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Calorimetric and Raman Study of the Phase Transition in [N(CH3)4]2ZnBr4

J. M. Igartua、I. Ruiz‐Larrea、M. Couzi 等 5 位作者1991-11-01physica status solidi (b)

Abstract Raman scattering and calorimetric measurements are used to study the ferro‐paraelastic phase transition undergone by [N(CH 3 ) 4 ] 2 ZnBr 4 at 287.19 K. The knowledge of its vibrational spectrum, together with the available elastic and thermal expansion data, allow to obtain the specific heat of the phase tra…

Crystal structures of chemical compoundsCrystallography and molecular interactionsSolid-state spectroscopy and crystallography

Effect of Alkalies and of a Reducing Atmosphere on the Corrosion of Refractories by Molten Aluminum

C. Allaire、Pau Desclaux1991-11-01Journal of the American Ceramic Society

The corrosion of aluminosilicate refractories by molten aluminum, such as in melting and holding furnaces, generally leads to the formation of an alumina deposit on the refractory. In the presence of alkalies and under a reducing atmosphere the extent of corrosion is increased. This could be related to the transformat…

Advanced ceramic materials synthesisRecycling and utilization of industrial and municipal waste in materials productionMagnesium Oxide Properties and Applications

THE MORPHOLOGY AND TAXONOMY OF THE PLANKTONIC DIATOMCHAETOCEROS COARCTATUSLAUDER (BACILLARIOPHYCEAE)

David U. Hernández‐Becerril1991-11-01Diatom Research

The diatom Chaetoceros coarctatus has been studied by light (LM) and electron microscopy (SEM, TEM), from preserved plankton samples collected in the Gulf of California and off the Pacific coast of Baja California. Observations include the finding of a number of rimoportulae in a single valve (terminal or intercalary)…

Marine and coastal ecosystemsAlgal biology and biofuel productionDiatoms and Algae Research

Variations in Yarn Properties Caused by a Series of Design Changes in a Friction Spinning Machine

J. P. Rust、P. R. Lord1991-11-01Textile Research Journal

The structure of friction open-end yarns made with a much modified DREF 3 friction spinning unit with replaced suction rolls and equipped with a comber roll assembly from a Platt 881 rotor spinning unit was studied and found to be dissimilar to that of ring spun yarns. Migration theory, as it is known in ring spinning…

Mechanical Behavior of CompositesTextile materials and evaluationsMaterial Properties and Processing

Phase Transitions in an Antiferroelectric Liquid Crystal TFMHPOBC

Tetsuya Fujikawa、Hiroshi Orihara、Yoshihiro Ishibashi 等 10 位作者1991-11-01Japanese Journal of Applied Physics

We studied phase transitions in an antiferroelectric liquid crystal TFMHPOBC (C 8 H 17 O-&benzf;-&benzf;-COO-&benzf;- * CH(CF 3 )C 6 H 13 ) by means of dielectric measurements and microscopic observations. Both a Goldstone mode and a soft mode were observed in the SmC * phase, but only a soft mode in the S…

Liquid Crystal Research AdvancementsNonlinear Optical Materials ResearchMolecular spectroscopy and chirality

High-field magnetization process and spin reorientation in (Nd1−xDyx)2Fe14B single crystals

Dong-Won Lim、Hiroaki Kato、Mitsuhiro Yamada 等 5 位作者1991-11-01Physical review. B, Condensed matter

The high-field magnetization process in the (${\mathrm{Nd}}_{1\mathrm{\ensuremath{-}}\mathit{x}}$${\mathrm{Dy}}_{\mathit{x}}$${)}_{2}$${\mathrm{Fe}}_{14}$B system has been investigated using single crystals with x=0, 0.125, 0.2, 0.33, 0.47, 0.6, and 1. Magnetization measurements were performed using steady magnetic fi…

Magnetic properties of thin filmsMagnetic Properties and ApplicationsMagnetic Properties of Alloys

