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Electrochemical Investigation of Photooxidation Processes Promoted by Sulfo-polyoxometalates: Coupling of Photochemical and Electrochemical Processes into an Effective Catalytic Cycle

Thomas Rüther、Victoria M. Hultgren、Brian P. Timko 等 6 位作者2003-07-24Journal of the American Chemical Society

Oxidative photocurrents measured upon irradiation by a 7-W visible light (wavelength 312-700 nm) demonstrated that the sulfo-polyoxometalate anion clusters [S2W18O62]4- (1a), [S2Mo18O62]4- (1b), and [SMo12O40]2- (2) may be activated photochemically to oxidize the organic substrates benzyl alcohol, ethanol, and (-)-men…

Polyoxometalates: Synthesis and ApplicationsChemical Synthesis and ReactionsAdvanced Nanomaterials in Catalysis

Highly Efficient Peptide Bond Formation to Functionalized Wells‐Dawson‐Type Polyoxotungstates

Sébastian Bareyt、Stergios Piligkos、Bernold Hasenknopf 等 7 位作者2003-07-24Angewandte Chemie International Edition

Making derivatives of organic side chains on polyoxometalates is an important prerequisite for their application in biology. Compounds α1- and α2-[P2W17O61{Sn(CH2)2CO2H}]7− (depicted) were prepared for the first time and coupled with alcohols and amines, including C-protected amino acids.

Metal-Organic Frameworks: Synthesis and ApplicationsPolyoxometalates: Synthesis and ApplicationsVanadium and Halogenation Chemistry

Highly stable polarization gratings in photocrosslinkable polymer liquid crystals

Hiroshi Ono、Akira Emoto、Fumihiro Takahashi 等 5 位作者2003-07-24Journal of Applied Physics

Highly stable polarization gratings have been prepared in photocrosslinkable polymer liquid-crystal films by the use of two orthogonally polarized He–Cd laser beams and subsequent annealing. The resulting pure polarization gratings exhibiting thermal stability up to 150 °C diffract the beam and convert the polarizatio…

Liquid Crystal Research AdvancementsAdvanced Fiber Laser TechnologiesPhotorefractive and Nonlinear Optics

Below bulk-band-gap photoluminescence at room temperature from heavily P- and B-doped Si nanocrystals

Minoru Fujii、Kimiaki Toshikiyo、Yuji Takase 等 5 位作者2003-07-24Journal of Applied Physics

Photoluminescence (PL) properties of heavily P- and B-doped Si nanocrystals (nc-Si) are studied. By simultaneously doping two types of impurities, nc-Si exhibit strong PL at around 0.9 eV at room temperature. The temperature quenching of the PL is very small. Although the PL peak energy is very close to that of dangli…

Semiconductor materials and devicesSilicon Nanostructures and PhotoluminescenceSemiconductor materials and interfaces

Surface Structures of SrTiO 3 (001): A TiO 2 -rich Reconstruction with a c(4 × 2) Unit Cell

Natasha Erdman、Oliver Warschkow、Mark Asta 等 6 位作者2003-07-24Journal of the American Chemical Society

We report the solution of the c(4 x 2) reconstruction of SrTiO(3) (001), obtained through a combination of high-resolution transmission electron microscopy, direct methods analysis, and density functional theory. The structure is characterized by a single overlayer of TiO(2) stoichiometry in which TiO(5) polyhedra are…

Ferroelectric and Piezoelectric MaterialsMagnetic and transport properties of perovskites and related materialsElectronic and Structural Properties of Oxides

First-Principles Calculations of PuO 2 ± x

L. Petit、A. Svane、Z. Szotek 等 4 位作者2003-07-24Science

The electronic structure of PuO(2+/-x) was studied using first-principles quantum mechanics, realized with the self-interaction corrected local spin density method. In the stoichiometric PuO2 compound, Pu occurs in the Pu(IV) oxidation state, corresponding to a localized f4 shell. If oxygen is introduced onto the octa…

