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第 196671 / 201947 页 · 当前展示 3,933,401–3,933,420 / 4,038,940 条匹配结果 · 摘要仅作预览

Influence of the counterion on the coordinating properties of (2,2′-bipyridyl)bis(oxalato)chromate(III) anion: crystal structures and magnetic properties of AsPh4[Cr(bipy)(ox)2]·H2O and [NaCr(bipy)(ox)2(H2O)]·2H2O

M. Carmen Muñoz、Miguel Julve、Francesc Lloret 等 5 位作者1998-01-01Journal of the Chemical Society Dalton Transactions

Two new chromium(III)-containing complexes of formula AsPh4[Cr(bipy)(ox)2]·H2O 1 and [NaCr(bipy)(ox)2(H2O)]· 2H2O 2 (bipy = 2,2′-bipyridine and ox = oxalate dianion) have been synthesized and characterized by single-crystal X-ray diffraction. The structure of 1 consists of discrete [Cr(bipy)(ox)2]– mononuclear anions,…

Metal-Organic Frameworks: Synthesis and ApplicationsMetal complexes synthesis and propertiesMagnetism in coordination complexes

Nature of the Blue-Phase-III–isotropic critical point: An analogy with the liquid-gas transition

М. А. Анисимов、V. A. Agayan、Peter J. Collings1998-01-01Physical review. E, Statistical physics, plasmas, fluids, and related interdisciplinary topics

The analogy with the liquid-gas critical point is analyzed to clarify the nature of the pretransitional behavior of physical properties in the vicinity of the Blue-Phase-III--isotropic transition in chiral liquid crystalline systems. The analogy is unusual: temperature serves as the ordering field and entropy plays th…

Liquid Crystal Research AdvancementsMaterial Dynamics and PropertiesMolecular spectroscopy and chirality

Catalysis by heteropoly compounds Part 39 The structure and redox behaviour of vanadium species in molybdovanadophosphoric acid catalysts during partial oxidation of isobutane

Kei Inumaru、Akiko Ono、Hiroshi Kubo 等 4 位作者1998-01-01Journal of the Chemical Society Faraday Transactions

The states and roles of vanadium of 11-molybdo-1-vanadophosphoric acid (H4PMo11VO40, PMo11V) catalyst in the partial oxidation of isobutane (2-methylpropane) were analysed by EPR, 51V and 31P NMR, IR spectroscopy, and redox titration, and compared with dodecamolybdophosphoric acid (H3PMo12O40, PMo12) catalyst. Thermal…

Polyoxometalates: Synthesis and ApplicationsCatalysis and Oxidation ReactionsChemical Synthesis and Reactions

Adsorption of albumin, collagen, and fibronectin on the surface of poly(hydroxybutyrate-hydroxyvalerate) (PHB/HV) and of poly(ε-caprolactone) (PCL) films modified by an alkaline hydrolysis and of poly(ethylene terephtalate) (PET) track-etched membranes

Laurence Rouxhet、Florence Duhoux、Olga Borecky 等 5 位作者1998-01-01Journal of Biomaterials Science Polymer Edition

The effect of alkaline hydrolysis on several surface properties of poly(hydroxybutyrate-hydroxyvalerate) (92/8) (PHB/HV) and poly(epsilon-caprolactone) (PCL) films and of poly(ethylene terephtalate) (PET) track-etched membranes have been characterized, as well as the adsorption of three proteins normally encountered b…

biodegradable polymer synthesis and propertiesElectrospun Nanofibers in Biomedical ApplicationsPolymer Surface Interaction Studies

A time-resolved reflectivity study of the amorphous-to-crystalline transformation kinetics in dc-magnetron sputtered indium tin oxide

Cleva W. Ow‐Yang、Doren Spinner、Yuzo Shigesato 等 4 位作者1998-01-01Journal of Applied Physics

Amorphous tin-doped indium oxide (ITO) was deposited to a thickness of 110 nm on 〈100〉-oriented Si substrates at ∼40–60 °C by dc-magnetron sputtering under a total Ar pressure of 2 Pa. The kinetics of crystallization of the a-ITO films in flowing N2 were investigated by in situ time-resolved reflectivity. The microstr…

ZnO doping and propertiesThin-Film Transistor TechnologiesTransition Metal Oxide Nanomaterials

Crystal structure determination

W. Clegg1998-01-01Medical Entomology and Zoology

1. The basis of the method 2. The method step by step 3. The method illustrated by edxamples 4. Further topics Appendix (Answers to problems)

X-ray Diffraction in Crystallography

Doxorubicin entrapped in sterically stabilized liposomes: effects on bacterial blood clearance capacity of the mononuclear phagocyte system.

