Materials Literature
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Herein,we report on the synthesis and lithium storage properties of electrospun one-dimensional（1D） CuFe2O4 nanomaterials.1D CuFe2O4nanotubes and nanorods were fabricated by a single spinneret electrospinning method followed by thermal decomposition for removal of polymers from the precursor fibers.The as-prepared CuF…
The flow behavior and dynamic globularization of TC11 titanium alloy during subtransus deformation are investigated through hot compression tests. A constitutive model is established based on physical-based hardening model and phenomenological softening model. And based on the recrystallization mechanisms of globulari…
Anhydrous ytterbium chloride was obtained via solid-phase reaction from Yb2O3 with AlCl3 as a chlori- nation agent. The electrochemical behavior of the chlori- dized Yb2O3 was investigated on W electrodes in LiCl- KCl and LiCl-KCl-AlCl3 melts by cyclic voltammetry and square wave voltammetry. The results showed that t…
The fabrication of molybdovanadophosphoric acids incorporated into SBA-15 mesoporous silicas has been achieved via a one-pot procedure. The as-obtained composite materials were well characterized by XRD, TEM, and nitrogen adsorption-desorption which indicated that the composite materials possessed good mesoporous char…
什么时候在层之间被设置，而材料的 crystallinity 被减少。没有任何看得清的减少，这 nanocatalyst 能也在它的催化活动被恢复并且再使用至少六次。为白酒和酚的 acetylation 的这个新方法有几个关键优点，包括温和、环境地友好的反应条件，以及对优秀收益和灵巧的病情的检查好。
A chemical system for facile and accurate detection of 2,4-dichlorophenol(DCP) via iron(II) phthalocyanine(Fe(II)Pc) catalyzed chromogenic reaction is reported for the fi rst time. In this system, DCP could be oxidized by dioxygen with the catalysis of Fe(II)Pc and then coupled with 4-aminoantipyrine(4-AAP) to generat…
多围的碳 nanotube (MWCNT ) 上的非结晶的碳 nanoparticles (a-CNPs ) 电影，在硅底层上扔了，从 polydiallyldimethylammonium 的甲醇暂停用电极淀积联合被综合修改氯化物的 MWCNT。MWCNT 的低电压的 electrophoretic 免职和 a-CNPs 的高电压的电气化学的免职被执行在 MWCNT 的表面上产出同质地依附的 a-CNPs，并且与对底层的好粘附形成一部合成电影。这种可伸缩的技术能生产 a-CNP/MWCNT 电影的一个大区域。并且地排放调查证明 a-CNP/MWCNT 电影有 3.17 V m1 的刺激电场(在 10 一 cm2 ) 并且 4.6…
为下一代设备的灵活透明电极的发展在碳电子学研究作为主要话题被指定下一五年了。在迄今为止测试的材料， graphene 和 graphene 基于的所有候选人之中， nanocomposites 显示出高效。尽管一些早期的反氧化测试被报导了，估计基于碳的电极的可靠性的在里面深的变老研究以前从来没被执行过。在这个工作，我们在场估计 graphene 电极的变老的机制的造成分裂的方法论，它对另外的 carbonbased 和二维的材料也可扩展。在执行加速的氧化测试以后，我们用尽一切地分析把 nanoscale 和设备水平实验与 Weibull 概率的分析和通道水流模拟相结合的电极的收益，基于 Fowler-Nordheim/Direct…
Freestandingβ-SiC/SiOxCy/Cfreenanocomposite films were synthesized by melt spinning the polycarbosilane(PCS)precursor.Their microstructure were characterized by Fourier transform infrared(FT-IR),Xray diffraction(XRD)and Raman spectroscopy,morphology analysis was investigated by scanning electron microscope(SEM).Resist…
M (x) Al6 (1x ) Si2O13 的绝缘的陶艺做了多铝红柱石经由一起沉淀被综合技术。X 光检查衍射侧面表明这些 nanoparticles 被使结晶很好，多铝红柱石单位房间的卷作为掺杂物离子的离子的半径的一个函数被增加。TEM 图象为纯多铝红柱石样品显示出常规斜方晶的水晶形态学。同时，做的样品展出了更大的粒子尺寸的稍微弄歪的晶体形态学。表示的 DSC thermograms 多铝红柱石的发热的山峰温度与 M3+ 被转移到更低的价值离子插入。光致发光系列为多铝红柱石样品被学习，并且排放系列的紧张被 M3+ 离子类型影响，这被发现。它被发现那， Y3+ 做了完成的多铝红柱石在收音机波浪频率区域(1 MHz ) 的 0.01…
