Materials Literature
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Over the last two decades, several methods, of increasing sophistication, have evolved to measure boundary plane orientation by electron backscatter diffraction. Originally, metallographic sectioning was used to obtain the location of the boundary plane. The most recently designed approach allows the relative frequenc…
[001]-poled relaxor based ferroelectric Pb(Zn1∕3Nb2∕3)O3–(6–7)%PbTiO3 single crystals of [110]-length cut exhibit k31≈0.85 and very high d31∕s11E value. They are promising materials for sensors and actuators comprising an elastic substrate such as a metal shim or support, especially under dynamic loading conditions. I…
Abstract The reaction of iron(II) acetate with the tetradentate Schiff base like ligands H 2 L1 ((E,E)‐[{diethyl 2,2′‐[1,2‐phenylenebis‐(iminomethylidyne)]bis[3‐oxobutanato]}]) and H 2 L2 ([([3,3′]‐[1,2‐phenylenebis(iminomethylidyne)]bis(2,4‐pentane‐dionato)(2‐)‐N,N′,O2,O2′]) in the presence of 1‐meim (1‐methylimidazo…
We report on the contribution of optical phonon decay into acoustic phonon to the thermal conductivity [k(T)] of semiconductors. We have considered this mechanism as an acoustic phonon generation rate within the full modified Callaway theory to accurately describe experimental data of k(T) for Ge as a function of isot…
A focused ion beam (FIB) is used to sequentially reduce the contact length of an evaporated metal film to a multiwalled carbon nanotube (MWCNT). By using this FIB contact cutback technique, the contact resistance between an individual MWCNT and evaporated thin films of Au, Au∕Ti, and Ag are accurately determined. The…
Electrodeposited nanocrystalline materials are expected to have a homogeneous grain size and a narrow grain size distribution. In Co-Ni electrodeposited films, however, under certain conditions an undesired columnar grain structure is formed. Fully automated three-dimensional (3D) orientation microscopy, consisting of…
Abstract Nanocrystalline particles of Co 2+ doped lithium aluminate (Co 2+ :LAO) and Ni 2+ ‐doped lithium aluminate (Ni 2+ :LAO) were synthesized by sol–gel method. The crystalline nature and particle size of the samples were characterized by X‐ray diffraction analysis (XRD). The morphology and the presence Co 2+ and…
Echt süß: Doppelt hydrophile Blockcopolymere mit Glucoseresten bilden in wässriger Lösung Vesikel mit Zuckereinheiten auf der Oberfläche, die mit Zellen wechselwirken. Die „Sprache“ dieser Assoziation wurde untersucht, und die Informationsübertragung wurde durch Farbstofftransport von einem Vesikel zur Zelle nachgewie…
Abstract Monodispersed zinc oxide (ZnO) whiskers with different aspect ratios were successfully prepared via a simple solution route at low temperature. It is found that the diameter and aspect ratio of ZnO whiskers depend critically on the structure and type of ionic surfactant added in the reaction solution. To furt…
The pressure ($p$) -- temperature ($T$) phase diagram for microscopic magnetism in the multiferroic compound HoMn$_{2}$O$_{5}$ was established using neutron diffraction measurements under a hydrostatic pressure up to 1.25 GPa. At ambient pressure, incommensurate--commensurate--incommensurate magnetic phase transitions…
We carried out chymotryptic digestion of multimeric ATP-dependent Lon protease from Escherichia coli. Four regions sensitive to proteolytic digestion were located in the enzyme and several fragments corresponding to the individual structural domains of the enzyme or their combinations were isolated. It was shown that…
The scanning electron microscopy-based electron backscatter diffraction technique has been used to determine grain orientations of abnormally grown grains upon annealing in nanocrystalline Ni and Ni-20 at.% Fe electrodeposits. The results show that in nanocrystalline Ni and Ni-Fe, the first grown grains that can be de…
The optimization of magnetic and physical properties of electrical steel is imperative for many engineering applications. The key factors to improve magnetic properties are the steel composition as well as control of the crystallographic orientation and microstructure of the steel during processing. However, this requ…
The effect of ultraviolet (UV) photon assisted annealing on the structural, dielectric, and insulating properties of barium strontium titanate (BST) thin films was investigated. Isothermal-temporal annealing experiments revealed that the films annealed utilizing UV assist possessed enhanced crystallization and lattice…
Abstract We present an analytical device model for a graphene field‐effect transistor (GFET) on a highly conducting substrate, playing the role of the back gate, with relatively short top gate which controls the source–drain current The equations of the GFET device model include the Poisson equation in the weak nonloc…
The photovoltaic properties of Si∕SiO2 multiple quantum wells (QWs) embedded in lateral Schottky contacts are investigated. The QWs were fabricated by remote plasma enhanced chemical vapor deposition. By subsequent rapid thermal annealing, the two-dimensional Si layers are partially recrystallized, which gives rise to…
Abstract Chlorine‐doped ZnO thin films were grown by MOCVD on sapphire and fused silica. Chlorine is incorporated in substitution for oxygen and acts as a donor, leading to an increase of electron concentration. Transport properties were studied for samples with different chlorine content. Hall effect measurements sho…
In situ electron backscatter diffraction microstructural analysis of recrystallizing interstitial free steels deformed to strains of 0.75 and 1.6 has been carried out in a FEG-SEM. The experimental procedures are discussed, and it is shown that there is no degradation of the electron backscatter diffraction patterns a…
A contribution is made to the study of the negative difference effect (NDE) for AZ91 corroding in 1N NaCl. The volume of evolved hydrogen, the weight loss and the mass of Mg2+ ions was measured for applied current densities from 0 to 6 mA/cm2. The experimental results agreed with the standard model of Mg corrosion inv…
Engineering quantum dots (QDs) with a paramagnetic nitroxide radical tail yields a weakly fluorescent spin-labeled QD conjugate. Quenching of the intrinsic fluorescence of the QDs results from electron transfer between the QDs and nitroxide radical. Interestingly, when the paramagnetic properties of the nitroxide moie…