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X‐ray spectrometers in Russia: history of their development and present‐day status

I. A. Brytov、A. N. Mezhevich2002-05-01X-Ray Spectrometry

Abstract The background to the development and production of x‐ray instruments in the former USSR and Russia is due to the work of a number of scientists in educational and research institutions. The development of mass‐produced instruments and their practical introduction throughout the country were made possible by…

X-ray Spectroscopy and Fluorescence AnalysisX-ray Diffraction in CrystallographyCrystallography and Radiation Phenomena

Development of alumina primary coat for single crystal investment casting ceramic mould

Chao Yuan、Sam Jones、Paul Withey 等 4 位作者2002-05-01British Ceramic Transactions

The use of an alumina primary coat to eliminate the interaction between aluminium in NiAl single crystal alloy and silica in the ceramic investment casting mould has been examined in this study. The properties of the alumina slurry were characterised and the main factors controlling stability identified. It was found…

Advanced ceramic materials synthesisHigh-Temperature Coating BehaviorsAdditive Manufacturing and 3D Printing Technologies

Foamed Polymer Sandwich Composites Reinforced with Three-Dimensional Filler

Yusheng Yuan、F. Shutov2002-05-01Journal of Reinforced Plastics and Composites

Open-pore flexible polyurethane (PUR) foam with varioius pore sizes (1-8 mm) was used as filler to reinforce low-density closed-cell PUR flexible foam. The final composite has a sandwich structure, where the core zone has “foam-in-foam” structure and skin zones are unreinforced PUR foams. Compared to the regular, non-…

Electrospun Nanofibers in Biomedical ApplicationsPolymer composites and self-healingPolymer Foaming and Composites

Organic Thickeners for Water-Borne Paints

Johan H. Bieleman2002-05-01CHIMIA International Journal for Chemistry

Thickeners are used in paint systems to achieve particular rheological properties such as shear-rate dependent behavior, to control the viscosity at low and high shear rates, sag resistance and application viscosity. This contribution addresses the use and application of thickeners in water-borne paints.Examples of su…

Polymer Nanocomposites and PropertiesPolymer composites and self-healingEpoxy Resin Curing Processes

Defoamers in the Coatings Industry

Albert Frank、Wilfried Scholz2002-05-01CHIMIA International Journal for Chemistry

Foam bubbles can be a very severe problem in all kinds of coating systems. Mechanisms of foam stabilization and mechanisms of defoamers are briefly reviewed. The chemistry of different defoamer classes (mineral oil defoamers, silicone defoamers, silicone-free polymeric defoamers) together with their typical applicatio…

Polymer Foaming and Composites

Controlling calcium precipitation in an integrated anaerobic–aerobic treatment system of a “zero-discharge” paper mill

J.B. van Lier、Marc Árpád Boncz2002-05-01Water Science & Technology

The pulp and paper industry uses significant amounts of water and energy for the paper production process. Closing the water cycles in this industry, therefore, promises large benefits for the environment and has the potential of huge cost savings for the industry. Closing the water cycle on the other hand also introd…

Calcium Carbonate Crystallization and InhibitionCO2 Sequestration and Geologic InteractionsMinerals Flotation and Separation Techniques

Secondary electron emission for layered structures

SeGi Yu、Whikun Yi、Taewon Jeong 等 8 位作者2002-05-01Journal of Vacuum Science & Technology A Vacuum Surfaces and Films

Semiempirical theory for secondary electron emission is extended to cover the layered structure. Secondary electron emission for the two-layered structure, i.e., a thin film on a substrate, is calculated and compared with the experiment. Good agreement between the two indicates the usefulness of this theory for the la…

Semiconductor materials and devicesElectron and X-Ray Spectroscopy TechniquesPhotocathodes and Microchannel Plates

Dopant-dependent reflectivity and refractive index of microcrystalline molybdenum–bronze thin films

Zahid Hussain2002-05-01Journal of Applied Physics

Reflectivity spectra of HxMoO3 and LixMoO3 thin films were measured over the photon energy range from 0.4 to 4.2 eV. It was found that microcrystalline molybdenum bronzes have reflectances between 6% and 30% over the concentration x, range 0⩽x⩽0.64. Values for the real part of the refractive index n were also determin…

