a look at statistical correlation and multiple regressions of process variables with the quantity of dust and the zinc mass contained in the dust. A robust inline sampling…
PLA/PP polymer blends in various ratios (PLA:PP = 9:1, 4:1, 3:1, and 1:1), and their composites (PLA:PP = 1:1) with sisal fiber (10, 15 and 20 wt%) were fabricated using MAPP as compatibilizer. The aim of the work was to reduce the cost of biodegradable composites as well as to improve the impact strength of PLA using…
We evaluated diatom assemblages as indicators of anthropogenic stress from fi fty-four sites, distributed across 1,350 river kms of the Lower Mississippi River (LMR), as part of the National Rivers and Streams Assess- ment. We used multivariate analyses, as well as European- and regionally-derived stressor models, to…
We demonstrate that core/graded-shell CdSe/CdSe1-xSx/CdS giant semiconductor nanocrystals (g-NCs) have robust photoluminescence (PL) temperature response. At a size of 10.2 nm in diameter, these g-NCs undergo a PL drop of only 30% at 355 K relative to their PL intensity at 85 K. In comparison, the core/step-shell CdSe…
The microstructure, martensitic transformation and mechanical properties of as cast Ni 52 Ti 48−x Re x shape memory alloys (SMAs) were investigated. The microstructure of these alloys consists of B19′ martensite phase as a matrix and B2 austenite in small percentages in addition to some precipitations of NiTi intermet…
The connection of a power transformer to the grid is associated with magnetizing inrush currents that may result in power quality issues as well as faulty relay tripping. In distributed generation, the transformer may instead be premagnetized from the source to avoid this. In this paper, a VSI is directly coupled to a…
This study focused on expanding existing knowledge about benthic diatoms and their use as indicators of biological quality and physical disturbance in six Mediterranean watercourses within the Rio Mannu di Porto Torres basin in northwestern Sardinia, Italy. Benthic diatoms were collected from 11 stations during a 1-ye…
The synthesis of carbon nanomaterials (CNMs) by a chemical vapor deposition method using three different plant oils as precursors is presented. Because there are four parameters involved in the synthesis of CNM (i.e., the precursor, reaction temperature of the furnace, catalysts, and the carrier gas), each having thre…
Abstract Polymerbasierte sphärische Aktivkohle (PBSAK) kann durch die Integration von reaktiven Komponenten in das Porensystem funktionalisiert werden. Dadurch erschließen sich neue Anwendungsbereiche für diese Adsorbentien. So kann imprägnierte PBSAK als Breitbandsorbens für Atemschutzanwendungen und zur Entfernung v…
Abstract The article investigates the effects of long term environmental aging on thermal and mechanical properties of epoxy‐silica hybrids. These nanostructured materials, prepared by non‐aqueous sol‐gel process and in situ generation of nanosilica during epoxy curing at room temperature, present the potential to be…
This paper investigates not fully explained voltage offsets observed by several researchers during the measurement of the Seebeck coefficient of high Z materials. These offsets, traditionally attributed to faulty laboratory procedures, have proven to have an irreducible component that cannot be fully eliminated in spi…
Abstract BACKGROUND Biosynthesis of Ag nanoparticles ( AgNPs ) utilizing renewable materials and nontoxic chemicals has become highly desirable and is currently receiving tremendous attention. In this study, a facile and cellulose‐based approach was developed to biosynthesize AgNPs through tandem hydrolysis of silver…
During the last decade, dendritic polymers including random hyperbranched polymers, dendrigrafts, dendrons and dendrimers characterized by a highly branched structure of great regularity, a compact shape, a large number of reactive end groups, and room between the branches for taking up guest molecules have attracted…
Photochromism is a chemical process in which a compound undergoes a reversible change between two states having separate absorption spectra, i.e. different colors. The change of color in one direction occurs under influence of electromagnetic radiation, usually UV light, and in the other direction by altering or remov…
ABSTRACT Chromatography is a widely used technique in protein separation, and the adsorbents are essential to separate target proteins from raw mixtures. In this study, porous cellulose beads were prepared with a direct dissolution of microcrystalline cellulose (MCC) using an ionic liquid solvent 1‐butyl‐3‐methylimida…
First principles calculations are performed to investigate the structural stability, elastic, lattice dynamical and thermal properties of osmium carbides with various crystal structures. Our calculation indicates that the I 4 Te type structure is energetically the most favourable for Os 4 C. Based on stress–strain rel…