Materials Literature
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The influence of humidity on the dielectric constant and leakage current of self-assembled porous silica films which have two-dimensional hexagonal periodic porous structures was investigated quantitatively by proposing a new water adsorption model. The amount of adsorption was calculated by the modified Rayleigh mode…
A new monomeric diiron beta-Keggin derivative, [(CH3)2NH2]5[beta-SiFe2W10O36(OH)2(H2O)Cl].7H2O (1) with non-adjacent substituted sites has been obtained in good yield by reaction of Fe(III) cations with [gamma-SiW10O36]8- in aqueous solution. The use of hydrogen bonding counter-cations produced a disorder-free polyani…
Chitosan is a linear polysaccharide obtained from chitin deacetylation. Several applications of chitosan have been proposed in specialized literature: water treatment, cosmetic, food additives, development of biomaterials, and mainly drug delivery. In the present paper chitosan was hydrophobized by esterification reac…
Mechanical testing after neutron irradiation is a critical research tool for evaluating materials for fusion systems, such as silicon carbide fiber silicon carbide matrix (SiC/SiC) composites. However, single-axis tensile testing, which is required to build a fundamental database, requires large specimens. Therefore m…
The gamma-deprotonation of a samarium(III) bis(trimethylsilyl)amide complex derived from a dimetallated trans-dioxaporphyrinogen has been achieved through stabilisation of the counter cation within the macrocyclic cavity.
Certain commercial aluminum alloys can become electrochemically activated by heat-treatment as a result of enrichment of the trace element Pb at the surface. For a better understanding of the nature of activation, Pb enrichment resulting from annealing for 1-24 h at 300-600°C in air, followed by quenching in water, wa…
We performed ion irradiation experiments on diamond samples at room temperature, probed by in-situ Raman spectroscopy. Different ions are used with energies of 200 or 400 keV. The intensity of diamond Raman band (at 1332 cm−1) decreases exponentially as the ion fluence increases. Results from different ions demonstrat…
A novel DTPA-tris(amide) derivative ligand, DTPA-N,N''-bis[bis(n-butyl)]-N'-methyl-tris(amide)(H2L3) was synthesized. With Gd3+, it forms a positively charged [Gd(L3)]+ complex, whereas with Cu2+ and Zn2+ [ML3], [MHL3]+ and [M2L3]2+ species are formed. The protonation constants of H2L3 and the stability constants of t…
Biomedical polymers that are designed to degrade faster at slightly acidic pH values may potentially be developed for use in drug delivery, pharmaceutical formulation and regenerative medicine. Water-soluble polyacetals derived from two well known pendent functionalised tyrosine-based diphenol monomers were prepared.…
A study was carried out to examine copper immersion deposition on AZ91 magnesium alloy in a hydrofluoric acid-containing bath. The role of fluoride and the effect of bath temperature were investigated. The study was performed by measuring the ac impedance and open-circuit potentials in combination with X-ray photoelec…
Nanoscale grains of crystalline TixSn1-xO2 were directly grown over the whole range of [Ti]/([Ti] + [Sn]) ratio (x = 0.00-1.00) in aqueous solutions at near room temperature.
Abstract This article provides an overview of the identification systems for various grades of wrought stainless steels, namely, the American Iron and Steel Institute numbering system, the Unified Numbering System, and proprietary designations. It elaborates on five major families of stainless steels, as defined by th…
Using two complementary methods: x-ray absorption and crystal field spectroscopies, the Ni sites and their distribution in glass have been determined, in order to rationalise the structural dependence of glass properties. In borate glasses, the structure of the glass related to its composition is responsible for the N…
In 10MW High Temperature Gas-cooled Reactor (HTR-10), the wear of graphite components generates the graphite dust to influence the normal working of the reactor. The graphite dusts come from three parts: core, unload pipe and load pipe. Based on the graphite wear experiments, we here estimated that the graphite genera…
Ni-ceria cermets with 7.5, 11, and 14 vol % of Ni manufactured by a novel method, called net-shape technology, are presented and evaluated.The method is a combination of conventional ceramic sintering and a polymer precursor impregnation technique.Ceria powder with a carbon pore former is sintered, constructing a rigi…
There are several methods of testing porosity and relevant quantities such as pore size, pore size distribution, pore diameter etc. The intra-yarn porosity of polyester staple yarns with different cross-section shapes has been studied in this paper using mercury porosimetry, a technique which is wide-spread in the pap…
This paper presents an advanced finite-element model for analyzing the dynamic behavior of electromechanical devices. The numerical approach includes nonlinear supply circuits, eddy-current and hysteresis effects, and mechanical quantities. The motion of the armature can be handled by means of two alternative approach…
The synthesis of structurally well defined poly(ε-caprolactone) (PCL)–silica nanocomposites was performed following two synthetic routes:( 1) “graft from” anionic ring opening polymerization of CL initiated from the surface of silica nanoparticles that have been previously modified by grafting of hydroxyl groups, and…
We study the transmission properties of a nonlinear periodic structure containing alternating slabs of a nonlinear right-handed material and a linear left-handed material. We find that the transmission associated with the zero-averaged refractive-index gap exhibits a bistable characteristic that is relatively insensit…
The objective of this study was to evaluate the capacity of three clinically useful tissue sources: tricuspid valve leaflet (TVL), carotid artery (CA), and jugular vein (JV), to generate myofibroblasts for potential use in a tissue-engineered cardiac valve replacement. Tissue biopsies of clinically appropriate sizes o…