Materials Literature
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We present a bio-electrospinning technique for preparing cell-containing, oriented tubular scaffold intended for use as a nerve guide conduit (NGC). With a coaxial spinneret, solutions of PC-12 cells and poly(l-lactic acid) (PLLA) were delivered to the core and shell parts of the spinneret, respectively. When electros…
Monoclinic HfO 2:Eu,M (M = Li, Ta, Nb, V) powders were prepared with the Pechini method. The M-dopants were added for charge compensation of Eu 3+ positioned in Hf (IV) site. This was hoped to enhance the host-to-activator energy transfer and consequently the overall efficiency of X-ray excited luminescence. Only in t…
Abstract 2,2′‐Bis[bis(pentafluorophenyl)boryl]azobenzenes were synthesized. X‐ray crystallographic analysis exhibits a planar core structure of the azobenzene moiety, double intramolecular N–B coordination, and two tetracoordinate boron atoms. The 2,2 ′ ‐diborylazobenzenes show fluorescence emission with orange and re…
Although numerous small molecules have been synthesized with sulfenamide bonds (R(2)N-SR), this is the first report of the synthesis of polysulfenamides. These polymers are readily synthesized at room temperature using secondary diamines and dithiosuccinimides. The dithiosuccinimides were readily synthesized in one st…
Combinatorial pulsed laser deposition (CPLD) using two targets was used to produce a range of transition metal-substituted perovskite-structured Sr(Ti(1-x)M(x))O(3-δ) films on buffered silicon substrates, where M = Fe, Cr, Ni and Mn and x = 0.05-0.5. CPLD produced samples whose composition vs distance fitted a linear…
A water-soluble polycarbonate with dimethylamino pendant groups, poly(2-dimethylaminotrimethylene carbonate) (PDMATC), is synthesized and characterized. First, the six-membered carbonate monomer, 2-dimethylaminotrimethylene carbonate (DMATC), is prepared via the cyclization reaction of 2-(dimethylamino)propane-1,3-dio…
Goethite and kaolinite are ubiquitous in natural environments. In soils they are often cemented together as a binary association, which has a significant influence on the structure and properties of soils. In this study, the mineralogy (using X-ray diffraction [XRD], thermal analyses, and infrared analysis), interacti…
A stable Eu3+ → Eu2+ reduction is accomplished by thermal annealing in N2 ambient of Eu2O3 films deposited by magnetron sputtering on Si substrates. Transmission electron microscopy and x-ray diffraction measurements demonstrate the occurrence of a complex reactivity at the Eu2O3/Si interface, leading to the formation…
Dendrimers are highly branched, open, covalent assemblies of branch cells (monomers) radially attached to a core in successive layers or generations. Major types of dendrimers include polyamidoamine, polypropylenimine, multiple antigen peptide, chiral, and Fréchet-type dendrimers. Their structure and dynamics can be e…
Gold nanoparticles protected by carboxylated alkane thiols were coupled with a BrO 3 – -SO 3 2– /HSO 3 – pH oscillator which had large-amplitude and long-period oscillations. Reversible, repetitive, and sustainable pH-responsive switching between the assembled and disassembled states of the gold nanoparticles was achi…
Natural fiber-reinforced composites were prepared using jute, sisal, and coir fibers as the reinforcement and polypropylene as the matrix. Fiber proportion was varied as a part of the experimental design and composites were characterized for mechanical properties. A set of simple expressions were obtained for predicti…
Abstract The time dependence of the domain switching current density, J sw ( t ), under pulsed voltages on a ferroelectric parallel‐plate capacitor is the consequence of region‐by‐region polarization reversals across the film. As the distributive coercive voltage of domain nucleation increases from zero to the maximum…
Industrial surveys shows that manufacturing companies define the qualities of thermal removing process based on the dimension and physical appearance of the cutting material surface. Therefore, the roughness of the surface area of the material cut by the plasma arc cutting process and the rate of the removed material…
By dynamic light scattering we studied the temperature dependence of scattered intensities and relaxation rates for pure twist and pure bend modes in a colloidal system of BaTiO(3) single domain nanoparticles and liquid crystal octylcyanobiphenyl (8CB) close to the nematic to smectic-A phase transition. From the exper…
We have measured the local structure of superconducting K(0.8)Fe(1.6)Se(2) chalcogenide (T(c) = 31.8 K) by temperature dependent polarized extended x-ray absorption fine structure (EXAFS) at the Fe and Se K-edges. We find that the system is characterized by a large local disorder. The Fe-Se and Fe-Fe distances are fou…
In this article, we study superfluid behavior of a gas of spatially indirect magnetoexcitons with reference to a system of two graphene layers embedded in a multilayer dielectric structure. The system is considered as an alternative of a double quantum well in a GaAs heterostructure. We determine a range of parameters…
The post-functionalization of poly(3-hexylthiophene) (P3HT) via various synthetic routes is reported. Well-defined and monofunctionalized ω-thiol-terminated P3HT, ω-carboxylic acid-terminated P3HT, ω-acrylate-terminated P3HT, and ω-methacrylate-terminated P3HT are obtained in high yields through a straightforward proc…
Bacterial spores, such as those of the Bacillus genus, are extremely resilient, being able to germinate into metabolically active cells after withstanding harsh environmental conditions or aggressive chemical treatments. The toughness of the bacterial spore in combination with the use of spores, such as those of Bacil…
The microstructural and magnetic property changes of DyF(3)-doped (Nd(26.06), Dy(6.51))-Fe(bal) -B(0.97)-M(2.39) (wt. %) (M = Cu, Al, Co, and Nb) sintered magnets as functions of the sintering conditions were studied. The sintering conditions for the optimum core-shell microstructure were determined. When the magnets…
PbS colloidal nanocrystal (NC) assemblies with monomodal and bimodal size distribution have been fabricated by slow evaporation of solvent on silicon substrates. The interparticle distances of the assembled structures have been carefully defined, both in the plane and in the z direction, perpendicular to the substrate…