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Synthesis of Group IV (Zr, Hf)−Group VIII (Fe, Ru) Heterobimetallic Complexes Bearing Metallocenyl Diphosphine Moieties and Their Application to Catalytic Dehydrogenation of Amine−Boranes

Takamasa Miyazaki、Yoshiaki Tanabe、Masahiro Yuki 等 5 位作者2011-03-30Organometallics

A series of heterobimetallic complexes, including [M 1 Me(μ-η 5:η 1 -C 5 H 4 PEt 2 ) 2 M 2 Cp*] ( 5a, M 1 = Zr, M 2 = Ru; 5b, M 1 = Hf, M 2 = Ru; 5c, M 1 = Zr, M 2 = Fe) have been prepared and characterized by X-ray analyses. Dehydrogenation of Me 2 NH·BH 3 takes place in the presence of a catalytic amount of these he…

Hydrogen Storage and MaterialsAsymmetric Hydrogenation and CatalysisCarbon dioxide utilization in catalysis

Slow Release of NO by Microporous Titanosilicate ETS-4

Moisés L. Pinto、João Rocha、José R. B. Gomes 等 4 位作者2011-03-30Journal of the American Chemical Society

A novel approach to designing nitric oxide (NO) storage and releasing microporous agents based on very stable, zeolite-type silicates possessing framework unsaturated transition-metal centers has been proposed. This idea has been illustrated with ETS-4 [Na(9)Si(12)Ti(5)O(38)(OH)·xH(2)O], a titanosilicate that displays…

Catalytic Processes in Materials ScienceCatalysis and Oxidation ReactionsIndustrial Gas Emission Control

Fabrication and Intermolecular Interactions of Silk Fibroin/Hydroxybutyl Chitosan Blended Nanofibers

Kuihua Zhang、Qiaozhen Yu、Xiumei Mo2011-03-30International Journal of Molecular Sciences

The native extracellular matrix (ECM) is composed of a cross-linked porous network of multifibril collagens and glycosaminoglycans. Nanofibrous scaffolds of silk fibroin (SF) and hydroxybutyl chitosan (HBC) blends were fabricated using 1,1,1,3,3,3-hexafluoro-2-propanol (HFIP) and trifluoroacetic acid (TFA) as solvents…

Bone Tissue Engineering MaterialsElectrospun Nanofibers in Biomedical ApplicationsSilk-based biomaterials and applications

A Stable Molecular Entity Derived from Rare Iron(II) Minerals: The Square‐Planar High‐Spin‐d6 FeIIO4 Chromophore

X. Wurzenberger、H. Piotrowski、Peter Klüfers2011-03-30Angewandte Chemie International Edition

The odd couple: The red chromophore of both the rare silicate mineral gillespite (BaFeSi4O10; see picture, left, on sanbornite, BaSi2O5) and the bis(meso-oxolanediolato)ferrate(II) anion in its lithium salt (right) is the square-planar, high-spin-d6 ferrous center. The unusual combination of structure and spin state f…

Magnetism in coordination complexesCrystal Structures and PropertiesChemical Synthesis and Characterization

Photoluminescent Lanthanide-Doped Silica Nanotubes: Sol−Gel Transcription from Functional Template

Yan Qiao、Huanfa Chen、Yiyang Lin 等 6 位作者2011-03-30The Journal of Physical Chemistry C

Functional photoluminescent materials have emerged as a fascinating research subject holding great promise in versatile applications. In this report, photoluminescent lanthanide-organic hybrid nanofibers in hydrogels are fabricated through supramolecular self-assembly, which can serve as functional soft templates to p…

Mesoporous Materials and CatalysisPolyoxometalates: Synthesis and ApplicationsDiatoms and Algae Research

AnisotropicHc2ofK0.8Fe1.76Se2determined up to 60 T

E. D. Mun、M. M. Altarawneh、C. H. Mielke 等 7 位作者2011-03-30Physical Review B

The anisotropic upper critical field, ${H}_{c2}(T)$, curves for ${\mathrm{K}}_{0.8}$Fe${}_{1.76}$Se${}_{2}$ are determined over a wide range of temperatures down to 1.5 K and magnetic fields up to 60 T. Anisotropic initial slopes of ${H}_{c2}$ $~$ $\ensuremath{-}1.4$ T/K and $\ensuremath{-}4.6$ T/K for magnetic field…

Physics of Superconductivity and MagnetismRare-earth and actinide compoundsIron-based superconductors research

Solvothermal Assembly of a Series of Organic–Inorganic Hybrid Materials Constructed from Keggin Polyoxometalate Clusters and Copper(I)–Organic Frameworks

