Materials Literature
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A series of new double N -alkylated dimethine cyanine dyes were synthesized, and their crystal structures and spectral properties, as well as their interaction with biomolecules and living cells, were investigated.
We investigate electrical and magnetic properties of an A-site-ordered perovskite SrCu 3 Fe 4 O 12 and clarify its negative thermal expansion mechanism.
In this paper, the application of non-local fractional continuum model for plane strain and plane stress elasticity is presented. The kinematics and stress concepts are discussed, and governing equations in terms of displacements for both plane problems are defined. The numerical implementation utilising generalised f…
The tert-butylsulfanylphthalonitrile has been prepared with optimized synthetic procedure. Metal free (H2Pc) and metallo phthalocyanines (Pcs) (ZnPc, CoPc, CuPc, PbPc) have been synthesized by cyclotetramerization of tert-butylsulfanylphthalonitrile in the presence of DBU and metal salts. Thus, tert-butylsulfanyl grou…
Manufacture and performance of a composite carbon-based supercapacitor that employs a gel polymer ionic liquid electrolyte to achieve stable, long cycle life, high-current draw energy storage is discussed in this paper. This supercapacitor when cycled galvanostatically can achieve a discharge capacitance of 43.0 mF pe…
The thermal, rheological, and mechanical behavior of copolymers of lactide, isosorbide, and three different phthalic acids are studied in a wide range of compositions. A linear behavior in glass transition temperature (Tg) with respect to the mole fraction of isosorbide and phthalate content in the copolymers is obser…
Some new Cu(II) complexes containing [1,2,3]-triazole-based bidentate salicylaldimine and its analogues with terminal substituent (F, Cl, Br and I) have been synthesieed. All the target complexes and their uncoordinated ligands were elucidated by elemental analysis and spectroscopic techniques (UV-visible, FT-IR, 1D,…
Pr2O3 and Pr6O11 doped ZnO thin films were prepared by the sol–gel method respectively. The microstructure and electrical characteristics of the samples were investigated by X-ray diffraction (XRD), atomic force microscopy (AFM), varistor dc parameter analyser and impedance analyser. Two kinds of Pr-oxide doped ZnO th…
A clear structure-property relationship was revealed in a series of triphenylene-based dimers, which contained two triphenylene nuclei each bearing five β-OC4H9 substituents and are linked through a flexible O(CH2)nO polymethylene chain (n=6-12). Dimers with the linkage close to twice the length of the free side chain…
The return of supercooled water to a stable equilibrium condition is an irreversible process which, in large enough samples, takes place adiabatically. We investigated this phenomenon in water by fast imaging techniques. As water freezes, large energy and density fluctuations promote the spatial coexistence of solid a…
X-ray photon correlation spectroscopy (XPCS) of swollen rubber containing spherical silica nanoparticles is reported. It is shown that irradiation by intense X-rays leads to the breakdown of cross-links, thereby inducing the local rearrangement of silica nanoparticles. This rearrangement process depends on the cross-l…
Thermally stimulated luminescence glow curves of CaB4O7:Dy samples after β-irradiation showed glow peaks at ~335, 530 and 675 K, with a heating rate of 2 K/s. The main peak at 530 K was analyzed using the Tmax-Tstop method and was found to be composed of at least five overlapping glow peaks. A curve-fitting program wa…
A novel hydrophilic PAMPS-PAAm brush pattern is fabricated to selectively capture blood cells from whole blood. PAMPS brushes provide antifouling surfaces to resist protein and cell adhesion while PAAm brushes effectively entrap targeted proteins for site-specific and cell-type dependent capture of blood cells.
In this paper we present the measurement of temperature differences between the ambient air and the body temperature of a sheep (Heidschnucke) and its applicability for thermoelectric energy harvesting from livestock, demonstrated via the test of a specially tailored TEG system in a real-life experiment. In three meas…
Superhydrophobic surfaces aid biochemical analysis by limiting sample loss. A system based on wells here tolerated tilting up to 20° and allowed air logic transfer with evidence of mixing. Conditions for intact transfer on 15 to 60 μL drops using compressed air pressure operation were also mapped.
Abstract In vielen biologischen Systemen wird die Erkennung von Oberflächen durch die Wechselwirkung von Kohlenhydrat‐spezifischen Proteinen (Lektinen) mit den Kohlenhydratepitopen (Liganden) der ungeordneten Glycokonjugatschicht (Glycokalyx) der Zellen gesteuert. Damit es zu einer erfolgreichen Anbindung kommt, müsse…
This theoretical study suggests that CH⋅⋅⋅π stacking interactions between monomeric units can be used to design novel single-chain magnets (SCMs), as the sign of coupling is predictable and such chains inherently yield negative axial anisotropy, a condition often difficult to achieve in conventional SCMs.
A facile fabrication of flower-shaped porphyrin Janus colloids with oriented arrangement was demonstrated based on the interfacial assembly and water droplet template. The as-fabricated colloidal crystals from flower-shaped Janus particles show a special optical signal produced from the hierarchical structures.
Several experiments reveal the inhomogeneous character of the superconducting state that occurs when the carrier density of the two-dimensional electron gas formed at the LaXO3/SrTiO3 (X=Al or Ti) interface is tuned above a threshold value by means of gating. Re-analyzing previous measurements, that highlight the pres…
Microcrystalline cellulose (MCC) was prepared by hydrochloric acid hydrolysis from Muli bamboo (Melocanna baccifera) fibers to tap its potential as a green source of MCC. The cellulose and α-cellulose yield from the original material were 62.5 and 54.8 % respectively. The physicochemical properties of the prepared MCC…