G. Storm、M. T. ten Kate、Peter K. Working 等 4 位作者1998-01-01PubMed

The introduction of long-circulating liposomes sterically stabilized by surface coating with polyethylene glycol has expanded the potential for drug targeting to tumors. In recent clinical studies, evidence of significant antitumor activity has been obtained with the industrially prepared formulation of long-circulati…

Nanoparticle-Based Drug DeliveryNanoplatforms for cancer theranosticsCancer Research and Treatments

A novel ‘build-bottle-around-ship’ method to encapsulate metalloporphyrins in zeolite-Y. An efficient biomimetic catalyst

Bi‐Zeng Zhan、Xiaoyuan Li1998-01-01Chemical Communications

Electrostatic interaction is introduced between the host and guest in the synthesis of faujasite-Y confined metallotetrakis(N,N,N-trimethylanilinium) porphyrin cations (MTMAnP4+); the synthesized composites display high catalytic activity in the oxidation of cyclohexene.

Porphyrin and Phthalocyanine ChemistryMetal-Catalyzed Oxygenation MechanismsSurface Chemistry and Catalysis

Synthesis of phthalocyanine-doped silica mesostructured materials by ferrocenyl surfactant

Hao Zhou、Hisahiro Sasabe、Itaru Honma1998-01-01Journal of Materials Chemistry

Photosensitive copper phthalocyanine-(CuPc) doped silica mesoporous materials (in powder) have been directly synthesized by a self-organizing coassembly process using a functional surfactant, 11-ferrocenyltrimethylundecylammonium (ferrocenyl TMA) molecules. This simple method shows that it is not necessary to dope mol…

Mesoporous Materials and CatalysisPorphyrin and Phthalocyanine ChemistrySurface Chemistry and Catalysis

Layer Charge Estimation of Smectites Using Infrared Spectroscopy

Sabine Petit1998-01-01Clay Minerals

A new method of measuring the layer charge of smectites by IR spectroscopy is proposed based on the integrated intensity measurement of the band assigned to the ammonium fundamental upsilon 4 mode of NH (super +) 4 -exchanged clays. Measurements are made before and after Li fixation (Hofman & Klemen effect). These all…

Mesoporous Materials and CatalysisClay minerals and soil interactionsIron oxide chemistry and applications

SYNTHESIS OF METAL OXIDE PARTICLES FROM AQUEOUS MEDIA: THE HOMOGENEOUS ALKALIN1ZAT1ON METHOD

Galo J. de A. A. Soler-Iltia、Matı́as Jobbágy、Roberto Candal 等 5 位作者1998-01-01Journal of Dispersion Science and Technology

An analysis of the urea method as a way to synthesize uniform colloidal particles is presented. Various selected cases of precipitation and coprecipitation are reviewed to illustrate the inherent complexities of the method. The importance of the kinetics of urea hydrolysis is recognized. The concept of trajectory is u…

Adsorption and biosorption for pollutant removalSurfactants and Colloidal SystemsMesoporous Materials and Catalysis

Synthesis of 3,4-diarylpyrroles and conversion into dodecaarylporphyrins; a new approach to porphyrins with altered redox potentials

Noboru Ono、Hirokazu Miyagawa、Takahiro Ueta 等 5 位作者1998-01-01Journal of the Chemical Society Perkin Transactions 1

3,4-Diarylpyrroles (1) have been directly prepared in 20–50% yield by the reaction of β-nitrostyrenes with aqueous TiCl3 in 1,4-dioxane. Pyrroles 1 were also prepared via Barton–Zard pyrrole synthesis using the reaction of α-nitrostilbenes with ethyl isocyanoacetate followed by de-ethoxycarbonylation. 3,4-Diarylpyrrol…

Porphyrin and Phthalocyanine ChemistryMetal-Catalyzed Oxygenation MechanismsSynthesis and Characterization of Pyrroles

Assembly of alternating TiO2/v\CdS nanoparticle composite films

Encai Hao、Bai Yang、Junhu Zhang 等 6 位作者1998-01-01Journal of Materials Chemistry

A composite film comprising TiO2 and CdS nanoparticles was fabricated based on an alternating deposition method; this was confirmed by UV–VIS spectroscopy, TEM, and photocurrent measurements.

TiO2 Photocatalysis and Solar CellsAdvanced Photocatalysis TechniquesQuantum Dots Synthesis And Properties

Crystal structure, ferromagnetic ordering and magnetic anisotropy for two cyano-bridged bimetallic compounds of formula Mn2(H2O)5Mo(CN)7·nH2O

Joulia Larionova≠、J. Sanchíz、Olivier Kahn 等 5 位作者1998-01-01Chemical Communications

Slow diffusion of aqueous solutions containing K4[MoIII(CN)7]·2H2O and a MnII salt, respectively, affords well shaped single crystals of two cyano-bridged bimetallic phases ordering ferromagnetically with a pronounced magnetic anisotropy in the magnetically-ordered phase.

