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Polytetrafluoroethylene by XPS

Michael Ackeret1992-03-01Surface Science Spectra

X-ray photoelectron spectroscopy was used to analyze a 1 cm2, 0.13 mm thick coupon of polytetrafluoroethylene (PTFE). The material was examined as received from the manufacturer following a cleaning with isopropyl alcohol and trichlorotrifluoroethane. The PTFE coupon was examined with a Hewlett-Packard 5950B ESCA syst…

X-ray Spectroscopy and Fluorescence AnalysisNuclear Physics and ApplicationsElectron and X-Ray Spectroscopy Techniques

Crystal and molecular structures of 1,4-dibromo- and 1,4-diiodocubane

N. Kawai、D. F. R. Gilson、James F. Britten 等 5 位作者1992-03-01Canadian Journal of Chemistry

The crystal structure of 1,4-dibromocubane has been determined by X-ray diffraction. The crystal is monoclinic, P2 1 /n, a = 6.878(1), b = 6.960(7), c = 8.793(2) Å, β = 113.08(2)°, Z = 2, R = 0.055. The C—Br bond length, at 1.926 Å, is shorter than usual and the carbon framework is probably distorted by longer bonds a…

Magnetism in coordination complexesLanthanide and Transition Metal Complexes

Degumming of silk with oxalic acid

M L Gulrajani、Arnab Chatterjee1992-03-01OpenAlex

t Introduction Silk consists mainly of fibroin and sericin along with very small amounts of waxy substances, mineral salts and colouring matter. The sericin is also referred to as silk gum and its removal is, therefore, called degumming. The sericin is removed by hydrolytically breaking it into smaller water-soluble f…

Silk-based biomaterials and applicationsSilkworms and Sericulture Research

Preventative maintenance of turbine-generator stator windings

R.E. Fenton、Beth Gott、Clyde V. Maughan1992-03-01IEEE Transactions on Energy Conversion

The authors discuss stator winding deterioration mechanisms and their consequences. Inspection and test procedures which will detect these mechanisms, as well as programs to arrest them, are also discussed. The analysis is broken down into sections on the slot region of the stator winding and on the end winding region…

High voltage insulation and dielectric phenomenaPower Transformer Diagnostics and InsulationNon-Destructive Testing Techniques

Minor loops in magnetization-dependent Preisach models

Ferenc Vajda、E. Della Torre1992-03-01IEEE Transactions on Magnetics

It is noted that the moving model and the product model have different variations in the height of minor loops and thus a means of differentiating between the models. Measurements show that, for particulate magnetic recording media, the moving model yields more realistic results and that previous reversible magnetizat…

Physics of Superconductivity and MagnetismMagnetic properties of thin filmsMagnetic Properties and Applications

Gap‐Fill with PECVD SiO2 Using Deposition/Sputter Etch Cycles

G. C. Schwartz、Pauline Johns1992-03-01Journal of The Electrochemical Society

We have studied a process for filling narrow spaces between adjacent metallic conductors (gaps). The process consists of cycles of deposition of by plasma‐enhanced chemical vapor deposition (PECVD) and sputter etching in Ar. For a fixed process and metal thickness, as the gaps decrease in size, i.e. , as the aspect ra…

Metal and Thin Film MechanicsThin-Film Transistor TechnologiesCopper Interconnects and Reliability

Experimental Evaluation of the Consequences of Uranium Bed Air-Ingress Accidents

G.R. Longhurst、A.G. Heics、W.T. Shmayda 等 4 位作者1992-03-01Fusion Technology

To help resolve unknowns regarding consequences of air-ingress accidents in uranium beds, a series of experiments was conducted at Ontario Hydro Research Division with the participation of Princeton Plasma Physics Laboratory and the Idaho National Engineering Laboratory. These experiments involved exposure of uranium…

Nuclear reactor physics and engineeringRadioactive element chemistry and processingNuclear Materials and Properties

Thermodynamic Calculations on the Chemical Vapor Deposition of Silicon Nitride and Silicon from Silane and Chlorinated Silanes

Frank Einar Kruis、B. Florence Scarlett、Robert Bauer 等 4 位作者1992-03-01Journal of the American Ceramic Society

After a discussion of the thermochemical values of the Si–H–Cl–N system which occur in the literature, CVD phase diagrams are presented which include contours of constant deposition efficiency. The temperature range considered is from 800 to 2600 K. A number of chlorinated silanes as well as silane can be used as a si…

Advanced ceramic materials synthesisMetal and Thin Film MechanicsSemiconductor materials and devices

Linear and non-linear transient patterns in the splay Freedericksz transition of nematics

Agnes Buka Lorenz Kramer1992-03-01Journal de Physique II

A three-dimensional linear analysis of transient patterns occuring during the splay Freedericksz transition is presented including contributions relevant for the electrically driven case. The most rapidly growing modes have a wave vector predominantly along the initial directore alignment. The onset of the pattern for…

Liquid Crystal Research AdvancementsNonlinear Dynamics and Pattern FormationQuantum optics and atomic interactions

Quecksilberverbindungen mit Cyancarbanionen. I. Synthese und Kristallstruktur von Diquecksilber(I)‐bis(tricyanmethanid)

K. Brodersen、Jürgen Hofmann1992-03-01Zeitschrift für anorganische und allgemeine Chemie

Abstract Innerhalb der triklinen Elementarzelle, Raumgruppe P 1 , mit den Gitterkonstanten a = 5,2794(1) Å, b = 9,9279(1) Å, c = 11,3376(2) Å, α = 71,004(4)° und β = 74,601(4)° befinden sich zwei Formeleinheiten. Das den Strukturaufbau charakterisierende dreidimensionale Netzwerk resultiert aus sp 3 ‐hybridisierten Di…