Luminescence Properties of Advanced MaterialsPhotorefractive and Nonlinear OpticsTransition Metal Oxide Nanomaterials

Tritium Measurements for 6Li-Enriched Li2TiO3 Breeding Blanket Experiments with D-T Neutrons

A. Klix、Kentaro Ochiai、Yasuaki Terada 等 7 位作者2002-05-01Fusion Science & Technology

The JAERI Fusion Neutronics Source (FNS) group has carried out experiments with breeding blanket mock-ups composed of layers of beryllium, ferritic steel F82H and 6Li enriched lithium titanate ceramics, Li2TiO3. Pellets of enriched Li2TiO3 with a diameter of 12 mm and a thickness of 2 mm were used as detectors inside…

Fusion materials and technologiesNuclear Physics and ApplicationsMuon and positron interactions and applications

“Prometheus” Setup for Study of Tritium Superpermeation

А. А. Yukhimchuk、С. К. Гришечкин、M. E. Notkin 等 9 位作者2002-05-01Fusion Science & Technology

The experimental setup is put in operation designed to study the phenomenon of the superpermeation of hydrogen isotopes, including tritium, through metals and to demonstrate the possibility of membrane pumping. The permeation of atomic hydrogen through the niobium membrane was shown to occur in the superpermeation reg…

Fusion materials and technologiesHydrogen Storage and MaterialsParticle accelerators and beam dynamics

Removal and Control of Tritium in Lithium Target for International Fusion Materials Irradiation Facility (IFMIF)

H. Nakamura、M. Ida、M. Sugimoto 等 5 位作者2002-05-01Fusion Science & Technology

This paper describes removal and control of tritium of liquid lithium (Li) target for IFMIF. To produce intense neutrons, 40 MeV deuteron beam with a current of 250 mA is injected into a liquid Li flow with a speed of 20 m/s. D-Li reaction produces tritium with a production rate of 7 g/y. Tritium in Li is removed by a…

Fusion materials and technologiesParticle accelerators and beam dynamicsMuon and positron interactions and applications

Synthesis of a Star-Shaped Copolymer with a Hyperbranched Poly(3-methyl-3-oxetanemethanol) Core and Tetrahydrofuran Arms by One-Pot Copolymerization

Jian Hou、Deyue Yan2002-05-01Macromolecular Rapid Communications

A star-shaped copolymer consisting of a hyperbranched poly(3-methyl-3-oxetanemethanol) core and polytetrahydrofuran arms was obtained by a one-step cationic copolymerization of 3-methyl-3-oxetanemethanol with tetrahydrofuran initiated by BF3·OEt2. Tetrahydrofuran served as a solvent at the earlier stage of the polymer…

Fuel Cells and Related MaterialsSynthetic Organic Chemistry MethodsDendrimers and Hyperbranched Polymers

Amino acid residues in conodont elements

Anne Kemp2002-05-01Journal of Paleontology

Thermally unaltered conodont elements, brachiopods, and vertebrates were analyzed with reverse phase high profile liquid chromatography to locate and quantify amino acid remnants of the original organic matrix in the fossils. No consistent similarities in amino acid content were found in conodont taxa, and criteria ba…

Hydrocarbon exploration and reservoir analysisEndodontics and Root Canal TreatmentsCalcium Carbonate Crystallization and Inhibition

Simulation of hydrogen outgassing in ultrahigh vacuum chamber and fusion device by recombination limited model

K. Akaishi、M. Nakasuga、Y. Funato2002-05-01Journal of Vacuum Science & Technology A Vacuum Surfaces and Films

To simulate hydrogen outgassing in an ultrahigh vacuum (UHV) chamber and a fusion device, an outgassing theory based on the recombination limited model is presented, where the time evolution of hydrogen concentration in the wall of the vacuum chamber is described by a one-dimensional diffusion equation. The hydrogen o…

Magnetic confinement fusion researchFusion materials and technologiesMuon and positron interactions and applications