29 旋转原子磁性的回声的 Si 魔术的角度( 29 Si 妈 NMR )， 27 艾尔妈 NMR ，和扫描电子显微镜( SEM )。与增加温度， microcline 粉末转变成亚稳的 KAlSiO 在进一步转变成纯 kalsilite 前的 4 多形体。kalsilite 和亚稳的 KAlSiO 的混合物 当热水的反应在 2 h 以内被执行时， 4 多形体被获得；但是在 2 h 以后， kalsilite 是占优势的产品。KOH 的集中，需要比 4.3 M 大，是影响 kalsilite 的合成的一个重要参数。
We reported a bifunctional material, Cr-salen implanted conjugated microporous polymer(Cr-CMP), which is able to capture excellent CO2amounts and has a remarkable catalytic activity towards the cycloaddition reaction of CO2to epoxides forming cyclic carbonates at mild conditions without additional solvents. This heter…
Highly ordered mesoporous NiMoO4material was successfully synthesized using mesoporous silica KIT-6 as hard template via vacuum nanocasting method. The structure was characterized by means of XRD, TEM, N2adsorption-desorption, Raman and FT-IR. The mesoporous NiMoO4with the coexistence of α-NiMoO4and β-NiMoO4showed wel…
Objective To investigate the cytotoxicity of superparamagnetic iron oxide nanoparticles(SPIONs)modified by chitosan or sodium oleate,so as to provide experimental evidence for future clinical application.Methods The morphology of chitosan-SPIONs or sodium oleate-SPIONs was observed by transmission electron microscope(…
以便模仿热剧降的电镀双阶段(DP ) 钢(wt%) 0.15C0.1Si1.7Mn， DP 钢被不同退火获得时间表。在铁酸盐谷物，马氏体的体积部分，和马氏体的好结构上浸泡温度，时间，和冷却的率的效果被学习。结果证明 DP 钢的收益力量(YS ) 对退火敏感安排，当全部的延伸没在退火上有显著依赖时时间表。增加从 790 ～ 850 浸泡温度吗？？
Anodized composite films containing Si C nanoparticles were synthesized on Ti6Al4 V alloy by anodic oxidation procedure in C4O6H4Na2 electrolyte. Scanning electron microscopy(SEM), energy dispersive spectroscopy(EDS) and X-ray photoelectron spectroscopy(XPS) were employed to characterize the morphology and composition…
The effects of substituent type and position on the proton transfer reaction of 3-hydroxytropolone(3-OHTRN) have been investigated theoretically by using density functional theory at the level of B3LYP/ 6-31+G** method. The influence of solvent on the proton transfer reactions of substituted 3-OHTRN has been examined…
In this paper, we adopted hot-pressing treat- ment to convert the regular reduced graphene oxide (RGO) from chemical exfoliation to the high-quality graphene (HQG), and then the HQG/poly vinylidene fluoride (PVDF) composite films were prepared by spin coating. The microstructural characterizations and property mea- su…
像长带的 FeCo 电影由从内在地各向同性的连续 FeCo 电影的一个传统的平版画过程是有图案的。长带有图案的 FeCo 电影显示出一架强壮的在里面飞机有沿着长带的长度方向的容易的轴的单轴的磁性的 anisotropy。当应用的地分别地在难轴和容易的轴附近时，顽磁比率，切换的地，和 coercivity 的尖依赖显示长带有图案的 FeCo 电影的磁化颠倒机制是协调旋转和领域墙 depinning。长带有图案的 FeCo 电影和计算磁滞现象的试验性的磁滞现象环的一致性与单轴的 anisotropy 模型显示的一架简单在里面飞机循环长带有图案的 FeCo 电影作为单个域表现。墙和强壮的在里面飞机 anisotropy 域使长带有图案的…
A novel fluid dynamics route for scalable and efficient production of graphene and its analogues is demonstrated.Atomic force microscopy and transmission electron microscopy analyses strongly suggest that the bulk layered materials(graphite,BN,MoS2,and WS2)are efficiently exfoliated into individual layers containing m…