Polycarbonate‐polystyrene block copolymers and their application as compatibilzing agents in polymer blends

Rishan Jiang、Roderic P. Quirk、James L. White 等 4 位作者1991-11-01Polymer Engineering and Science

Abstract The synthesis of a block copolymer with polystyrene (PS) and polycarbonate (PC) segments is described. It is produced by anionic polymerization of the styrene and endcapping with a hydroxyl group followed by subsequent reaction with phosgene and bisphenol‐A. The polystyrene/polycarbonate block copolymer was u…

Polymer crystallization and propertiesPolymer Nanocomposites and Propertiesbiodegradable polymer synthesis and properties

Precise determination of aluminum content in AlGaAs

K. H. Chang、Chi‐Hung Lee、Jiabin Wu 等 8 位作者1991-11-01Journal of Applied Physics

The Al composition of AlGaAs has been determined by four methods: high-resolution transmission electron microscopy (HRTEM), reflection high-energy electron diffraction (RHEED), photoluminescence (PL), and double-crystal x-ray diffraction (DCXRD). HRTEM is direct and the most accurate method because it does not involve…

Semiconductor materials and devicesElectron and X-Ray Spectroscopy TechniquesSurface and Thin Film Phenomena

Dynamics and relaxation of large Barkhausen discontinuity in amorphous wires

Л. В. Панина、Minoru Mizutani、K. Mohri 等 5 位作者1991-11-01IEEE Transactions on Magnetics

Domain wall processes (domain wall configuration, propagation, and collapse) in magnetostrictive amorphous wires of the composition Fe/sub 77.5/Si/sub 7.5/B/sub 15/ were investigated. The wires were held under tensile stress (up to 1700 MPa in the case of as-quenched). The domain wall length and normal mobility (or da…

Magnetic properties of thin filmsMetallic Glasses and Amorphous AlloysMagnetic Properties and Applications

Large-Scale Extension and Recovery of Plain Woven Fabrics

Rajesh D. Anandjiwala、G. A. V. Leaf1991-11-01Textile Research Journal

This paper describes an attempt at a theoretical study of large-scale tensile defor mation of plain woven fabrics. The basis of the investigation is to use a more realistic approximation of nonlinear yarn bending behavior for both the undeformed fabric state and the stress analysis than has been used by most previous…

Mechanical Behavior of CompositesTextile materials and evaluationsStructural Analysis and Optimization

The effect of a lateral substituent on the mesomorphic properties of 4-cyanophenyl 4-(4-alkyloxybenzoyloxy)benzoates

Yoshihide Masuda、Yoshiaki Sakurai、Hisanori Sugiura 等 6 位作者1991-11-01Liquid Crystals

The thermal properties of 4-cyanophenyl 4-(4-alkyloxybenzoyloxy)benzoates having a lateral substituent have been examined. Commencing with the nonyloxy homologue the hydrogen derivative shows a smectic A phase having a partially bilayered arrangement (SAAd). When the substituents are introduced at position X, the SAd…

Liquid Crystal Research AdvancementsSynthesis and Properties of Aromatic CompoundsPhotochromic and Fluorescence Chemistry

Formation of Condensed Chlorides During Mixed Oxidation–Chlorination of Iron at 1000 K

S. Y. Lee、M. J. McNallan1991-11-01CORROSION

The mixed oxidation-chlorination of iron in gas mixtures of Ar, O2, and Cl2 at 1000 K has been investigated by thermogravimetric analysis and examination of the corrosion products by optical and scanning electron microscopy and X-ray diffraction analysis. Vapor phase transport of iron chlorides influences the rate of…

Thermal and Kinetic Analysis

The role of cysteine 206 in allosteric inhibition of Escherichia coli citrate synthase. Studies by chemical modification, site-directed mutagenesis, and 19F NMR.

