Materials Literature
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Abstract A mixture of acetylene and xylene is used as the carbon source to directly synthesize carbon nanotube (CNT)/alumina (Al 2 O 3 ) microsphere hybrid structures by CVD. The hybrid structures are modulated by varying the acetylene ratio and reactor temperature. The addition of acetylene can significantly improve…
Abstract Erbium‐doped yttrium oxide films are prepared from yttrium acetylacetonate (Y(C 5 H 7 O 2 ) 3 ) and erbium (III) tris(2,2,6,6‐tetramethyl‐3,5‐heptanedionate) (Er(TMHD) 3 ) under standard conditions by UV‐aerosol‐assisted metal‐organic (AA‐MOCVD), using air with controlled humidity as the carrier gas. The stru…
Spherical, triangular (prismatic) and square plate shaped gold nanoparticles have been synthesised from HAuCl4 · 3H2O solution using the aqueous leaf extract of Cocculus hirsutus. Nanoparticles are characterised using higher resolution transmission electron microscope, X-ray diffraction and UV–Vis absorption spectrosc…
We investigated the interactions of different types of human and porcine renal proximal tubule-derived cells with core-shell CdSe@ZnS quantum dots (QDs) coated with polymerized histidine-formaldehyde (pHF). The results revealed that porcine and human proximal tubule cells showed a markedly different uptake behavior. T…
The high level of accumulated expertise by ULIS and CEA/LETI on uncooled microbolometers made from amorphous silicon with 45, 35, and 25 μm enables ULIS to develop video graphics array (VGA) and extended graphics array (XGA) infrared focal plane array (IRFPA) formats with 17-μm pixel pitch to fulfill every application…
We examine the growth and evolution with time of bipyramidal gold nanoparticles grown by a seed-mediated process. The nanoparticles are characterized both by their physical dimensions determined by transmission electron microscopy and by the wavelength position of their localized surface plasmon resonance. Each growth…
Abstract Sodium nitrate (mineral nitratine, NaNO 3 , space group R $ \bar 3 $ c at room temperature) is a material used in a great variety of fields, such as the molten salt technology. It is also of very interest from a crystallographic point of view, being iso‐structural with calcite (CaCO 3 ). We performed several…
Pt–Bi films were synthesized on glass and thermally oxidized silicon substrates by e-beam evaporation and annealing. The structures were characterized using X-ray diffraction (XRD) and transmission electron microscopy/selected area electron diffraction (TEM/SAED) techniques. Single-phase PtBi was obtained at an anneal…
Structurally well-defined trimethylated chitosan-O-poly(ε-caprolactone) (TMC-O-PCL) was synthesized under mild homogeneous conditions, using sodium dodecyl sulfate-dimethylated chitosan complex (SDC) as an organosoluble intermediate. The effect of chitosan molecular weight (MW) on the preparation, organosolubility, se…
The effect of laser irradiation on the optical properties of thermally evaporated Se100−x Te x (x=8, 12, 16) chalcogenide thin films has been studied. The result shows that the irradiation causes a shift in the optical gap. The results have been analyzed on the basis of laser irradiation-induced defects in the film. T…
Abstract This article reports the application of Fourier Transform Infrared‐Attenuated Total Reflectance (FTIR‐ATR) technique for investigation of in situ polymerization of polyurethane‐urea elastomers. Formulations comprising of diisocyanates, a polyether diol and a diamine based chain extender have been used in this…
Photoemission replenishment criterion (PRC) is widely used to evaluate the onset conditions for negative corona discharges in atmospheric air. The relationship between the PRC and the air density is built up in this paper, which is validated for a wide range of electrode radii and low air densities. The total effectiv…
We report on the influence of a silicon nitride gate dielectric in graphene-based field-effect transistors (FETs). The silicon nitride is formed by a plasma-enhanced chemical vapor deposition method. The process is based on a low-density plasma at a high pressure (1 torr), which results in a low degradation of the gra…
The side-arms of neurofilaments (NFs) have been proposed to be highly disordered, leading to an entropically and electrostatically based repulsion that modulates interfilament spacing. To characterize the behavior of two interacting polymer brushes in a system of this type, we performed molecular dynamics simulations…
A technique adapted from the guarded-comparative-longitudinal heat flow method was selected for the measurement of the thermal conductivity of a nuclear fuel compact over a temperature range characteristic of its usage. This technique fulfills the requirement for non-destructive measurement of the composite compact. A…
Abstract Poly(vinyl alcohol) (PVA), a well‐known synthetic biodegradable, biocompatible, and hydrophilic polymer is susceptible to several structural modifications, due to the presence of hydroxyl groups in its backbone. PVA was grafted with L (+)‐lactic acid (LA) in molar ratios VA/LA (1/1, 1.5/1, and 2.2/1), mangane…
Abstract Isotactic PP nanocomposites filled with Fe@FeO nanoparticles are fabricated by a facile ex situ method. The nanofillers are dispersed in a boiling PP/xylene solution. X‐ray diffraction is used to determine the nanofiller effects on the crystallinity of PP. The crystallinity along the (040) plane is found to d…
Abstract A poly(acrylamide) (PAM) aqueous dispersion with high solid was successfully synthesized through two‐phase polymerization of acrylamide (AM) in aqueous poly(ethylene glycol) (PEG) solution. To prepare stable PAM aqueous dispersion, the effects of initiator, monomer and PEG concentration on the stability of th…
Thermal conduction strongly influences the programming energy and speed in phase-change-memory devices. The thermal conductivity of the crystalline phase of Ge2Sb2Te5can be strongly anisotropic due to phase impurities at grain boundaries. This letter models this effect using effective medium arguments, lends further s…
In this paper, CdSe nanocrystal dissolution in an aqueous solution was studied. It was found that light is a key factor affecting the dissolution of nanocrystals. In the presence of light, the electrons generated from CdSe nanocrystals reduce water to hydrogen and hydroxide ions (OH-) while photo-generated holes oxidi…