Molecular Sensors and Ion DetectionMagnetism in coordination complexesLanthanide and Transition Metal Complexes

Tritium Aging of Zirconium Cobalt

A.G. Heics、W.T. Shmayda1992-03-01Fusion Technology

Zirconium cobalt (ZrCo) is being evaluated as an alternative to uranium for tritium storage. The pumping speed and pressure-composition-temperature isotherm profiles for the ZrCo hydrogen and tritium systems were measured to determine isotopic differences and the effect of He-3 induced aging on ZrCo performance. Hydro…

Fusion materials and technologiesHydrogen Storage and MaterialsAmmonia Synthesis and Nitrogen Reduction

The modelling of segmented laminations in three dimensional eddy current calculations

B.C. Mecrow、A.G. Jack1992-03-01IEEE Transactions on Magnetics

A formulation is presented for the inclusion of segmentation effects in a three-dimensional eddy current model of large laminated iron cores. The model has been developed for the study of eddy currents induced in the end laminations of turbogenerator stator cores. It includes magnetic nonlinearity and represents the o…

Electric Motor Design and AnalysisMagnetic Properties and ApplicationsNon-Destructive Testing Techniques

Encyclopedia of Textiles

Judith Jerde1992-03-01Medical Entomology and Zoology

Spanning nearly 5000 years of textile history, this book covers the field from the first practical and decorative use of fabrics to the introduction of modern synthetic materials. Organized in an A to Z format, the work provides information on fabric, fabrication methods, machine processes (felting, weaving) and more.…

Textile materials and evaluations

Molecular Orientation in Injection-molded Polypropylene Copolymers with Ethylene

Mitsuyoshi Fujiyama、Tetsuo Wakino1992-03-01International Polymer Processing

Abstract Flexural test specimens were injection-molded from random and block polypropylene copolymers with various ethylene contents at cylinder temperatures of 200 to 320°C. Properties such as flexural modulus (FM), flexural strength (FS), heat distortion temperature (HDT), Izod impact strength (IIS), and mold shrink…

Polymer crystallization and propertiesInjection Molding Process and PropertiesPolymer Foaming and Composites

Temperature dependence of the interfacial dielectric loss process in glass bead‐filled polyethylene

P. A. M. Steeman、J. F. H. Baetsen、Frans H.J. Maurer1992-03-01Polymer Engineering and Science

Abstract The temperature dependence of the interfacial dielectric loss process in glass bead‐filled high density polyethylene (HDPE) due to an interfacially adsorbed water layer has been studied. The frequency of maximum dielectric loss shifts to lower frequencies with decreasing temperature. This is thought to be due…

High voltage insulation and dielectric phenomenaDielectric materials and actuators

Novel inhibitors of prolyl 4-hydroxylase. 2. 5-Amide substituted pyridine-2-carboxylic acids

Howard Tucker、Dudley F. Thomas1992-03-01Journal of Medicinal Chemistry

A series of 5-[(arylcarbonyl)amino]- and 5-(arylcarbamoyl)pyridine-2-carboxylic acids has been prepared and tested for activity as inhibitors of the enzyme prolyl 4-hydroxylase (EC 1.14.11.2). All the analogues prepared were inhibitors of the enzyme in vitro, the best compounds being equipotent with the known inhibito…

Metabolism and Genetic DisordersEnzyme Structure and FunctionBiochemical and Molecular Research

X-Ray Diffraction Analysis of Titanium Carbonitride 30/70 and 70/30 Solid Solutions

J.M. Guilemany、I. Sanchiz、Xavier Alcobé1992-03-01Powder Diffraction

Abstract X-ray powder data and refined cell parameters for two titanium carbonitride solid solutions are presented. Some deviations from Vegard's law were observed.

Advanced materials and compositesX-ray Diffraction in CrystallographyPowder Metallurgy Techniques and Materials

Tritium Permeation and Related Studies on Barrier Treated 316 Stainless Steel

E.R. Gilbert、R.P. Allen、David L. Baldwin 等 11 位作者1992-03-01Fusion Technology

To verify the performance of permeation-resistant cladding for tritium targets designed for a New Production Reactor Light-Water Reactor, a tritium test facility was designed, developed, fabricated, and certified. Testing is ongoing to verify the performance of reference-designed targets. Accurate measurements were ta…

Fusion materials and technologiesNuclear reactor physics and engineeringNuclear Materials and Properties

The Corrosion Behavior of Polycrystalline and Single Crystal Chromium: A Revised Model

J.A.L. Dobbelaar、J.H.W. de Wit1992-03-01Journal of The Electrochemical Society

A revised model for the corrosion behavior of pure chromium has been developed. This model applies to both polycrystals and single crystals. The model has been developed using results from polarization and impedance measurements. In the revised model, the observed diffusion controlled process has been ascribed to surf…

Corrosion Behavior and InhibitionAluminum Alloy Microstructure PropertiesHydrogen embrittlement and corrosion behaviors in metals

Nonlinear Analysis Techniques for Shear Band Formation at High Strain-Rates

Athanasios E. Tzavaras1992-03-01Applied Mechanics Reviews

One of the most striking manifestations of instability in solid mechanics is the localization of shear strain into narrow bands during high speed, plastic deformations of metals. According to one theory, the formation of shear bands is attributed to effective strain-softening response, which results at high strain rat…

Laser-Plasma Interactions and DiagnosticsEnergetic Materials and CombustionHigh-Velocity Impact and Material Behavior