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Scanning Electron and Ion Microscopy of Nanostructures

Natasha Erdman、David C. Bell2015-08-10Royal Society of Chemistry eBooks

This chapter discusses the basic principles of scanning electron microscopy (SEM) and scanning helium ion microscopy (HeIM) and their application to nanoscale imaging and microanalysis. Different modes of imaging and their advantages for the examination of nanostructures are explained. A review of microscope design is…

Advanced Electron Microscopy Techniques and ApplicationsElectron and X-Ray Spectroscopy TechniquesIon-surface interactions and analysis

Benchmark calculations on the nuclear quadrupole-coupling parameters for open-shell molecules using non-relativistic and scalar-relativistic coupled-cluster methods

Lan Cheng2015-08-10The Journal of Chemical Physics

Quantum-chemical computations of nuclear quadrupole-coupling parameters for 24 open-shell states of small molecules based on non-relativistic and spin-free exact two-component (SFX2C) relativistic equation-of-motion coupled-cluster (EOM-CC) as well as spin-orbital-based restricted open-shell Hartree-Fock coupled-clust…

Advanced Chemical Physics StudiesSolid-state spectroscopy and crystallographyMolecular Spectroscopy and Structure

Infrared absorption modeling of VOx microbolometer

Mehdi Aggoun、Jianliang Jiang、Mughees Khan2015-08-10Proceedings of SPIE, the International Society for Optical Engineering/Proceedings of SPIE

The absorption model plays an important role in the design of the microbolometer structure regarding the determination of the optimum thickness of the structure layers. Moreover, the infrared absorption depends on the wavelength of the radiation and the material properties. In this paper, we presented an Infrared abso…

Transition Metal Oxide NanomaterialsInfrared Target Detection MethodologiesThermal Radiation and Cooling Technologies

Study on thermal properties of poly(vinyl alcohol) and polyurethane composites with multiwalled carbon nanotubes/silica nanohybrids

Hongyan Xie、Qing Ye、Jin Liu 等 7 位作者2015-08-10Journal of Thermoplastic Composite Materials

Two kinds of multiwalled carbon nanotubes/silica nanohybrids (CNTs/SiO 2 ) were synthesized via a sol–gel method by coating SiO 2 on the surfaces of CNTs that had been functionalized with poly(sodium- p-styrenesulfonate) (PSS). The influence of the nanohybrids on the thermal properties of poly(vinyl alcohol) (PVA) and…

Supercapacitor Materials and FabricationPolymer Nanocomposites and PropertiesConducting polymers and applications

Structural Integrity Issues in High Temperature Nuclear Plant: Experience from Operation of the UK Advanced Gas Cooled Reactor Fleet

David Dean、Julian G Johns2015-08-10NCSU Libraries Repository (North Carolina State University Libraries)

The Advanced Gas Cooled Reactor (AGR) fleet operated by EDF Energy in the UK are a unique example of high temperature civil nuclear plant that has operated commercially over significant timescales.AGR plant contain a graphite core with carbon dioxide used as the primary coolant and importantly key metallic boiler, rea…

Nuclear Materials and PropertiesGraphite, nuclear technology, radiation studiesNuclear and radioactivity studies

Keyway Root Crack Arrest in an AGR Graphite Brick

Muhammad Treifi、Barry Marsden、Graham Hall 等 4 位作者2015-08-10NCSU Libraries Repository (North Carolina State University Libraries)

The graphite bricks in an advanced gas-cooled reactor (AGR) core are subject to fast neutron irradiation which leads to significant dimensional and material properties changes. These changes vary across the relatively thick (~100mm) wall section of a typical graphite moderator brick due to the fluence and temperature…

Graphite, nuclear technology, radiation studies

Combustive Properties of Specimens Treated with Methylenepiperazinomethyl-Bis-Phosphonic Acid (Mn+)s

Yeong-Jin Chung2015-08-10Applied Chemistry for Engineering

이 연구에서는 메틸렌피페라지노메틸-비스-포스폰산 금속염( $PIPEABPM^{n+}$ )과 메틸렌피페라지노메틸-비스-포스폰산(PIPEABP)으로 처리된 리기다 소나무의 연소성을 시험하였다. 15 wt%의 메틸렌피페라지노메틸-비스-포스폰산 금속염과 메틸렌피페라지노메틸-비스-포스폰산 수용액으로 각각 리기다 소나무에 3회 붓칠하여 실온에서 건조시킨 후, 콘칼로리미터(ISO 5660-1)를 이용하여 연소성을 시험하였다. 그 결과, 메틸렌피페라지노메틸-비스-포스폰산 금속염으로 처리한 시험편은 메틸렌피페라지노메틸-비스-포스폰산을 처리한 시험편에 비해 최대질량감소율( $MLR_…

