Materials Literature
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The dependence of the microhardness H of macroporous silicon layers formed on the duration t an of electrochemical anodization at a constant current density of J = 20 mA/cm2 is studied. It is shown that the nonlinear run of the dependence H(t an) is due to the influence exerted on the microhardness not only by the sur…
Electromagnetic characteristics of metal polarization gratings are studied by means of the finite-difference time-domain technique in the case of long-wavelength diffraction of electromagnetic waves. Dimensions of gratings with rectangular bridges providing for optimal regimes of propagation of H - and E -polarized wa…
The state of gold deposited from a chloride solution on the surface of the porous magnetite-carbon composite obtained from modified birch saw dust at 400 and 800°C was studied by electron microscopy, X-ray photoelectron spectroscopy, and XRD analysis. The shape and size of the deposited gold crystallites depend on the…
The electrodeposition of ZnO nanorods was performed on ITO glass. The optimization of two process parameters (solution temperature and growth time) has been studied in order to control the orientation, morphology, density, and growth rate of ZnO nanorods. The structural and optical properties of ZnO nanorods were syst…
자동차 산업의 발달과 함께 환경오염 문제가 심각해지면서 연간 300,000톤 이상 발생하는 폐타이어의 재활용에 대한 관심이 높아지고 있다. 본 연구에서는 폐타이어 재활용을 목적으로 40, 80, 140 mesh 크기의 폐타이어 분말을 선별한 후, 입도 분석을 통하여 크기를 확인하고 그 형상을 SEM을 통해 관찰하였다. 또한 각각의 폐타이어 분말을 Virgin PP와 혼합하고 Intermeshing Corotating Twin Screw Extruder를 이용하여 TPV를 제조하고 특성 분석을 하였다. 이 중 효과가 좋은 140 mesh의 폐타이어 분말과 Virgin…
The effective water management in a polymer electrolyte membrane fuel cell (PEMFC) is one of the key strategies for improving cell performance and durability. In this work, an ex situ measurement was carried out to understand the water droplet behavior on the surface of gas diffusion layer (GDL) as a fundamental study…
Despite the discovery of new superconductors classes, high-Tc oxides continue to be a current topic, because of their complex phase diagrams and doping-dependant effects (allowing one to investigate the interaction between orbitals), as well as structural properties such as lattice distortion and charge ordering, amon…
Phase equilibria in the Tl 2 S-SnS-PbS quasi-ternary system were studied by differential thermal, X-ray powder diffraction, and microstructural analyses. The following schemes were constructed: the state diagrams of the partially quasi-binary sections Tl 4 SnS 3 -Tl 4 PbS 3 , PbS-Tl 4 SnS 3 , and PbS-Tl 2 Sn 2 S 3 , t…
The energetic evaluations of graphite-to-diamond transition by electron irradiation are performed. The heat conduction problem is solved for the diamond synthesis when a pulse-periodic source of energy is located within a graphite cylinder; time dependences of temperature and pressure are found. It is shown, that the…
We study the stability of the radial-hedgehog solution on a three-dimensional (3D) spherical shell with radial boundary conditions, within the Landau-de Gennes theory for nematic liquid crystals. We show that the radial-hedgehog solution has no zeroes for a sufficiently narrow shell, for all temperatures below the nem…
During the initial feasibility test using actual used nuclear fuel (UNF) cladding in FY 2012, an incubation period of 30–45 minutes was observed in the initial dry chlorination. The cladding hull used in the test had been previously oxidized in a dry air oxidation pretreatment prior to removal of the fuel. The cause o…
Phase equilibria and critical phenomena in the lithium nitrate-water-acetonitrile ternary system were studied by a visual polythermal method within the range of −20 to 50°C. In this ternary system, the constituent liquid binary system is characterized by phase separation with an upper critical solution temperature. It…
Super duplex stainless steels (sDSS) are excellent for use under severely corrosive conditions such as offshore and marine applications like pipelines and flanges. sDSS has better mechanical properties and corrosion resistance than the standard duplex stainless steel (DSS) but it is easier for a sigma phase to appear,…
In this study, TiAlSiN coatings have been successfully synthesized on stainless steel and tungsten carbide substrate by a hybrid coating method employing a cathodic arc and a magnetron sputtering source. TiAl and Si target were vaporized with the cathodic arc source and the magnetron sputtering source, respectively. P…
Abstract Carbon dioxide generated from construction materials and construction material industry among the fields of construction isapproximately 67 million tons. It is about 30% of the carbon dioxide generated in the fields of construction. In order to reducecarbon dioxide in the fields of construction, it is necessa…
The primary purpose of this research is to investigate how much the complexing agent in electroless Cu electrolytes will affect adhesion strength between copper film and Ta diffusion barrier for Cu interconnect of semiconductor. The adhesion strength using rochelle's salt as complexing agent was higher than the case o…
The complexation reaction of 4,13-diaza-18-crown-6 (DA18C6) with Y3+ cation was studied in some binary mixed solvent solutions of acetonitrile (AN) with methanol (MeOH), ethanol (EtOH), 2-propanol (2-PrOH) and methyl acetate (MeOAc) at different temperatures by conductometric method. The obtained data show that in all…
지오폴리머 반응은 매우 복잡하며, 플라이애쉬 화학조성, 입도분포, 자극제 농도와 종류, 양생온도, 양생시간 등이 지오폴리머 물성에 많은 영향을 미치고 있는 것으로 알려져 있다. 이 연구에서는 양생조건이 플라이애쉬 기반 지오폴리머 강도에 미치는 영향을 실험하기 위하여, 양생온도, 고온양생 전 전치시간, 고온에서의 양생시간 등을 변화시켜 양생조건 변화에 따른 지오폴리머 페이스트의 압축강도, SEM, 공극특성 등에 대하여 분석하였다. 실험 결과 양생온도가 높을수록 지오폴리머의 강도는 증가하였으며, 전양생시간이 길어질수록 지오폴리머 강도는 증가되었으나, 고온양생에서의 양생…
Wear and corrosion of the engine parts surrounded with combustion chamber is more serious compared to the other parts of the engine because temperature of the exhaust gas in a combustion chamber is getting higher and higher with increasing of using the heavy oil of low quality. Therefore, an optimum repair weldment as…
Simulation studies on catalytic methanation reaction in externally cooled tubular reactor filled with monolithic catalysts were carried out using a general purpose modelling tool $gPROMS^{(R)}$ . We investigated the effects of operating parameters such as gas space velocity, temperature and pressure of feeding gas on…