Materials Literature
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Nitrile butadiene rubber (NBR) comes into widespread applications due to the excellent performances, but it is susceptible to aging during its storage and usage periods. This paper surveys the external factors that act on the aging process of NBR. The aging of NBR in liquid environment, and non-liquid environment such…
Linear isotactic polypropylene (PP) was chemically modified by solvent-free, peroxide-initiated grafting of trimethylolpropane trimethacrylate and triallyl trimesate. The resulting coagent-modified PP materials possessed bimodal molecular weight and branching distributions, whose populations varied with coagent struct…
Here we report a facile approach to enhance the dispersibility of ethylene vinyl acetate copolymer (EVA)/silica nanocomposites (for the EVA/silica nanocomposites and interaction between silica nanoparticles (nanosilica) and EVA by adding EVA-g-acrylic acid (EVAgAA) as a compatibilizer, which was formed by grafting acr…
The repetitive impulsive surges from inverters has been found undoubtedly to cause insulation reliability flaws in inverter-fed motors. To mitigate this problem, PD detection and life testing under sinusoidal and/or repetitive square voltages should be performed on new types of inverter-fed motor insulation, according…
Extensive numerical results for the thermodynamic density of states (i.e. quantum capacitance) of a two‐dimensional massless Dirac fermion fluid in a doped graphene sheet are presented. In particular, by employing the random phase approximation, the impact of screening exerted by a metal gate located nearby a graphene…
This study is focused on the clay deposits at Akerebiata area in Ilorin (north-central Nigeria), southwestern basement complex, Nigeria. The chemical and mineralogical compositions of the clays were investigated with the aim of determining their provenance, weathering history and most suitable use. X-Ray Diffraction (…
This Paper Aims to Determine by Experiment Total Force and Stress of Deformation Depending on Punch Stroke and the Level of Deformation on Severe Plastic Deformation of Aluminum by Multiaxial Cold Forging. the Deformation Force in Multiaxial Forging Depends on a Number of Parameters of whom the most Important are: Str…
Polyethylene has been one of the widely studied polymeric insulation materials. One of the major issues related to polymeric materials is the easy formation of space charge which may cause electric field enhancement. In this paper, a numerical simulation based on a bipolar charge injection/transport model is used to o…
In this work the usefulness of the technique of thermally stimulated depolarization currents (TSDC) to the study of the secondary relaxations in amorphous solids, and particularly of the Johari-Goldstein (JG) relaxation, is emphasized. The features of the JG relaxation are carefully analyzed, and the contribution of t…
Manufacturing and characterizing hydroxycamptothecin inclusion liposomes, establishing their quality standard and testing their in vitro anti-tumor activity is of significance for potential application. The neutralization agitation method was used to prepare hydroxycamptothecin inclusion and film evaporation method wa…
The manufacturing of metal–ceramic composites was investigated as part of subproject “C3–CerMetComp” at the ECEMP Excellence Cluster in Dresden. Three different manufacturing technologies were investigated: (i) Thermal spraying for the preparation of metal–ceramic multilayers; (ii) tape casting of layered composites f…
Time-resolved synchrotron X‑ray powder diffraction data were used to investigate the dehydration behavior of the chalcophanite (ZnMn 3 O 7 ·3H 2 O) structure from 300 to 1060 K. Rietveld refinements revealed two obvious phase changes, at ∼450 and ∼950 K, corresponding to the dehydration of chalcophanite followed by tr…
Tetrapyrazinocorrolazines — first corrolazine derivatives with annulated heterocycles — have been prepared as phosphorus(V) complexes by the reaction of metal free tetrapyrazinoporphyrazines [( R 8 TPyzPA ) H 2 ] (R = Ph, Me) with phosphorus(III) chloride or bromide in pyridine. Oxophosphorus(V) complexes [( R 8 TPyzC…
The results from a comprehensive investigation of the structure, phase and chemical composition, microhardness, and nanomechanical and tribological properties of chromium-doped coatings of hydrogenised amorphous carbon a-C:H:Cr are presented. The coatings are deposited via reactive magnetron sputtering in an Ar + C2H2…
This paper explores the crystal chemical features of the bulk and the outermost (001) surface layers of two trioctahedral Li-rich mica-1M (space group C2) polytypes, i.e., a polylithionite (MLG-114) from Li-mica granitic pegmatite at St. Austell (SW England) and a Fe 2+ -rich polylithionite (Ch-140) from a rhyolite at…
The aim of this work is to evaluate the catalytic properties (activity, selectivity, and stability) of PtNi catalysts supported on Ce–Zr−α-Al 2 O 3 (CZA) in the liquid-phase conversion of glycerol and to relate them to the results of the EXAFS characterization. The PtNi/CZA catalyst presents the highest global activit…
In this paper, magnetic and fluorescent bifunctional YbPO4:Er,Dy microspheres were synthesized via a simple solvothermal method. The prepared microspheres exposed to 980 nm near-infrared (NIR) laser light emitted bright upconversion fluorescence (450-570 nm) after calcination at high temperatures (>800°C). Results of…
Considering the versatility of 5,10,15,20-tetrakis(pentafluorophenyl)porphyrin (TPPF 20 ) to react with nucleophiles we highlight here the synthesis and characterization of several mono- and tetra-thiocarboxylate derivatives. The selective displacement of the para-fluorine groups in TPPF 20 by thiocarboxylic acids dem…
First chiral bornane[2,3-b]pyrazino-fused [30]trithiadodecaazahexaphyrins were prepared by a crossover condensation of R-(+)- or S-(–)-bornane[2′,3′-b]-2,3-dicyanopyrazine and 2,5-diamino-1,3,4-thiadiazole using two different methods. R-(+)- and S-(–)-enantiomers were characterized by their optical rotations and circu…
Silver nanoparticles (AgNPs) were successfully synthesized and impregnated on silica using chemical reduction methods. XPS and Ag K-edge XANES analysis revealed that the impregnation of AgNPs onto silica using a chitosan + sodium borohydride (NaBH4) method results in higher silver loading and Ag(0)/Ag(I) ratio compare…