Risk and Safety AnalysisThermal and Kinetic AnalysisMarine and Coastal Research

Development of Friction Type EQS for APR1400 Nuclear Power Plant

Hong-Pyo Lee、Myung-Sug Cho、Keun-Kyeong Kim 等 4 位作者2015-08-10NCSU Libraries Repository (North Carolina State University Libraries)

This paper presents the development of the friction-type Eradi-Quake System (EQS) for APR 1400 NPP.Consisting of a sliding bearing assembly with damping and mass energy regulator spring, EQS is the seismic isolation system to be applied widely to industrial facilities.For the nuclear power plant structure, the seismic…

Nuclear Materials and PropertiesNuclear Engineering Thermal-HydraulicsNuclear and radioactivity studies

Unravelling Radicals Reactivity Towards Carbon Nanotubes Manipulation/Functionalization

Zois Syrgiannis、Aurelio Bonasera、Eleonora Tenori 等 4 位作者2015-08-10Current Organic Chemistry

Carbon Nanotubes (CNTs) chemistry is under constant evolution, as a consequence of the deep interest of the scientific community in finding new applications for these versatile materials. New and old synthetic protocols are used for improving the control of the functionalization degree of the final materials and for o…

Carbon Nanotubes in CompositesConducting polymers and applicationsFullerene Chemistry and Applications

High temperature coefficient of resistance for a ferroelectric tunnel junction

Xiaolin Zhao、Jianlu Wang、Bobo Tian 等 13 位作者2015-08-10Applied Physics Letters

An infrared detector is proposed that is based on a ferroelectric tunnel junction (FTJ) working under bolometer-like principles. Electron tunneling, either direct or indirect, through the ferroelectric barrier depends on the temperature of the devices. During tunneling, infrared radiation alters the polarization of th…

Gas Sensing Nanomaterials and SensorsTransition Metal Oxide NanomaterialsAcoustic Wave Resonator Technologies

Secondary electron imaging of monolayer materials inside a transmission electron microscope

Ovidiu Cretu、Yung‐Chang Lin、Kazu Suenaga2015-08-10Applied Physics Letters

A scanning transmission electron microscope equipped with a backscattered and secondary electron detector is shown capable to image graphene and hexagonal boron nitride monolayers. Secondary electron contrasts of the two lightest monolayer materials are clearly distinguished from the vacuum level. A signal difference…

Advanced Electron Microscopy Techniques and ApplicationsElectron and X-Ray Spectroscopy TechniquesSurface and Thin Film Phenomena

Effect of p-GaN layer doping on the photoresponse of GaN-based p-i-n ultraviolet photodetectors

Jun Wang、Jin Guo、Feng Xie 等 8 位作者2015-08-10Proceedings of SPIE, the International Society for Optical Engineering/Proceedings of SPIE

We report on two-dimensional (2D) numerical simulations of photoresponse characteristics for GaN based p-i-n ultraviolet (UV) photodetectors. Effects of doping density of p-GaN layer on the photoresponse have been investigated. In order to accurately simulate the device performance, the theoretical calculation include…

GaN-based semiconductor devices and materialsGa2O3 and related materialsPhotocathodes and Microchannel Plates

Mesoscale Characterization of Nanoparticles Distribution Using X‐ray Scattering

Cédric Gommes、Gonzalo Prieto、Jovana Zečević 等 7 位作者2015-08-10Angewandte Chemie

Abstract The properties of many functional materials depend critically on the spatial distribution of an active phase within a support. In the case of solid catalysts, controlling the spatial distribution of metal (oxide) nanoparticles at the mesoscopic scale offers new strategies to tune their performance and enhance…

Mesoporous Materials and CatalysisMagnetic Properties and Synthesis of FerritesIron oxide chemistry and applications

Temporal Tracking of Mineralization and Transcriptional Events Associated with Shell Formation During the Early Life History of Pearl Oyster Pinctada maxima

