Materials Literature
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The CO(2) sorption and polymer swelling of hydroxytelechelic polybutadiene (HTPB) and poly(ethylene glycol) (PEG) have been investigated as a function of temperature and CO(2) pressure by combining in situ near-infrared spectroscopy with molecular modeling. The results reported here for the PEG-CO(2) system are in a v…
Bistable shape memory actuators were fabricated by microsystem technology processes and characterized with regard to their use in tactile graphic displays. The actuators were realized as sputter-deposited buckled metallic thin-film carriers, having structured Ti-Ni-Cu and Ti-Ni-Hf shape memory alloys on the top and at…
This work describes the fabrication, characterization, and protein adsorption behavior of charged polymer gradients. The thin gradient films were fabricated by a two-step technique using UV-initiated free-radical polymerization in a reactor with a moving shutter. A homogeneous layer of cationic poly(2-aminoethyl metha…
Urchin-like nickel particles and prickly nickel chains were selectively prepared by a facile low-temperature chemical reduction method at ambient conditions. The synthetic process involved the chemical reduction of nickel ions and the oriented growth of nickel nanocrystals under kinetic control independent of surfacta…
In this letter, using both off-resonant and resonant Raman spectroscopic techniques, the correlation of optical phonons and structural disorder in As+ implanted ZnO single crystals has been investigated. An additional broad peak shoulder at 550 cm−1 between the transverse optical and longitudinal optical (LO) phonons…
A modified citrate-gel method for the preparation of Bi 3.25 La 0.75 Ti 3− x M x O 12 (BLTM x, M = Mo, W, Nb, V) ferroelectric powder and ceramics is presented. The cosubstituent precursors used were ammonium metal citrate aqueous solutions, which were prepared using corresponding metal oxides as starting materials (V…
On the basis of a quasi-static theory, the sensitivity of surface plasmon resonance to the refractive index of the surrounding medium is investigated for gold nanoboxes with fixed inner edge length. It is found that the refractive index sensitivity increases near-exponentially as the wall thickness is decreased. Howev…
Abstract This study investigates the effect of hemp fibres on the shear and elongational rheology of polypropylene (PP). The parameters studied were hemp content (0‐30%) and maleic anhydride polypropylene (MAPP) addition (0‐0.6%). Shear rheology revealed that fibre content mainly influences low shear rate properties l…
Magnetization, frequency dependent dielectric, and structural studies on 0.73BiFeO3–0.27PbTiO3 in the temperature range from 300 to 600 K reveal anomalies in the unit cell parameters and the intrinsic value of the dielectric constant, free from space charge contributions, at the antiferromagnetic transition temperatur…
Several new protic ionic liquids (PILs) were prepared by mixing trifluoroacetic acid (TFA) with various heterocyclic amines using different base:acid ratios (1:1 and 1:2). Their specific conductivities have been measured by electrochemical impedance spectroscopy and were found ranging from 0.71 to 9.07 mS·cm −1 at 27.…
Adding conductive fillers to nonconductive polymers is a common way to make soft conductive materials such as conductive adhesives. An important issue is how to achieve high volume conductivity with acceptable mechanical performance. Two questions pertaining to this issue were studied in this paper. One question was w…
We present experimental contact angle data for surfaces, which were surface-engineered with a hydrophobic micropattern of hexagonal geometry. The chemically heterogeneous surface of the same hexagonal pattern of defects resulted in faceted droplets of hexagonal shape. When measuring the advancing contact angles with a…
Herein, we report an experimental analysis of the photogenerated current of very thin and uniform dye-sensitized nanocrytalline titanium oxide (nc-TiO 2 ) electrodes coupled to high-quality one-dimensional photonic crystals. The effect of well-defined optical absorption resonances are detected both in optical spectros…
n -ZnO / p -silicon nanowire (SiNW) photodiodes were prepared by radio frequency reactive magnetron sputtering of n-type zinc oxide at room temperature on photoresist filled p-SiNWs, which were fabricated by electroless metal deposition method at 323 K. Our n-ZnO/p-SiNW photodiodes showed good temperature- and light-i…
In this report, the specific contact resistance between a thin film single wall carbon nanotube electrode and a deposited silver contact was measured. The specific contact resistance was found to be 20 mΩ cm2, which is an order of magnitude higher than typically observed in standard Si photovoltaic technology. We demo…
Generalized spectroscopic ellipsometry determines the principal monoclinic optical constants of thin films consisting of slanted titanium nanocolumns deposited by glancing angle deposition under 85° incidence and tilted from the surface normal by 47°. Form birefringence measured for wavelengths from 500 to 1000 nm ren…
Co 2 MnSi / Cr / Co 2 MnSi (001)-fully epitaxial current-perpendicular-to-plane giant magnetoresistance (CPP-GMR) devices were fabricated via an UHV magnetron sputtering system. The relationship between the degree of chemical ordering in Co2MnSi (CMS) and the CPP-GMR characteristics was investigated systematically aga…
The next generation of medical devices and engineered tissues will require development of scaffolds that mimic the structural and functional properties of the extracellular matrix (ECM) component of tissues. Unfortunately, little is known regarding how ECM microstructure participates in the transmission of mechanical…
Quartz crystal microbalance and cyclic voltammetry are used to investigate the influence of the supporting salt of polyelectrolyte solutions on the buildup and the structure of PSS/PAH polyelectrolyte multilayers (PSS: poly(4-styrene sulfonate); PAH: poly(allylamine hydrochloride)). This film constitutes a model polye…
Here we report a detailed study aimed on understanding the origin of ferromagnetism in Ni-doped ZnO films. A pulsed laser deposition technique was used to deposit Ni-doped (5 at. %) ZnO films on sapphire (0001) substrates under different oxygen pressures ranging from 10−6 to 0.1 Torr. Films were characterized using nu…