Haiyan Liu、Hua Wu、Jin Yang 等 6 位作者2011-03-30Crystal Growth & Design

Seven polyoxometalate (POM) hybrid materials based on Keggin polyanion building blocks and copper(I)–organic frameworks with pyrazine derivatives, namely, [Cu I 4 (2Et,3Me-Pyr) 5 (SiW 12 O 40 )] ( 1 ), [Cu I 4 (2,6-Pyr) 4 (SiW 12 O 40 )] ( 2 ), [Cu I 4 (2,5-Pyr) 4 (SiW 12 O 40 )(H 2 O) 2 ] ( 3 ), [Cu I 4 (2,3,5,6-Pyr)…

Metal-Organic Frameworks: Synthesis and ApplicationsPolyoxometalates: Synthesis and ApplicationsAdvanced Nanomaterials in Catalysis

Density profiles of a colloidal liquid at a wall under shear flow

J. M. Brader、Matthias Krüger2011-03-30Molecular Physics

Using a dynamical density functional theory we analyse the density profile of a colloidal liquid near a wall under shear flow. Due to the symmetries of the system considered, the naive application of dynamical density functional theory does not lead to a shear induced modification of the equilibrium density profile, w…

Phase Equilibria and ThermodynamicsMaterial Dynamics and PropertiesRheology and Fluid Dynamics Studies

Defect energetics in SrTiO3symmetric tilt grain boundaries

H.-S. Lee、Teruyasu Mizoguchi、J. Mistui 等 6 位作者2011-03-30Physical Review B

Atomic structures and the defect energetics of three symmetric tilt boundaries of SrTiO${}_{3}$, [$1\overline{1}0$](111)\ensuremath{\Sigma}3, [001](210)\ensuremath{\Sigma}5, and [001](510)\ensuremath{\Sigma}13, were systematically investigated by a first-principles projector augmented wave method and high angular annu…

ZnO doping and propertiesSemiconductor materials and devicesElectronic and Structural Properties of Oxides

Synthesis of Redox‐Active, Intramolecular Charge‐Transfer Chromophores by the [2+2] Cycloaddition of Ethynylated 2H‐Cyclohepta[b]furan‐2‐ones with Tetracyanoethylene

Taku Shoji、Junya Higashi、Shunji Ito 等 6 位作者2011-03-30Chemistry - A European Journal

Ethynylated 2H-cyclohepta[b]furan-2-ones 5-15 have been prepared by Pd-catalyzed alkynylation of 3-iodo-5-isopropyl-2H-cyclohepta[b]furan-2-one (2) with the corresponding ethynylarenes or the reaction of 2-iodothiophene with 3-ethynyl-5-isopropyl-2H-cyclohepta[b]furan-2-one (4) under Sonogashira-Hagihara conditions. C…

Radical Photochemical ReactionsSynthesis and Properties of Aromatic CompoundsPhotochromic and Fluorescence Chemistry

Phalloidin-Functionalized Hyperbranched Conjugated Polyelectrolyte for Filamentous Actin Imaging in Living Hela Cells

Kai Li、Kanyi Pu、Liping Cai 等 4 位作者2011-03-30Chemistry of Materials

A phalloidin-functionalized hyperbranched conjugated polyelectrolyte (HCPE-phalloidin) is synthesized and used for direct filamentous actin (F-actin) imaging in living Hela cells. Different from commercially available organic dye-phalloidin conjugates, which require sophisticated techniques to be delivered into living…

Advanced biosensing and bioanalysis techniquesLuminescence and Fluorescent MaterialsDendrimers and Hyperbranched Polymers

Understanding the Multiple Length Scales Describing the Structure of Bottle‐brush Polymers by Monte Carlo Simulation Methods

Hsiao‐Ping Hsu、Wolfgang Paul、Kurt Binder2011-03-30Macromolecular Theory and Simulations

Abstract Bottle‐brush polymers contain a long flexible macromolecule as a backbone to which flexible side chains are grafted. Through the choice of the grafting density and the length of the side chains the local stiffness of this cylindrical molecular brush can be controlled, but a quantitative understanding of these…

Advanced Polymer Synthesis and CharacterizationPolymer Surface Interaction StudiesForce Microscopy Techniques and Applications

Layer-by-Layer Assembled Solid Polymer Electrolyte for Electrochromic Devices

Anh Chien Nguyen、Avni A. Argun、Paula T. Hammond 等 5 位作者2011-03-30Chemistry of Materials

A new solid polymer electrolyte film fabricated by layer-by-layer (LbL) assembly is presented. The electrolyte film consists of four interbonding layers per deposition cycle, which combines electrostatic and hydrogen bonding in the same structure. Linear poly(ethylene imine) (LPEI) and poly(ethylene oxide) (PEO) are u…