Radioactive element chemistry and processingNuclear Materials and PropertiesNuclear materials and radiation effects

Template Effect of Crystalline Poly(vinyl alcohol) for Selective Formation of Aragonite and Vaterite CaCO3 Thin Films

Naoya Hosoda、Ayae Sugawara‐Narutaki、Takashi Kato2003-07-24Macromolecules

Aragonite thin films of calcium carbonate are selectively formed on crystalline poly(vinyl alcohol) matrices in the presence of poly(acrylic acid) in CaCO 3 solution. For thin film formation, this is the first example in which aragonite is formed selectively by cooperation of only synthetic organic macromolecules. In…

biodegradable polymer synthesis and propertiesPolymer composites and self-healingCalcium Carbonate Crystallization and Inhibition

PVK-Modified Single-Walled Carbon Nanotubes with Effective Photoinduced Electron Transfer

Wei Wu、Shuang Zhang、Yong Li 等 10 位作者2003-07-24Macromolecules

SWNTs are among the most attractive one-dimen-sional materials in the scientific world. Recently, con-siderable work has been done to modify SWNTs in order to bring these fascinating carbon structures into the fold of (macro)molecular chemistry and to endow SWNTs with ultimate new characteristics.1 The polymer wrap-pi…

Organic Electronics and PhotovoltaicsCarbon Nanotubes in CompositesConducting polymers and applications

Room-temperature ultraviolet-emitting In2O3 nanowires

Huaqiang Cao、Xianqing Qiu、Liang Yu 等 5 位作者2003-07-24Applied Physics Letters

Semiconductor In2O3 nanowires embedded in an alumina template were fabricated using template technology. Scanning electron microscopy and transmission electron microscopy observations show that the In2O3 nanowire single crystal has an average diameter around 80 nm and a length over 10 μm. A strong photoluminescence (P…

ZnO doping and propertiesGas Sensing Nanomaterials and SensorsNanowire Synthesis and Applications

Medium permittivity bismuth zinc niobate thin film capacitors

R. Thayer、Clive A. Randall、Susan Trolier‐McKinstry2003-07-24Journal of Applied Physics

Thin films were fabricated via metalorganic decomposition methods with three compositions: Bi1.5Zn1.0Nb1.5O7, Bi1.5Zn0.5Nb1.5O6.5, and Bi2Zn2/3Nb4/3O7. The Bi1.5Zn0.5Nb1.5O6.5 composition is a low temperature phase with the cubic pyrochlore structure. This phase may undergo a peritectoid decomposition at 700 °C to the…

Ferroelectric and Piezoelectric MaterialsMicrowave Dielectric Ceramics SynthesisNuclear materials and radiation effects

Characterization of Shrimp Shell Deproteinization

Aline Percot、Christophe Viton、Alain Domard2003-07-24Biomacromolecules

The aim of this paper was to contribute to the interpretation of the mechanism of shrimp shell deproteinization. We used amino acid analysis to quantify the amount of proteins remaining in chitin. NaOH 1 M was added to a demineralized shrimp shell powder with a solution-to-solid ratio of 15 mL/g at ambient temperature…

Nanocomposite Films for Food PackagingProtein Hydrolysis and Bioactive PeptidesSilk-based biomaterials and applications

Theory of Luminescent Emission in Nanocrystal ZnS:Mn with an Extra Electron

Nguyen Que Huong、Joseph L. Birman2003-07-24arXiv

We consider the effect of an extra electron injected into a doped quantum dot $ZnS:Mn^{2+}$. The Coulomb interaction and the exchange interaction between the extra electron and the states of the Mn ion will mix the wavefunctions, split the impurity energy levels, break the previous selection rules and change the trans…

Mesoscale and Nanoscale PhysicsMaterials Science

Response of aluminum nitride (including a phase change) to large strains, high strain rates, and high pressures

Gordon R. Johnson、Timothy J. Holmquist、Stephen R. Beissel2003-07-24Journal of Applied Physics

