Materials Literature
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We developed a hydrogen arc discharge exfoliation method for the synthesis of graphene sheets (GSs) with excellent electrical conductivity and good thermal stability from graphite oxide (GO), in combination with solution-phase dispersion and centrifugation techniques. It was found that efficient exfoliation and consid…
Optically transparent paper of densely packed cellulose nanofibers is prepared without any additives. This material has the same chemical constituents as conventional paper, the only difference being the fiber width and the size of the interstitial cavities. This optically transparent paper exhibits high Young's modul…
Irena , a tool suite for analysis of both X-ray and neutron small-angle scattering (SAS) data within the commercial Igor Pro application, brings together a comprehensive suite of tools useful for investigations in materials science, physics, chemistry, polymer science and other fields. In addition to Guinier and Porod…
Abstract The evolution of FTIR spectra of PS during oxidation is studied in the range 450‐1300 cm –1 . We show that the small scale of the PS structure leads to a significant scattering cross section for Fröhlich surface modes associated to stretching modes in siloxane bridges. The kinetics of the evolution of both bu…
Abstract Up and down: Differential sensing of serine and tyrosine is achieved with aligned CdS nanowire arrays by exploring the pH‐dependent PL behavior of the nanowire arrays toward exposure to the two amino acid solutions (see picture). magnified image The differential sensing of tyrosine and serine is achieved with…
La 0.9 Hf 0.1 MnO 3 (LHMO) films were grown on (001) SrTiO3 (LHMO/STO) and (001) 0.7% Nd-doped STO (LHMO/STON) substrates under the same conditions by using pulsed laser deposition technique. The x-ray diffraction and rocking curve measurements demonstrated high epitaxy and good crystallinity obtained in our films. Th…
The synthesis and characterization of three new 4-pyridyl porphyrin-peptidyl-phosphonate compounds, containing a diphenyl 3-pyridylmethyl-phosphonate moiety, is described in this article. Nitrogen atoms in the pyridine rings of the obtained compounds were alkylated using methyl iodide, to give additional three, water…
Abstract A cellular automata is introduced to model the locally resolved oxide thickness, the stress, and the etching rate dynamics at the silicon electrolyte contact along a macroscopically long line (1 mm). Short‐ and long‐range interaction mechanisms are considered to achieve current oscillations. Extended chronoam…
Impedance spectroscopy has been used to investigate conductivity within boron-doped diamond in an intrinsic/delta-doped/intrinsic (i-δ-i) multilayer structure. For a 5 nm thick delta layer, three conduction pathways are observed, which can be assigned to transport within the delta layer and to two differing conduction…
The developed curved image plate (CIP) is a one-dimensional detector which simultaneously records high-resolution X-ray diffraction (XRD) patterns over a 38.7 degrees 2theta range. In addition, an on-site reader enables rapid extraction, transfer and storage of X-ray intensity information in </=30 s, and further quali…
Abstract Porous silicon (PS) is fabricated by anodization in aqueous hydrofluoric acid solution in the transition region between meso and macro pores. In the employed process the pore‐diameters are adjustable from 30 nm up to 100 nm using the same electrolyte as well as the same doping density of the wafer. Furthermor…
The reversal time of the magnetization of single-domain ferromagnetic particles is estimated for mixed uniaxial and cubic anisotropy energies possessing nonparaboloidal saddles and well bottoms or either. The calculation generalizes the existing adaptation of the Kramers escape rate theory to fine ferromagnetic partic…
The lattice dynamics of Pb1−xLax(Zr0.9Ti0.1)O3 (PLZT X/90/10) with X=0, 2, 4, 10% of La was studied by means of Far Infrared, Raman and terahertz spectroscopies in the temperature range of 20–800 K. Infrared active soft phonons with anomalies near the paraelectric-ferroelectric phase transition were found for all the…
Abstract Der Einbau eines Amid‐Sauerstoffatoms in das Gerüst des Dawson‐Polyoxometallat(POM)‐Clusters [P 2 V 3 W 15 O 62 ] 9− (siehe Bild) ermöglicht elektronische Wechselwirkungen zwischen den organischen und anorganischen Teilen des Moleküls: Die Redoxeigenschaften des gesamten Hybrid‐POM lassen sich mithilfe der or…
Au nanoparticles stabilized by poly(methyl methacrylate) (PMMA) were used as a catalyst to grow vertically aligned ZnO nanowires (NWs). The density of ZnO NWs with very uniform diameter was controlled by changing the concentration of Au-PMMA nanoparticles (NPs). The density was in direct proportion to the concentratio…
A library of 20 000 transposon (Tn5) mutants of the gram-negative bacterium Pseudomonas putida CA-3 was generated and screened for adverse affects in polyhydroxyalkanoates (PHA) accumulation. Two mutants of interest were characterized phenotypically. CA-3-126, a mutant disrupted in a stress-related protein Clp proteas…
We show evidence of a dependence of the enhancement of the Raman scattering cross section on the length of the gradient in graded silver island films. A factor-of-three increase in the Raman signal is observed for gradients with length of the order of 0.5 mm when compared to gradients of the order of 9 mm. Scanning el…
We investigate dielectrophoretic deposition of single-walled carbon nanotubes using an in situ detection system. Pairs of electrodes are stimulated with a small-amplitude, low-frequency voltage superimposed on a large-amplitude, high-frequency dielectrophoretic voltage. Measuring the magnitude of the current both at d…
By carefully controlling the experimental parameters, large-scale nanosponges of group II-B metal (Zn and Cd) on Si substrates are fabricated through a vacuum vapor deposition route (VVD). The as-prepared products are systematically characterized by the techniques of powder x-ray diffraction (XRD), scanning electron m…
Stable ligation: A series of dendritic porphyrins, such as that depicted in which benzyl ether dendrons were linked to a porphyrin core through 1,2,3-triazole links, was synthesized. Absorption and fluorescence spectra showed a stable axial ligation at the zinc center of the porphyrin core by triazole links in dendrit…