Luke D. Gardner、Scott F. Cummins、David Mills 等 5 位作者2015-08-10Current Biotechnology

Background: Molluscan larval ontogeny is a highly conserved process comprising three principal developmental stages; trochophore, veliger and metamorphosis into the juvenile. A characteristic that is unique to each of these stages is shell design, termed prodissoconch I, prodissoconch II and dissoconch in bivalves. Th…

Marine Bivalve and Aquaculture StudiesCalcium Carbonate Crystallization and Inhibition

Polyurethanes modified by hydroxyapatite as biomaterials

Piotr Król、Bożena Król、Kinga Pielichowska 等 5 位作者2015-08-10Polimery

Polyurethane composites were obtained in the reaction of HDI or HMDI diisocyanate, polycaprolactone diol and 1,4-butanediol in 1,4-dioxane solution containing dispersed hydroxyapatite. The distribution of hydroxyapatite particles in the polymer matrix has been examined using SEM-EDX method. By applying DSC, TOPEM DSC…

Bone Tissue Engineering Materialsbiodegradable polymer synthesis and propertiesAdditive Manufacturing and 3D Printing Technologies

Observing Nucleation Transition in Stretched Natural Rubber through Self-Seeding

Han Liu、Guangsu Huang、Jian Zeng 等 8 位作者2015-08-10The Journal of Physical Chemistry B

Potential competition between fringed-micelle nucleation (N1) and folded-chain nucleation (N2) widely exists in strain-induced crystallization (SIC). However, during uniaxial deformation, no in situ observational evidence of nucleation transition from N2 to N1 in SIC of natural rubber (NR) has been reported yet. In th…

Polymer crystallization and propertiesPolymer Nanocomposites and Propertiesbiodegradable polymer synthesis and properties

Carbon Nanotube-thermally Reduced Graphene Hybrid/Styrene Butadiene Rubber Nano Composites: Mechanical, Morphological andDielectric Studies

Jiji Abraham、Maya Mg、Soney C. George 等 5 位作者2015-08-10Research and reviews: journal of engineering and technology

Styrene Butadiene Rubber composites with mixture of carbon nanotube and thermally reduced graphene were prepared and morphological, mechanical and dielectric properties of the composites were studied. Aim of this study is to understand the dispersion and reinforcement behaviour of hybrid filler in rubber matrix. Impro…

Carbon Nanotubes in CompositesPolymer Nanocomposites and PropertiesPolymer Nanocomposite Synthesis and Irradiation

Melting behavior of thin polyethylene films

Tisato Kajiyama、Hirohiko Yakabe、Daisuke Kawaguchi 等 5 位作者2015-08-10Journal of Plastic Film & Sheeting

Melting behavior in thin films of linear low-density polyethylene (LLDPE) and high-density polyethylene (HDPE) was studied by local thermal analysis (µTA). Even in the films thinner than 100 nm, the melting temperature ( T m ) was successfully observed by µTA. For LLDPE, T m decreased as the thickness became thinner t…

Polymer crystallization and propertiesMaterial Dynamics and PropertiesPolymer Nanocomposites and Properties

Facile synthesis of functional copolymers with pendant vinyl groups by using asymmetrical divinyl monomers

Hongjun Yang、Tao Bai、Xiaoqiang Xue 等 7 位作者2015-08-10Journal of Applied Polymer Science

ABSTRACT Polymers bearing pendant vinyl groups have attracted significant attraction because they can be further modified for required applications, but their syntheses are still a big challenge. Herein, allyl methacrylate was catalyzed using a phosphazene base to homopolymerize or copolymerize with 2‐(N, N‐dimethylam…

Advanced Polymer Synthesis and CharacterizationSynthetic Organic Chemistry MethodsCovalent Organic Framework Applications

Fermi velocity modulation of spin-dependent transport in graphene

Qing‐Ping Wu、Zhengfang Liu、Ai-Xi Chen 等 4 位作者2015-08-10Journal of Physics D Applied Physics

We study spin-dependent transport in a two-dimensional graphene structure with Rashba spin–orbit interaction and spatially-varying Fermi velocity. The numerical results show that the spin precession and Brewster-like angle induced by the Rashba spin–orbit interaction can be tuned efficiently by the Fermi velocity. Cha…

Graphene research and applicationsQuantum and electron transport phenomenaTopological Materials and Phenomena