Materials Literature
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Abstract A series of azobenzene derivatives containing glycine, l-alanine, l-valine, l-leucine, and l-isoleucine were synthesized and their gelation properties were examined. Although the azobenzene derivatives containing glycine, l-alanine, and l-leucine exhibited very low gelation abilities, other compounds of l-iso…
A common problem in synthetic organic chemistry is attaining proper contact between lipophilic organic compounds and inorganic salts. Various strategies, for example, phase transfer catalysis (Starks, C. M.; Liotta, C. L.; Halpern, M. Phase Transfer Catalysis: Fundamentals, Applications and Industrial Perspectives; Ch…
The clay minerals in Podzols and podzolic soils developed under coniferous forests in the Subarctic and Cool-temperate zones are characterized by the predominance of smectite and/or mica-smectite interstratified minerals in the eluvial horizons and chlorite-vermiculite intergrade in the illuvial horizons. A large amou…
This work reports the effect of pH on the process of mullite formation from mixtures of alumina and silica sols. The pH of the mixtures determines the charges of particle surfaces and affects their interactions and distributions. Mullite formation from amorphous precursors with an Al:Si molar ratio of 1:3, prepared fr…
Analysis of polarization curves and impedance spectra has shown that the surface chemistry of galvanized steels plays an important role in determining their corrosion behavior. Zn-Ni samples that were untreated or had been treated in a 10 mM Ce(NO3)3 solution had the lowest corrosion rates in 0.5 N NaCl. The efficienc…
Halloysite template has a tubular microstructure; its wall has a multi-layer aluminosilicate structure. A new catalytic method is adopted here, through the in-situ reduction of Pd ions on the surface of tubular halloysite by methanol to initiate electroless plating; the detailed deposition features of Pd nanoparticles…
A novel polymer thin film embedded carbon nanotube (PECNT) sensor was developed for ultra-low-power micro thermal sensing. The basic fabrication process of this sensor includes AC electrophoretic manipulation of multi-walled carbon nanotubes (MWNT) bundles on a silicon substrate and embedding them inside parylene C la…
The guanidinium chloride- and urea-induced unfolding of FprA, a mycobacterium NADPH-ferredoxin reductase, was examined in detail using multiple spectroscopic techniques, enzyme activity measurements and size exclusion chromatography. The equilibrium unfolding of FprA by urea is a cooperative process where no stabiliza…
In order to optimise the hot die processes of Ti–10V–2Fe–3Al alloy, the effects of forging processes on the microstructures and mechanical properties were studied and processing maps were used to try to aid the process design. The results show that processing maps for Ti–10V–2Fe–3Al alloy exhibit three process ranges,…
The association of the cationic dye indoheptamethine cyanine with various anionic dyes (four sulfonephthaleins and five xanthenes) in aqueous solutions was detected using the Vis-spectroscopic method. The values of the association constants are within the range (10(4) to 7×10(7) mol-1 L). In all the cases a substantia…
Abstract The interactions of hardness ions (i. e., Ca, Mg, Ba) with anionic polymeric scale inhibitors (SI) containing different functional groups has been investigated using a turbidity technique. It has been found that all SI tested form insoluble salts with hardness ions under the experimental conditions used (pH 7…
As a function of film orientation, the intrinsic effective piezoelectric coefficient e31,f is generally formulated for a substrate-constrained ferroelectric film. Numerical results are obtained for Pb(ZrxTi1−x)O3 (PZT) thin films with tetragonal and rhombohedral compositions. It is illustrated that the optimal orienta…
Abstract The liquid‐crystalline behaviour of copper( II ) and nickel( II ) complexes of a mesogenic Schiff‐base ligand derived from N , N' ‐disalicylidene‐1,2‐phenylenediamine (salophenH 2 ) and of the corresponding trinuclear mixed copper( II )/lanthanum( III ) and nickel( II )/lanthanum( III ) complexes was investig…
The structures of eight heterophase interfaces between cubic ZrO2 and NiO simulated by molecular dynamics (MD) are compared with those of the corresponding isolated surfaces to better understand the factors influencing interface formation and coherency in ceramic oxides. The near coincident site lattice (NCSL) theory…
The rates of DPPH (diphenylpicrylhydrazyl) trapping and the sonolytical products obtained during the sonolysis of thioethers at normal and low temperature are reported. CS2, lower sulfides, thiophene, and sulfurized species are the common products during the ultrasonic irradiations. Hydrocarbons are also obtained duri…
(1-x)Pb(Mg1/3Nb2/3)O3-xPbTiO3 (PMN-PT) and (1-x)Pb(Zn1/3Nb2/3)O3-xPbTiO3 (PZN-PT) single crystals are considered to behave like soft Pb(Zr,Ti)O3 (PZT) ceramics because of their small mechanical quality factor Qm and poor stability under external disturbances (Qm > 500-1000 for hard PZT ceramic, and Qm < 100 for soft P…
This paper describes various illumination and image processing techniques for yarn characterization. Darkfield and back-lit illuminations are compared in terms of depth of field tolerance and image quality. Experiments show that back-lit illumination is superior in terms of depth of field tolerance and contrast. Three…
A novel retrocommunication link utilizing reflective multiple quantum well (MQW) optical modulators and nonmechanical beam steering and tracking is demonstrated. Large aperture reflective MQW modulators using AlGaAs/GaAs are optimized and manufactured. The modulators exhibit a contrast ratio larger than 4:1 and a modu…
ABSTRACT: The combined effects of mica (0% to 1.2% [w/w]), carnauba wax (0% to 0.8% [w/w]), glycerol (0% to 6% [w/w]), and sodium caseinate (10% to 13% [w/w]) concentrations on water vapor barrier and mechanical properties of coated paper were studied. A Doehlert matrice was used to investigate the main effects of the…
Abstract Based on the [2‐(2‐nitrophenyl)propoxy]carbonyl (nppoc) group, six new photolabile protecting groups ( 2, 8, 9b, 16b, 25b , and 26 ), each covalently linked to a 9 H ‐thioxanthen‐9‐one (Tx) unit functioning as an intramolecular triplet sensitizer, were synthesized. Linkers were introduced between the Me group…