Debris reduction for copper and diamond-like carbon thin films produced by magnetically guided pulsed laser deposition

Ying Y. Tsui、H. Minami、D. Vick 等 4 位作者2002-05-01Journal of Vacuum Science & Technology A Vacuum Surfaces and Films

The effectiveness of debris reduction using magnetically guided pulsed laser deposition (MGPLD) is reported here. KrF laser pulses (248 nm) of 100 mJ energy were focused to intensities of 6×109 W/cm2 onto the surface of a copper or a carbon source target and a magnetic field of 0.3 T as used to steer the plasma around…

Metal and Thin Film MechanicsDiamond and Carbon-based Materials ResearchLaser-induced spectroscopy and plasma

Effect of Pressing on the Infrared Spectra of Single Cotton Fibers

Runying Chen、Kathryn A. Jakes2002-05-01Applied Spectroscopy

Fourier transform infrared spectra of single fibers of cotton and 18% NaOH treated cotton were obtained before and after fiber pressing to investigate the effect of pressing on the sample. Pressing resulted in improved spectral quality in some regions (e.g., OH stretching) and deteriorated spectral quality in other re…

Dyeing and Modifying Textile FibersTextile materials and evaluations

Dielectric behaviors under high electric field for Pb(Zr1/3Nb2/3)O3–PbTiO3–BaTiO3 relaxor ferroelectric ceramics

Xiaoli Wang、Haydn Chen2002-05-01Journal of Applied Physics

The dielectric behaviors of Pb(Zn1/3Nb2/3)O3–PbTiO3–BaTiO3 (PZN–PT–BT) relaxor ferroelectric ceramics of several compositions have been investigated under high alternating electric field. In the broad temperature range of the diffuse phase transition, they show highly induced polarization. An unusual linear relation o…

Ferroelectric and Piezoelectric MaterialsDielectric materials and actuatorsMicrowave Dielectric Ceramics Synthesis

Studies on ground EPDM vulcanisate as filler in window seal formulation

Chacko Jacob、Anil K. Bhowmick、P. P. De 等 4 位作者2002-05-01Plastics Rubber and Composites Macromolecular Engineering

The processability, curing characteristics, and mechanical properties of a window seal compound based on highly filled and oil extended EPDM rubber (R-EPDM) containing ground EPDM vulcanisate of known composition (W-EPDM) simulating the waste window seal product have been studied. A conventional mechanical grinder wit…

Asphalt Pavement Performance EvaluationPolymer Nanocomposites and PropertiesTribology and Wear Analysis

A New Strontium Lithium Titanium Oxide, SrLi2Ti6O14: Crystal Growth and Structure Determination

I. Koseva、P. Peshev、Stanislav Péchev 等 5 位作者2002-05-01Zeitschrift für Naturforschung B

A new strontium lithium titanate with composition SrLi 2 Ti 6 O 14 has been discovered in the ternary system SrO - Li 2 O - TiO 2 . Single crystals of this compound have been grown by the flux method. The structure of SrLi 2 Ti 6 O 14 has been solved using X-ray data (Mo-K α radiation, orthorhombic, space group Cmca,…

Ferroelectric and Piezoelectric MaterialsMicrowave Dielectric Ceramics SynthesisNuclear materials and radiation effects

Bis[citrato(3−)-O1,O3,O6]silicate: A Dianionic Complex with Hexacoordinate Silicon(IV) and Two Tridentate Dioato(2−)olato(1−) Ligands

Reinhold Tacke、M. Penka、Friedrich Popp 等 4 位作者2002-05-01European Journal of Inorganic Chemistry

Simple preparative methods for the synthesis of a hexacoordinate silicate dianion with two tridentate citrato(3−) ligands have been developed. Thus, treatment of tetramethoxysilane with two molar equivalents of citric acid and two molar equivalents of tri(n-butyl)amine in tetrahydrofuran yielded tri(n-butyl)ammonium b…

Mesoporous Materials and CatalysisPolyoxometalates: Synthesis and ApplicationsSynthetic Organic Chemistry Methods