Ferroelectric and Piezoelectric MaterialsAdvanced Battery Materials and TechnologiesConducting polymers and applications

Nanofibrous scaffold prepared by electrospinning of poly(vinyl alcohol)/gelatin aqueous solutions

Chao Yang、Xiaomian Wu、Yinghui Zhao 等 5 位作者2011-03-30Journal of Applied Polymer Science

Abstract A series of nanofibrous scaffolds were prepared by electrospinning of poly(vinyl alcohol) (PVA)/gelatin aqueous solution. PVA and gelatin was dissolved in pure water and blended in full range, then being electrospun to prepared nanofibers, followed by being crosslinked with glutaraldehyde vapor and heat treat…

Advanced Sensor and Energy Harvesting MaterialsElectrospun Nanofibers in Biomedical ApplicationsSilk-based biomaterials and applications

Glancing angle deposited ITO films for efficiency enhancement of a-Si:H/μc-Si:H tandem thin film solar cells

Jung Woo Leem、Jae Su Yu2011-03-30Optics Express

Indium tin oxide (ITO) thin films with relatively high transparency and low absorption are prepared by glancing angle deposition (GLAD) method and their effect on the device performance of a-Si:H/μc-Si:H tandem thin film solar cells is theoretically investigated by applying the experimentally measured physical data of…

Thin-Film Transistor TechnologiesPhotonic Crystals and ApplicationsOptical Coatings and Gratings

Local structure of Ba(Ti,Zr)O3perovskite-like solid solutions and its relation to the band-gap behavior

Igor Levin、Eric Cockayne、V. Krayzman 等 6 位作者2011-03-30Physical Review B

Local structures in BaTi${}_{1\ensuremath{-}x}$Zr${}_{x}$O${}_{3}$ solid solutions were analyzed using x-ray absorption fine structure (XAFS) measurements and density-functional theory (DFT) calculations. We demonstrate that for low concentrations of Ti, isolated Ti atoms in the relatively large octahedral sites of th…

Ferroelectric and Piezoelectric MaterialsMicrowave Dielectric Ceramics SynthesisThermal Expansion and Ionic Conductivity

Surface-Initiated Nitroxide-Mediated Polymerization from Ordered Mesoporous Silica

Hélène Blas、Maud Save、Cédric Boissière 等 5 位作者2011-03-30Macromolecules

This work describes, for the first time, the nitroxide-mediated polymerization (NMP) of styrene initiated from an SG1-based alkoxyamine grafted on both the inner and outer surfaces of ordered mesoporous silica (OMS) particles. The OMS particles with various morphologies were synthesized by sol−gel chemistry in the pre…

Advanced Polymer Synthesis and CharacterizationMesoporous Materials and CatalysisPolymer Surface Interaction Studies

Influence of the contact angle of silica nanoparticles at the air–water interface on the mechanical properties of the layers composed of these particles

Duyang Zang、Emmanuelle Rio、Giles Delon 等 6 位作者2011-03-30Molecular Physics

We have studied the properties (surface pressure, compression and shear moduli, texture) of silica nanoparticle layers at the air–water interface. Particle hydrophobicity or, equivalently, the contact angle between particles, air and water, is the main factor that influences surface organization and surface elastic mo…

Proteins in Food SystemsSurfactants and Colloidal SystemsPickering emulsions and particle stabilization

Anharmonic phonon effects in Raman spectra of unsupported vertical graphene sheets

Jingjing Lin、Liwei Guo、Qingsong Huang 等 7 位作者2011-03-30Physical Review B

Temperature-dependent Raman scattering is performed on unsupported vertical graphene sheets, which are approximate to free graphene without supporting the substrate. Here the observed G peak line shift with temperature is completely consistent with the theoretical prediction based on the first-principles calculation o…

Graphene research and applicationsThermal properties of materialsThermal Radiation and Cooling Technologies

ANALYTICAL SOLUTIONS FOR VIBRATION OF SIMPLY SUPPORTED NONLOCAL NANOBEAMS WITH AN AXIAL FORCE

Chuandong Li、C.W. Lim、Jilin Yu 等 4 位作者2011-03-30International Journal of Structural Stability and Dynamics

This paper presents exact, analytical solutions for the transverse vibration of simply supported nanobeams subjected to an initial axial force based on nonlocal elasticity theory. Classical continuum theory is inherently size independent while nonlocal elasticity exhibits size dependence. The latter has significant ef…

Composite Structure Analysis and OptimizationNumerical methods in engineeringNonlocal and gradient elasticity in micro/nano structures