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Synthesis and preliminary characterization of octakis (chloropropyldimethylsiloxy) octasilsesquioxane

Devaney Ribeiro do Carmo、Newton Luiz Dias Filho、Nelson Ramos Stradiotto2004-09-01Materials Research

Octakis (hydridodimethylsiloxy) octasilsesquioxane was hydrosilated with allyl chloride using Spiers catalyst (H2PtCl6). This reaction was monitored using FT-IR spectroscopy. The synthesized product was characterized by 13C, 29Si NMR (MAS), SEM, FT-IR, Thermogravimetric techniques. The three propyl groups alpha, beta,…

Los Angeles Test and Polished Stone Value of ophite in Cantabria: a petrophysical interpretation

G. Fernández Maroto、L. M. Suárez del Río2004-09-01Materiales de Construccion

Crushed aggregate obtained from certain ophite outcrops in Cantabria was tested with the Los Angeles and polished stone value (PSV) procedures. Linear regression analysis was used to identify the pétrographie parameters that account for aggregate performance in these two tests. The most abundant and common minerals in…

''Geopolymers": same basic chemistry, different microstructures

A. Palomo、A. Fernández-Jiménez、M. Criado2004-09-01Materiales de Construccion

The present paper describes the effect of certain working variables on the microstructural evolution of oven-dried, alkali-activated fly ash. The results show that the main reaction product in the activation process (in all the systems studied) is an amorphous aluminosilicate gel with a three-dimensional structure. No…

Thin copolymer-cased light-emitting display made with fluorine-foped tin oxide substrates

Rudolf Lessmann、Ivo Alexandre Hümmelgen2004-09-01Materials Research

Seven-segment displays are used to show numerical quantities in electronic equipment, being present in most of the low-end electronics. In this work we describe a novel organic light emitting display made with poly(1,10 decanedioxy 2 methoxy - 1,2 phenylene - 1,2 ethenylene - 3,6 dimethoxy - 1,4 phenylene - 1,2 etheny…

HPMA and HEMA copolymer bead interactions with eukaryotic cells

Cristina D. Vianna-Soares、Kim Cherng-Ju、Kadriye Ciftci 等 4 位作者2004-09-01Materials Research

Two different hydrophilic acrylate beads were prepared via aqueous suspension polymerization. Beads produced of a hydroxypropyl methacrylate (HPMA) and ethyleneglycol methacrylate (EDMA) copolymer were obtained using a polyvinyl alcohol suspending medium. Copolymers of 2hydroxyethyl methacrylate (HEMA), methyl methacr…

Microstructure and mechanical properties of WC-Co reinforced with NbC

Wilson Acchar、Cordt Zollfrank、Peter Greil2004-09-01Materials Research

Cemented carbides such as tungsten carbide-cobalt WC-Co composites have been widely used as cutting tool materials. Several reports have shown the influence of different factors such as grain size, type and amount of binder phase and the addition of hard particles on the properties of WC-Co. The purpose of this work w…

The use of a vickers indenter in depth sensing indentation for measuring elastic modulus and vickers hardness

Adonias Ribeiro Franco Jr.、Giuseppe Pintaúde、Amilton Sinatora 等 5 位作者2004-09-01Materials Research

Depth sensing indentation is a powerful experimental technique for determining mechanical properties of materials. In this work a computational routine was developed based on Oliver-Pharr method for measuring a more precise values of elastic modulus using a Fischerscope H100 depth sensing indentation apparatus, with a…

Effect of the deposition conditions of platinum electrodes on their performance as resistive heating elements

Andrei Ionut Mardare、Cezarina Cela Mardare、Ednan Joanni2004-09-01Materials Research

The performance of different platinum electrodes used as resistive heating elements was studied. Pt films having different thickness were deposited by RF magnetron sputtering at room temperature followed by post-deposition annealing at 700 ºC or made in-situ at 700 ºC. The Pt films were deposited over oxidized silicon…

Nucleation and growth microstructural study of ti films on 304 SS substrates

Rogério de Almeida Vieira、Maria do Carmo de Andrade Nono2004-09-01Materials Research

Coating of steel surfaces with titanium films has been studied with the objective to protect them against corrosion, and to create an intermediate film for CVD diamond and TiN film deposition. In this work, the nucleation, growth mechanisms and microstructural formation of the titanium films deposited on 304 stainless…

Effects of annealing on electrical and optical properties of a multilayer InAs/GaAs quantum dots system

Adenilson José Chiquito、Yuri Alexander Pusep、Sérgio Mergulhão 等 6 位作者2004-09-01Materials Research

A systematic investigation of the properties of the InAs/GaAs self-assembled quantum dots (SAQDs) system subjected to a post-growth annealing using capacitance-voltage, Raman scattering and photoluminescence measurements is presented. The application of both electrical and optical methods allowed us to obtain reliable…

The Monastery of Uclés (Cuenca, Spain): characterization and deterioration of building materials

M. Álvarez De Buergo、R. Fort、M. Gómez-Heras2004-09-01Materiales de Construccion

Building materials from the Monastery of Uclés façades, in Cuenca (16th-18 th centuries), have been characterised, as well as identified their deterioration forms. Characterization consisted of the determination o mineralogical and petrographical properties of building materials; petrophysical and petrochemical charac…