Lynda J. Donald、Brian R. Crane、Deborah H. Anderson 等 4 位作者1991-11-01Journal of Biological Chemistry

Escherichia coli citrate synthase is strongly and specifically inhibited by NADH, but this inhibition can be prevented by reacting the enzyme with Ellman's reagent. We have now labeled the single reactive cysteine covalently with monobromobimane and isolated and sequenced the bimane-containing cyanogen bromide peptide…

Protein Structure and DynamicsEnzyme Structure and FunctionBiochemical and Molecular Research

An Impedance Study of a Carbon Fiber/Vinyl Ester Composite

Deepak Kaushik、M. N. Alias、Richard D. Brown1991-11-01CORROSION

The electrochemical behavior of a carbon fiber/vinyl ester composite in 3.5% NaCI solution was investigated. The technique chosen for the study was electrochemical impedance spectroscopy (EIS), which enables time-dependent data to be acquired nondestructively on single samples. The data from the measurement technique…

Fuel Cells and Related MaterialsConducting polymers and applicationsSmart Materials for Construction

Internal stresses and elastic energy in ferroelectric and ferroelastic ceramics: Calculations by the dislocation method

N. A. Pertsev、G. Arlt1991-11-01Ferroelectrics

A method is proposed for calculating the internal stresses in ferroelectric and ferroelastic ceramics which is based on the modelling of the mechanical sources of stress by fictitious dislocations continuously distributed on the grain and twin boundaries. For tetragonal and orthorhombic ceramics with a lamellar twin s…

Ferroelectric and Piezoelectric MaterialsNumerical methods in engineeringAcoustic Wave Resonator Technologies

Clearance of liposomal gadolinium: In vivo decomplexation

Evan C. Unger、Thomas Fritz、Colin Tilcock 等 4 位作者1991-11-01Journal of Magnetic Resonance Imaging

The contrast agents gadolinium-DTPA (diethylenetriaminepentaacetic acid), Gd-DOTA (tetraazacyclododecanetetraacetic acid), and Gd-HP-DO3A (1,4,7-tris[carboxymethyl]-10-[2' hydroxypropyl]-1,4,7,10-tetraazacyclododecane) are used in humans as extracellular contrast agents. Although free Gd+ ion is toxic, the intact Gd3+…

Lanthanide and Transition Metal Complexes

Isotope and impurity effects on the glass transition and crystallization of pressure-amorphized hexagonal and cubic ice

G. P. Johari、Andreas Hallbrucker、Erwin Mayer1991-11-01The Journal of Chemical Physics

Amorphous solid D2O from hexagonal and cubic ices and H2O from (HF, NH3, and NH4F) doped hexagonal ice have been prepared by Whalley’s method, and their thermal behavior has been investigated by differential scanning calorimetry from 103 to 250 K. For a heating rate of 30 K min−1 , the temperature of the onset of the…

Luminescence Properties of Advanced MaterialsMaterial Dynamics and PropertiesGlass properties and applications

Luminescent nitridorhenium(V) complexes

Gregory A. Neyhart、Kevin J. Seward、James Boaz 等 4 位作者1991-11-01Inorganic Chemistry

ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTLuminescent nitridorhenium(V) complexesGregory A. Neyhart, Kevin J. Seward, James Boaz, and B. Patrick SullivanCite this: Inorg. Chem. 1991, 30, 24, 4486–4488Publication Date (Print):November 1, 1991Publication History Published online1 May 2002Published inissue 1 November 1…

Magnetism in coordination complexesLanthanide and Transition Metal ComplexesAtomic and Subatomic Physics Research

Phosphate Mineralogy and Equilibria in Two Kentucky Alfisols Derived from Ordovician Limestones

A. D. Karathanasis1991-11-01Soil Science Society of America Journal

Abstract The phosphate mineral distribution as it relates to in situ soil solution composition of two Alfisols developed from phosphatic Ordovician limestones in the inner Bluegrass Region of Kentucky was investigated. At both sites, microcrystalline apatite appeared to be the primary source of P. Surface weathering u…

Clay minerals and soil interactionsIron oxide chemistry and applicationsPhosphorus and nutrient management