Materials Literature
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Various nitrogenous bases, such as imidazoles, pyridines and amines were employed as axial ligands in epoxidation reaction of cyclooctene bytetra-n-butylammonium hydrogen monopersulfate (n- Bu 4 NHSO 5), in the presence of Mn ( III )-tetrakis(2,3-dimethoxyphenyl)porphyrin-acetate ( T (2,3- OMeP ) PorMnOAc ). T (2,3- O…
A detailed description of the distribution, interaction, and dynamics of molecules with biological activity dissolved in a hydrophobic bilayer, a simple model of a biological membrane, provides valuable information for a better understanding of drug functioning, which can be very useful in drug design. Here we present…
We study the scattering phase shift of Dirac fermions at graphene edge. We find that when a plane wave of a Dirac fermion is reflected at an edge of graphene, its reflection phase is shifted by the geometric phase resulting from the change of the pseudospin of the Dirac fermion in the reflection. The geometric phase i…
Abstract Green synthesis and characterisations of silver-polyvinyl alcohol nanocomposite films for possible environmental and biomedical applications such as wound dressing have been investigated. The synthesis was carried out in water, in an environmentally-friendly solvent using β-D-glucose as a reducing agent and i…
This work investigates jammed granular matter under conditions that produce heterogeneous mass distributions on a mesoscopic scale. We consider a system of identical disks that are confined to a narrow channel, open at one end and closed off at the other end. The disks are jammed by the local pressure in a gravitation…
A synthetic protocol for the construction of new meso-substituted pyrrolo[1,2-a]quinoxalinoporphyrins is described starting from 5-(4-amino-3-nitrophenyl)-10,15,20-triphenylporphyrin. The reaction of this porphyrin with 2,5-dimethoxytetrahydrofuran, followed by the reduction of the nitro group in the presence of NiCl2…
Measurements of the specific heat jump at the onset of superconducting transition in the iron-pnictide compounds revealed strong variation of its magnitude as a function of doping that is peaked near the optimal doping. We show that this behavior is a direct manifestation of the coexistence between spin-density wave a…
Carbon nanotubes (CNTs) can be grown in dense lithographically patterned forests to form framework structures that can be filled in via chemical vapor deposition to form solid structures. These solid structures can then be used in microelectromechanical systems (MEMS) applications. Initial testing with these structure…
This study investigates the cryogenic performances of a millimeter-size piezoelectric ultrasonic linear micromotor. The piezoelectric vibrator of the micromotor is made of Pb(In1/2Nb1/2)O3 -Pb(Mg1/3Nb2/3)-PbTiO3 single crystal and operated in first-bending wobbling mode. Experiments show that the piezoelectric single…
We report negative magnetoresistance in pulsed laser deposited single phase ZnO and Mg0.268Zn0.732O films and attribute it to the presence of oxygen interstitials (Oi) and zinc interstitials (Zni) as observed in the X-ray photoelectron spectra of the films. An interesting feature of reduction of negative magnetoresist…
In view of the scientific and technical challenges as well as the considerable economic stakes (amounting to millions of U.S. dollars), this chapter focuses on the recent developments on the corrosion of steel by sulfidogenic anaerobes. The corrosion layer is an active membrane where a looped interaction between the c…
We make a summary of our research and development efforts made about microbolometers (MBs) based on plasma-enhanced chemical vapor deposition (PECVD) materials, like noncrystalline semiconductors that provide high temperature coefficient of resistivity values, in conjunction with SiOx and SiNx dielectrics used for the…
A wood-based composite was prepared via simple electroless Ni-Cu-P plating on birch veneer for EMI shielding. The effects of CuSO 4 5H 2 O concentration on the metal deposition, elemental composition, phase structure, surface morphology, wettability, surface resistivity, and shielding effectiveness of coatings were in…
Pure nickel micro particles were chemically treated with various concentrations of NaOH and were subsequently annealed in 800 °C. The dimensions of the resulting nanosteps were tuned by simply varying the annealing time durations. Formation of Ni-NiO composite phase was confirmed by x-ray diffraction studies. The morp…
Abstract The paper presents the investigation of GdNiH3.2 hydride magnetocaloric properties. The isothermal magnetization in the fields up to 5 T and heat capacity data are obtained for GdNiH3.2 and GdNi compounds. The maximum value of magnetic entropy change ΔSM in GdNiH3.2 is extremely large and obtained in much low…
The permeability of the polymer walls of polyalkylcyanoacrylate nanocapsules varies by different degrees of chemical cross-linking. For this reason, different amounts of bivalent alkylcyanoacrylates are added to the monovalent alkylcyanoacrylate prior to an interfacial polymerization step in order to generate capsules…
The high potential of reversible (or regenerative) solid oxide cell (rSOCs) systems for energy storage application motivates the present study which focuses on predicting rSOC performance through mathematical modeling. An intermediate fidelity model that can be used for identifying favorable electrochemical and therma…
Optimal properties like piezoelectricity can be found in polarizable materials for which the structure changes sharply under small composition variations in the vicinity of their morphotropic phase boundary or the triple point in their isobaric temperature-composition phase diagram. In the latter, lead-free (Ba0.850Ca…
In this paper, we present our results of experimental and numerical pull-out tests on carbon nanotubes (CNTs) embedded in palladium. We prepared simple specimens by employing standard silicon wafers, physical vapor deposition of palladium and deposition of CNTs with a simple drop coating technique. An AFM cantilever w…
We present experiments and numerical simulations to investigate the collective behavior of submicrometer-sized particles immersed in a nematic micellar solution. We use latex spheres with diameters ranging from 190 to 780 nm and study their aggregation properties due to the interplay of the various colloidal forces at…