Magnetism in coordination complexesLanthanide and Transition Metal ComplexesAdvanced NMR Techniques and Applications

Modified Mg–Al hydrotalcite: a highly active heterogeneous base catalyst for cyanoethylation of alcohols

Pramod S. Kumbhar1998-01-01Chemical Communications

Modified Mg–Al hydrotalcite (Mg:Al = 3:1) prepared by thermal decarbonation followed by rehydration of a conventional Mg–Al hydrotalcite is found to be a highly active, reusable and air stable catalyst for cyanoethylation of alcohols.

Chemical Synthesis and ReactionsLayered Double Hydroxides Synthesis and ApplicationsMagnesium Oxide Properties and Applications

Synthesis and Magnetic Properties of Four New (Cu−Ni)2 Tetranuclear Complexes of General Formula [Cu(oxpn)Ni(μ-NCS)(H2O)(aa)]2(X)2 (oxpn = N,N‘-Bis(3-aminopropyl)oxamide; aa = Bidentate Amine; X = ClO4- or PF6-). Ferro- and Antiferromagnetic Alternation

Joan Ribas、C. Díaz、R. Costa 等 7 位作者1998-01-01Inorganic Chemistry

The reaction of ethanolic/water solutions of NiX 2 ·6H 2 O (X = NO 3 -, ClO 4 - ), bidentate amine N,N,N‘,N ‘-tetramethylethylenediamine (tmen) and N,N,N ‘-trimethylethylenediamine (trimen) with [Cu(oxpn)] (oxpn = N, N ‘-bis(3-aminopropyloxamide) and ammonium thiocyanate, in the presence of ammonium hexafluorophosphat…

Metal complexes synthesis and propertiesMagnetism in coordination complexesLanthanide and Transition Metal Complexes

Polymer Inclusion Compounds

Lei Huang、Alan E. Tonelli1998-01-01Journal of macromolecular science. Part C, Reviews in macromolecular chemistry and physics/Journal of macromolecular science. Reviews in macromolecular chemistry and physics

1. INTRODUCTION 1.1. Background Schlenk was the first to use the term inclusion compound (IC) to describe the crystalline adducts in which one component (host molecule) crystallizes into a matrix, isolating the second component (guest molecule) into cavities of well-defined geometry [1]. Most of the ICs reported have…

Advanced Polymer Synthesis and Characterizationbiodegradable polymer synthesis and propertiesCarbon dioxide utilization in catalysis

Carbon and energy flux constraints in continuous cultures of Alcaligenes eutrophus grown on phenol

David R. Leonard、N.D. Lindley1998-01-01Microbiology

Summary: The growth behaviour of Alcaligenes eutrophus on phenol was investigated in continuous cultures to identify the phenomena limiting both growth efficiency and substrate degradation rates. It was shown that the fixed stoichiometry of the meta pathway of phenol degradation, leading to equimolar quantities of pyr…

Enzyme Catalysis and Immobilizationbiodegradable polymer synthesis and propertiesMicrobial Metabolic Engineering and Bioproduction

XAFS study of zirconia-supported copper catalysts for the NO–CO reaction: Deactivation, rejuvenation and stabilization of Cu species

Yasuaki Okamoto、Takeshi Kubota、Hideki Gotoh 等 7 位作者1998-01-01Journal of the Chemical Society Faraday Transactions

A Cu/ZrO2 (1 wt.% Cu) catalyst shows high activity for the NO–CO reaction, even at low temperature (100–200 °C). However, the low-temperature activity is easily lost during prolonged reaction at 250 °C. The activity of the deactivated Cu/ZrO2 catalyst is completely restored by NO treatment (1% in He) at >250 °C or O2…

Catalytic Processes in Materials ScienceNanomaterials for catalytic reactionsPigment Synthesis and Properties

Highly polarized electron donors, acceptors and donor–acceptor compounds for organic conductors

Yoshiro Yamashita、Masaaki Tomura1998-01-01Journal of Materials Chemistry

New types of π-electron donors and acceptors with high polarizability are reviewed. TTF derivatives with polarizable substituents, π-extended TTF analogues fused with nitrogen-containing heterocycles and non-TTF donors (i.e. electron donors) and chalcogen atom-containing quinones, TCNQ and DCNQI analogues (i.e. electr…

Magnetism in coordination complexesMolecular Junctions and NanostructuresOrganic and Molecular Conductors Research