This article contains a description of a computational constitutive model for brittle materials subjected to large strains, high strain rates, and high pressures. The focus of this model is to determine the response of aluminum nitride under high velocity impact conditions that produce large strains, high strain rates…

High-pressure geophysics and materialsEnergetic Materials and CombustionHigh-Velocity Impact and Material Behavior

First-principles thermodynamics of transition metals and alloys: W, NiAl, PdTi

Graeme J. Ackland、Xiangyang Huang、Karin M. Rabe2003-07-24arXiv

We apply the pseudopotential density functional perturbation theory approach along with the quasiharmonic approximation to calculate the thermal expansion of tungsten and two important metallic alloys, NiAl and PdTi. We derive the theory for anisotropic crystal structures and test the approximation that the anisotropi…

Materials Sciencecond-mat.stat-mech

High-order density-matrix perturbation theory

Michele Lazzeri、Francesco Mauri2003-07-24arXiv

We present a simple formalism for the calculation of the derivatives of the electronic density matrix at any order, within density functional theory. Our approach, contrary to previous ones, is not based on the perturbative expansion of the Kohn-Sham wavefunctions. It has the following advantages: (i) it allows a simp…

Materials Science

Atomically precise placement of single dopants in Si

S. R. Schofield、N. J. Curson、M. Y. Simmons 等 7 位作者2003-07-24arXiv

We demonstrate the controlled incorporation of P dopant atoms in Si (001) presenting a new path toward the creation of atomic-scale electronic devices. We present a detailed study of the interaction of PH3 with Si (001) and show that it is possible to thermally incorporate P atoms into Si (001) below the H desorption…

Materials Science

Photoinduced three-dimensional orientational order in side chain liquid crystalline azopolymers

O. Yaroshchuk、Alexei D. Kiselev、Yu. Zakrevskyy 等 7 位作者2003-07-24Physical review. E, Statistical physics, plasmas, fluids, and related interdisciplinary topics

We apply experimental technique based on the combination of methods dealing with principal refractive indices and absorption coefficients to study the photoinduced three-dimensional (3D) orientational order in the films of liquid crystalline (LC) azopolymers. The technique is used to identify 3D orientational configur…

Liquid Crystal Research AdvancementsNonlinear Optical Materials ResearchOptical Polarization and Ellipsometry

Temperature dependence of field emission from cupric oxide nanobelt films

Jun Chen、Shaozhi Deng、Ning Xu 等 6 位作者2003-07-24Applied Physics Letters

Films of aligned cupric oxide nanobelts have been prepared in an aqueous solution at room temperature. Field-emission characteristics, including emission-current–applied-field plot and emission site distribution, have been studied using the transparent anode technique. In addition, the temperature dependence of the fi…

ZnO doping and propertiesNanowire Synthesis and ApplicationsCopper-based nanomaterials and applications

CHEMISTRY: Colloidal Molecules and Beyond

Alfons van Blaaderen2003-07-24Science

About a hundred years ago, Jean Perrin's experiments on colloids—particles a few nanometers to a few micrometers in diameter—convinced even the skeptics that matter consists of atoms and molecules. More recently, the analogy between atoms and colloids has led to insights into crystal nucleation and growth, the glass t…

Proteins in Food SystemsSurfactants and Colloidal SystemsPickering emulsions and particle stabilization

Negative magnetocaloric effect at the antiferromagnetic to ferromagnetic transition of Mn3GaC

Tetsuya Tohei、H. Wada、T. Kanomata2003-07-24Journal of Applied Physics

The magnetocaloric effect of Mn3GaC, which shows an antiferromagnetic to ferromagnetic transition at 165 K has been investigated. In this compound, magnetocaloric effect obtained at the transition is opposite to that of ordinary ferromagnetic systems, namely, negative magnetocaloric effect. It was found that a large m…

Magnetic and transport properties of perovskites and related materialsMXene and MAX Phase MaterialsThermal Expansion and Ionic Conductivity