Materials Literature
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A técnica de difração de neutrões é usada neste artigo para estudar amostras ferríticas, revestidas comaços inoxidáveisausteníticos através de soldadura por arco submerso. Este procedimento é frequentemente usado no fabrico de equipamentos de processo para as indústrias química e nuclear, por facilidade de execução e…
There are described the quasi-chemical reactions that take place between radiation defects and impurities in irradiated silicon. It has been experimentally investigated single-crystalline n- and p-type silicon doped, respectively, with phosphorus or boron, irradiated with high-energy electrons or protons and subjected…
In this study, dehydroxylation of alunite was studied. On the basis of thermogravimetric results and sulfur loss, dehydroxylation of alunite occurs from 508 to 577 °C. In this temperature range, temperature and time, as well as their interaction, have the greatest effect on alunite conversion (dehydroxylation) with 99…
The increasing prevalence of antibiotic-resistant bacterial strains has necessitated the synthesis of novel antibacterial agents. It was previously shown that naturally occurring metalloporphyrin hemin possesses dark antibacterial activity against Gram-positive bacteria. To improve hemin antibacterial activity, we syn…
In this study, a novel metal‐free phthalocyanine and three metallophthalocyanines carrying four 2‐[2‐(4‐tert‐butylphenoxy)ethoxy groups on the periphery were prepared by cyclotetramerisation of a dinitrile derivative in the presence of the corresponding divalent metal salts [zinc(ii), cobalt(ii), copper(ii)]. These ne…
Atualmente os aços inoxidáveis martensíticos tem sido utilizados para a fabricação de turbinas hidráulicas, devido principalmente a sua elevada tenacidade. Entretanto, estes aços apresentam algumas restrições com relação à regiões recuperadas por soldagem, principalmente em razão da formação de martensita não revenida…
A técnica de soldagem subaquática molhada com eletrodos revestidos apresenta um crescente potencial de aplicação para reparos submarinos em elementos estruturais de unidades flutuantes de produção de petróleo (profundidade até 20 m). Porém, ela apresenta problemas tais como o maior risco de fissuração a frio e de form…
High strength quenched and tempered (Q&T) steels offer obvious economic benefits originating from their advantageous strength to price and weight ratios. These steels are usually welded using ferritic consumables and for this combination the risk of hydrogen assisted cold cracking (HACC) is high. The use of austenitic…
Os aços inoxidáveis Duplex (AID) aliam uma excelente resistência à corrosão com elevada resistência mecânica devido à fina microestrutura bifásica composta por quantidades similares de ferrita (δ) e austenita (γ). Portanto, estas ligas são utilizados em tubulações e equipamentos industriais onde se requer elevada rela…
O fenômeno das bolhas no processo de soldagem subaquática molhada é de vital influência na qualidade final das soldas. O bom entendimento da formação e colapso das bolhas juntamente com o conhecimento do comportamento dos parâmetros de soldagem no decorrer do processo podem proporcionar melhorias nas práticas utilizad…
New fluorescent-tagged amines have been obtained starting from 4-chloro-7-nitro-2,1,3benzoxadiazole and oligopropylamines containing fragments of N-methylpropylamine close to those found in diatom frustules. Optical properties of new dyes and staining of silica structures in vivo and in vitro are described.
Realizou-se a avaliação de metal de solda com resistência a tração superior à 860MPa, para utilização na soldagem de aço grau R4 da norma IACS W22. Para tanto, foram soldadas juntas multipasse com preaquecimentos realizados à 200 e 250ºC pelo processo eletrodo revestido, utilizando um consumível com 4,0mm de diâmetro…
Abstract The constitutional zone refining model for the internal crystallization of granitic pegmatites stipulates that a highly fluxed and incompatible element‐enriched boundary layer melt evolves at the surface of crystal growth fronts in undercooled granitic melts. It has been argued that silicate‐rich inclusions i…
Electron microscopy (EM) provides access to structural information of macromolecular complexes in the 3-20 Å resolution range. Normal mode analysis has been extensively used with atomic resolution structures and successfully applied to EM structures. The major application of normal modes is the identification of possi…
Microreactors are miniaturized chemical reaction systems, which contain reaction channels with characteristic dimensions in the range of 10-500 µm. One possible application for microreactors is the conversion of ethanol to hydrogen used in fuel cells to generate electricity. In this paper a rigorous isothermal, steady…
Abstract The oxidative modification of Biolignin (BL) has been investigated to make it more suitable as an adsorbent for transition/heavy metals. BL is a by-product of a wheat straw organosolv process for the production of pulp, ethanol, and pentoses (CIMV S.A. pilot plant, Levallois Perret, France). It was subjected…
True colour measurements of wastewater samples, in terms of American Dye Manufacturers' Institute values, were used to evaluate the effectiveness of decolourisation of textile wastewater using spent green tea leaf powder waste. Raw wastewater samples with a true colour of 868 ADMI were used in the batch adsorption exp…
Silicon microwire arrays have attracted considerable attention recently due to the opportunity they present as highly efficient and cost-effective solar cells. In this study, we report on efficient Si microwire array solar cells with areas of 1 cm(2) and Air Mass 1.5 Global conversion efficiencies of up to 10.6%. Thes…
Protein-ligand interactions taking place far away from the active site, during ligand binding or release, may determine molecular specificity and activity. However, obtaining information about these interactions with experimental or computational methods remains difficult. The computational tool presented in this arti…
AIMS: Wool, a recalcitrant waste mainly composed of keratin, constituted a serious problem for the environment and was not effectively valorized. This study reported the optimization of wool-waste biodegradation by a new keratinolytic bacterium Bacillus pumilus A1. The in vitro digestibility and the antioxidant potent…