Materials Literature
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In an attempt to study the specific influence of cross-linking on the α relaxation in polymer networks, a series of model heterocyclic polymer networks (HPN) with well-defined cross-link densities and constant concentration of dipolar units were studied. Model HPN systems were prepared by simultaneous trimerization of…
Self-organized semiconducting structures can be generated by including conjugated chains in block copolymers, it is reported here. Thin films of rod–coil copolymers containing a conjugated and a non-conjugated segment show nanoribbons of the conjugated material (see Figure), indicating that this approach may open the…
We synthesized Pb(Ni 1/3 Nb 2/3 )O 3 (PNN) and performed selected-area electron diffraction (SAD) in order to investigate the structure of the B-site array. In addition to the reflection from the basic cell, the SAD pattern of sintered PNN corresponds to the reciprocal plane normal to the [011] zone axis and showed di…
A novel method of transient eddy current analysis for moving conductors is proposed. In the analysis, different moving coordinate systems are used at each finite element in the conductor, respectively. The velocities of the coordinate systems are determined automatically at each time-step for the purpose of reducing t…
The only Landau-type model for antiferroelectric phase transitions was proposed by Kittel, in which two interpenetrating sublattices with opposite polarizations of equal amplitude were assumed. The theory, however, did not include any mechanism to specify the relative spatial positions of the two sublattices, and ther…
To estimate the stray loss distribution in power transmission systems like transformers, a new 3D eddy current analysis technique has been developed. This technique is based on the Integral Equation Method with Surface Impedance Model and is suitable for calculating eddy currents in a magnetized substance that has a c…
A new multidentate ligand L, 1,2-bis{[3-(2-pyridyl)pyrazol-1-yl]ethoxy}ethane, has been synthesized by linking two 3-(pyridin-2-yl)pyrazoles with a 1,2-bis(ethoxy)ethyl spacer. Coordination of L with zinc(II) and europium(III) centres has led to mononuclear complexes of [Zn(L)](ClO4)2 (1) and [Eu(L)Cl2](ClO4) (2). X-r…
Infrared and Raman spectra (4000-200 cm−1) were recorded for 4-vinylpyridine and vibrational assignments made for fundamental modes on the basis of frequency shifts of the coordinated ligand, of the group vibrational concept and comparison with the assignments for related molecules. the infrared spectra of M(4-vinylpy…
I propose a model of fracture in which the curvature of the crack tip is a relevant dynamical variable and crack advance is governed solely by plastic deformation of the material near the tip. This model is based on a rate-and-state theory of plasticity introduced in earlier papers by Falk, Lobkovsky, and myself. In t…
Abstract Biodegradable lactic acid based poly(ester‐urethanes) (PEU) were polymerized and their structure and rheological properties were characterized. The polymerization process comprised two steps: lactic acid monomer was oligomerized to low molecular weight prepolymer, and this was then linked to high molecular we…
Results are presented for the corrosion process of low carbon steel, under the influence of the combined action of chloride and sulfate ions. The rust composition, the corrosion rates, and the corrosion potential of the rust layers are analyzed. An increase of the relative magnetite content as the corrosion rate incre…
For the evaluation of the dynamic hysteresis loops, a Neural Network (NN) combined with the Fourier Descriptor (FD) technique can be a simple computational instrument alternative to the classical approach. This method is suitable in those cases in which a distorted periodic magnetic field H, or flux density B, excites…
Foil-winding power transformers contain compact sets of flat conductors having a large aspect ratio. Modeling the eddy currents in the individual foils is therefore difficult and requires completely meshed conductors, especially when the influence of the thermal field on the local conductivity is considered. Coupled 2…
Abstract Reduced heptadecavanadate [V17O42]4− has been synthesized from [H3V10O28]3− by the reaction using palladium 1,5-COD complex, and characterized by a single crystal X-ray structure analysis. The structure can be regarded as a fused decavanadate and consists of an arrangement of thirteen edge shared VO6 octahedr…
Some different oxygen content La4Ni3O10+δ (δ=0.02,0.12,−0.22) compounds were prepared in order to study the influence of Ni3+ content on the electronic properties. A metal–metal transition was detected at 140 K for the as-prepared (La4Ni3O10.02) and reduced (La4Ni3O9.78) compounds. From the electrical conductivity, Se…
The effect of a variety of doping additives on the hydration resistance of calcined materials in the MgO–CaO system was investigated. Samples were prepared from lightly calcined flotation magnesite that was mixed with dolomite, as well as from analytically pure CaO and MgO; then, the samples were doped with additives…
The crystallization of Zr41Ti14Cu12Ni10Be23 (Vit 1) melts during constant heating is investigated. (Vit 1) melts are cooled with different rates into the amorphous state and the crystallization temperature upon subsequent heating is studied. In addition, Vit 1 melts are cooled using a constant rate to different temper…
A tank shield model of a transformer which is proposed by the Investigation Committee of IEE of Japan is analyzed. This is a model having the constraint that the maximum eddy current density should be less than a specified value. The automatic 3D mesh generation technique for hexahedral element is investigated for the…
This paper presents a three-dimensional coupled approach for transient simulation of electromagnetic devices. The approach is based on the A-V-A formulation, in which the eddy current field and the electric circuit equations are solved simultaneously. The Newton-Raphson procedure has been used to take the magnetic non…
Polypropylene is increasingly being used for the thermoforming of food packaging. Compared with amorphous materials, such as polystyrene, it is much more difficult to process and within the industry it is generally poorly understood. In the present study the effects of pigments and nucleating agent on the crystallisat…