Materials Literature
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Abstract Polymerization of p‐n‐ hexyloxyphenylacetylene (pHPA) by using a [Rh(norbornadine)Cl] 2 ‐triethylamine catalyst was carried out at room temperature to afford stereoregular helical poly( p ‐ n‐ hexyloxyphenylacetylene)s (PpHPAs). When ethanol and n ‐hexane were used as polymerization solvents, a bright yellow…
Photochemical etching of CdSe nanoplatelets was studied to establish a relationship between the nanocrystal surface and the photochemical activity of an exciton. Nanoplatelets were synthesized in a mixture of octylamine and oleylamine for the wurtzite (W) lattice or in octadecene containing oleic acid for the zinc-ble…
Using a femtosecond laser, we have transformed the laser-direct-writing technique into a highly efficient method that can process AgO(x) thin films into Ag nanostructures at a fast scanning rate of 2000 μm(2)/min. The processed AgO(x) thin films exhibit broad-band enhancement of optical absorption and effectively func…
Only a small fraction of all available metals has been used as electrode materials for carbon-based devices due to metal-graphene interface debonding problems. We report an enhancement of the bonding energy of weakly interacting metals by using a metal-graphene-metal sandwich geometry, without sacrificing the intrinsi…
The complex admittance of metal/oxide/pentacene thin film junctions is investigated under ambient conditions. At low frequencies, a contribution attributed to proton diffusion through the oxide is seen. This diffusion is shown to be anomalous and is believed to be also at the origin of the bias stress effect observed…
The image fractal analysis is actively used in all science branches. In particular in materials science the fractal analysis is applied to study microstructure of deformed metals because its structure can be interpreted as the fractal image. It is well known that such images can be described by fractal dimension. In t…
Hexagonal boron nitride (h-BN) is a promising dielectric material for graphene-based electronic devices. Here we investigate the potential of h-BN gate dielectrics, grown by chemical vapor deposition (CVD), for integration with quasi-freestanding epitaxial graphene (QFEG). We discuss the large scale growth of h-BN on…
Room-temperature ultraviolet lasing in [0001] oriented zinc oxide nanorods grown on silicon and fused silica substrates by a simple vapor transport and condensation process. These wide band-gap semiconductor nanorods form natural laser cavities with diameters varying from 150 to 350 nm and lengths up to 10 µm. Under o…
In 2011, a survey conducted all over the world says that more than 7 million humans around the world died of cancer. One in three women and one in two men developed cancer during their lifetime. About 15 percent of all deaths worldwide, was attributed to cancer. In some nations, cancer will surpass heart disease to be…
The performance of solid oxide fuel cells (SOFCs) is often determined by the polarization resistance of the electrodes. Electrochemical impedance spectroscopy (EIS) enables a deconvolution of individual electrochemical processes. In case of mixed ionic-electronic conducting (MIEC-) cathodes the impedance spectra resul…
Ethylene is the smallest ripening hormone in plants. In their Communication on page 5752 ff., T. M. Swager et al. show that from a simple mixture of single-walled carbon nanotubes and a copper(I) complex, chemoresistive devices can be prepared that are highly sensitive and selective to sub-ppm concentrations of ethyle…
Este trabalho teve por finalidade avaliar o desempenho fisico e mecânico de tres formulacoes de adesivo PVA atraves das normas brasileiras de compensados e avaliar os valores obtidos com os encontrados em literaturas relacionadas. O trabalho detalha o processo produtivo dos paineis, obtencao de corpos de prova e, fina…
Single crystal thin films of 10% yttrium doped barium zirconate (BZY10) have been prepared using chemical solution deposition on magnesium oxide substrates and annealed at 800 or 1000ºC. A focused ion beam lift out technique was used to prepare thin (< 100 nm) specimens for transmission electron microscopy (TEM) an…
The corn flour composite fillers were prepared by blending corn flour with rubber latex, dried, and cryogenically ground into powders, which were then melt-blended with rubber polymers in an internal mixer to form composites with enhanced mechanical properties. The composites prepared with melt-blending method were co…
Gold nanoparticles supported on yttria-stabilized zirconia (YSZ) were synthesized using a modified alcohol method which involves the stabilizing agent, polyvinylpyrrolidone (PVP). Two different average sizes (13.1 and 17.1 nm) of Au nanoparticles were synthesized. These catalysts were tested for gas phase CO oxidation…
Nacre is composed of about 95 vol.% aragonite and 5 vol.% biopolymer and famous for its “brick and mortar” microstructure. The phase transition temperature of aragonite in nacre is lower than the pure aragonite. In situ XRD was used to identify the phase transition temperature from aragonite to calcite in nacre, based…
Abstract The polyolefin blends of high‐density polyethylene (HDPE) with two types of fluorothermoplastics (THV500 and THV220); were prepared by melt compounding technique. The morphology, crystallization, and the viscoelastic measurements of the blends were carried out. The dispersion of THVs was studied by scanning e…
Our zero-dimensional and isothermal stationary model predicts the current-voltage (C/V) characteristics of anode supported SOFC single cells in the direct as well as in the reverse (electrolyzer) operation mode. An extended model is presented for the electrolyzer mode, taking the corrected cell temperature as addition…
The unsteady growth of ammonium chloride dendrites during crystallization from an aqueous solution in a thin capillary is experimentally investigated. The dependence of the crystal area S on the time t for various sectors located along primary branches and side branches is measured. The hypothesis that the ratio betwe…
Abstract Recently there has been interest in developing imaging contrast media for magnetic resonance imaging (MRI) that contain biologically rare, magnetically active nuclei such as fluorine. In principle, fluorinated contrast agents can be used to generate highly selective 19 F magnetic resonance images that can be…