Problems and Pitfalls in Diagnostic Electron Microscopy
Extended abstract of a paper presented at Microscopy and Microanalysis 2012 in Phoenix, Arizona, USA, July 29 – August 2, 2012.
Materials Literature
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Extended abstract of a paper presented at Microscopy and Microanalysis 2012 in Phoenix, Arizona, USA, July 29 – August 2, 2012.
A new method of calculating the spectral function of system-bath interaction during elementary biochemical reaction is proposed. This method was applied to the primary electron transfer in the photosynthetic reaction center of purple bacteria Rh. Sphaeroides. The calculated spectral functions differ significantly from…
Extended abstract of a paper presented at Microscopy and Microanalysis 2012 in Phoenix, Arizona, USA, July 29 – August 2, 2012.
In the article the results of the experiments on determining the possibility of ultrasonic coagulation of aerosol in air flow. The experiments were carried out at different rate of air flow. It is shown, that the application of ultrasonic influence allows to increase purification efficiency of gas flow in 3 to 6 times…
The possibility of the local polarization of epitaxial Ba 0.8 Sr 0.2 TiO 3 thin film is studied by means of piezoresponse force microscopy. The existence of a local polarized state depends on the duration of the applied pulse. The kinetics of polarized states explaining the experiment is considered in the context of p…
An original technique to obtain porous sheets from various inorganic substances (silicon dioxide, hydroxyapatite, and silver) using polymer matrices whose high-disperse structure is formed by the crazing mechanism has been described. The structure of a porous sheet and its characteristics can vary in wide ranges (the…
Polymers are normally used as insulators in many industrial applications due to their high resistivity but there are important developments where polymers can be used as conductors. Electrically conductive polymers find applications in electromagnetic shielding, antistatic coatings, organic light emitting diodes (OLED…
2,3,7,8,12,13,17,18-Octaethyl-21-methylporphyrin and 2,3,7,8,12,13,17,18-octaethyl-22,23-dimethylporphyrin monotriflate based on the former were synthesized. Basic and complexing properties of these compounds were studied by the method of spectrophotometric titration in acetonitrile-perchloric acid and acetonitrile-te…
The average energy expended by an energetic electron to create an ion pair in air, W air is an important quantity in radiation dosimetry. The data obtained by Domen and Lamperti using electron beams in the energy range from 15 to 50 MeV can be used to extract a value for W air if the electron stopping powers of graphi…
This study is performed primarily to investigate the effects of chemical modification on silica surface and the silica content on the thermal and gas barrier properties of a cyclo olefin copolymer (COC) matrix. The COC/SiO 2 nanocomposites were constructed from COC and three species of SiO 2 nanoparticles (AEROSIL A20…
In order to optimize our field-emitting silicon structures, the influence of geometric parameters like aspect ratio, aperture angle and curvature on the field enhancement factor was investigated by finite element simulations. A universal geometric model consisting of a rounded triangle and elliptic curvatures was take…
The hydrophilic states of stainless steel surface treated by the separate or combined use of gaseous ozone and heat were investigated by measuring the contact angle of a water droplet, the content of the surface carbon contaminants, and the adsorption isotherm of water vapor. Super-hydrophilic states of stainless stee…
This paper describes structure evaluation of GexSbyTez (GST) film fabricated by chemical vapor deposition (CVD). We successfully established composition controlled GST CVD with smooth surface by applying appropriate deposition conditions. By increasing Ge flow rate or reducing substrate temperature, the average grain…
The wheat midge, Sitodiplosis mosellana (Géhin) (Diptera: Cecidomyiidae), is one of the most serious pests of wheat worldwide. It overwinters as cocooned larvae in diapause and non-diapause forms. The cocoon is made of silk from the salivary glands. The silk glands, therefore, play an important role in the S. mosellan…
A technique for calculating the adhesion-diffusion formation of a multilayer metal-ceramic structure is presented. The development of this technique is dictated by requirements imposed on the wall of the liquid metal flow channel of a fusion reactor blanket. The parameters of the adhesion-diffusion process (pressure,…
The kinetics of generation of internal mechanical stresses σ( d ) in chromium, copper, gold, and aluminum thin films on single-crystal silicon substrates at different deposition rates has been experimentally investigated using the cantilever method. A two-step character of the variations in internal tensile stresses h…
In this work, PVDF-BaTiO3composites were prepared using cryogenic high-energy ball milling (HEBM). PVDF-BaTiO3mixtures with different weight fractions of submicrometric BaTiO3particles were subjected to 1 h of effective milling. By applying pressure at 200 °C the resulting powder was molded in the form of relatively t…
Electrical trees are defects which can grow in polymeric electrical insulation under high electrical stresses. Their name results from their visual aspect which resembles natural trees. The growth of electrical trees is a precursor to long-term electrical failure; however, the basic mechanism of tree initiation and gr…
The production and the application of hot-melt adhesives and adhesive compositions based on polyamide and the oligoamidoamine derivatives of dimerized fatty acids are studied. The possibility of synthesizing basic polyamide thermoplasts with desired physicochemical properties is shown.
Melamine and boron trioxide (B 2 O 3 ) were directly pyrolyzed in semi-closed system to prepare Boron doped g-C 3 N 4 . The analytic results of XRD, XPS and FTIR proved that g-C 3 N 4 is doped by boron successfully. The thermal decomposition of B doped g-C 3 N 4 has been studied using TGA-DTG technique. The iterative…