Materials Literature
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Abstract A new triphenylamine‐containing aromatic diamine, N , N ′‐bis(4‐aminophenyl)‐ N , N ′‐diphenyl‐1,4‐phenylenediamine, was prepared by the condensation of N , N ′‐diphenyl‐1,4‐phenylenediamine with 4‐fluoronitrobenzene, followed by catalytic reduction. A series of novel aromatic polyamides with triphenylamine u…
The synthesis of a series of polymeric Eu(III) complexes with polyester ligands, along with supporting emission spectra, luminescence lifetimes, and, for a Eu block copolymer film, atomic force microscopy (AFM) data, is presented. Dibenzoylmethane was derivatized with a hydroxyl initiator site (dbmOH, 1) for tin octoa…
This paper reports a computational method, the quantized elastic deformational model, that can reliably describe the conformational flexibility of a protein in the absence of the amino acid sequence and atomic coordinates. The essence of this method lies in the fact that, in modeling the functionally important conform…
Superconducting MgB2 thin films were prepared on 50-micrometer-thick, flexible polyamide Kapton-E foils by vacuum co-deposition of Mg and B precursors with nominal thickness of about 100 nm and a special ex-situ rapid annealing process in an Ar or vacuum atmosphere. In the optimal annealing process, the Mg-B films wer…
The superconductivities of samples prepared by several procedures were found to degrade under ambient environment. The degradation mechanism was studied by measuring the change of surface chemical composition of dense MgB2 pellets (prepared by hot isostatic pressure, HIPed) under atmospheric exposure using X-ray Photo…
Polarization hysteresis loops, x-ray diffraction (XRD) and temperature dependent dielectric constant under different electric fields for <110> oriented 0.7 Pb(Mg1/3Nb2/3)O3-0.3PbTiO3 single crystals were measured. The field-induced phase transition and the process of depolarization were discussed. The results show tha…
Coarsening in foams made from the pure liquid crystal, 8CB, has been studied. The foam was made in the nematic phase ($\textrm{T} = 35 ^{\circ}\textrm{C}$) by bubbling nitrogen through the pure liquid crystal. The coarsening behavior was investigated at three temperatures; at $\textrm{T} = 22 ^{\circ}\textrm{C}$ and $…
The novel SnO diskettes have been synthesized by evaporating either SnO or SnO(2) powders at elevated temperature. Disregard the source material being SnO or SnO(2), the SnO diskettes are formed at a low-temperature region of 200-400 degrees C. Two types of diskette shapes have been identified: the solid-wheel shape w…
Bagasse was converted into a thermo-moldable material by cyanoethylation. The effect of reaction conditions employed during the preparation of cyanoethylated bagasse (CE-B) fibers on dielectric properties of hot-pressed composites was studied. Increase in the nitrogen content of the cyanoethylated fiber, i.e., the nit…
Plant fibers are of increasing interest for use in composite materials. They are renewable resources and waste management is easier than with glass fibers. In the present study, longitudinal stiffness and strength as well as morphology of unidirectional sisal–epoxy composites manufactured by resin transfer molding (RT…
The geometries and electronic properties of small lithium-rich ${\mathrm{Al}}_{N}{\mathrm{Li}}_{5N}$ $(N=1--6,10)$ clusters are studied using first-principles simulations. Aluminum ions form a compact inner core configuration in the clusters that changes into a chainlike skeleton embedded in a lithium surrounding as t…
Poly(ester-urethane-imide)s were prepared by Diels–Alder polyaddition of 1,6-hexamethylene-bis(2-furanylmethylcarbamate) with various bismaleimides containing ester groups in the backbone. The Diels–Alder reaction was carried out in m-cresol, at 110°C, followed by thermal and chemical aromatization of tetrahydrophthal…
It was demonstrated that the oxyfluoride NbO2F with an ReO3-type structure is a promising electrochromic material with wide band gap. Measurement of diffuse reflectance spectra revealed the optical band gap of NbO2F (∼3.1 eV) to be wider than that of WO3 (∼2.6 eV). It was rendered electron conductive by heating at 770…
The origin of the microscopic motions that lead to stress relaxation in deeply supercooled liquid remains unclear. We show that in such a liquid the stress relaxation is locally anisotropic which can serve as the driving force for the hopping of the system on its free energy surface. However, not all hoppings are equa…
We report direct transmission electron microscopy evidence of self-organized, ordered array of coherent orthogonal column nanostructures in epitaxial La0.8Sr0.2MnO3 (LSMO) thin films grown on (001) LaAlO3 (LAO) using pulsed-laser ablation. The orthogonal column nanostructures have an orthorhombic structure and are epi…
The dielectric behavior of the pyrochlore (Bi3/4Zn1/4)2(Zn1/4Ta3/4)2O7 compound has been studied. A low-temperature dielectric relaxation was observed in a low-permittivity matrix with ε=∼60. The dielectric relaxation process follows a modified Debye model in the vicinity of the relaxation peak, and the relaxation rat…
Direct observation of polarization distribution at nanoscale by scanning force microscopy across partially etched Pb(Zr,Ti)O3 film ferroelectric capacitors with size 2×3 μm and preferential orientation (111) has revealed an anomalous polarization pattern characterized by polarization inversion in the center of the cap…
A short enumeration of the phytoplankton composition of some lakes and ponds of Bali is given, with discussion and illustration of rare or interesting taxa (Hariotina polychorda (KORSIKOV) E. HEGEWALD, Desmodesmus komarekii (E. HEGEWALD) E. HEGEWALD, Golenkinia brevispicula E. HEGEWALD et SCHNEPF, Staurastrum bibrachi…
The effect of 5- and 10-MeV electron irradiation and subsequent annealing upon the optical absorption of ${\mathrm{CdS}}_{1\ensuremath{-}x}{\mathrm{Se}}_{x}$ quantum dots embedded in a borosilicate glass matrix is studied. Gradual smearing and vanishing of the confinement-related maxima and a blue shift of the absorpt…
We derive thermodynamical functions for some large unit cell ionocovalent crystals from the well known quasiharmonic free energy model with the help of ab initio calculations. In order to keep the computation time within reasonable bounds the ab initio assessment applies only to the cohesive energy as a function of vo…