Materials Literature
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Ferrous tris-chelate compounds based on 2-(2'-pyridyl)benzimidazole (pybzim) have been prepared and characterized for studies of spin equilibria in fluid solution and when anchored to the surface of mesoporous nanocrystalline (anatase) TiO(2) and colloidal ZrO(2) thin films. The solid state structure of Fe(pybzim)(3)(…
We report high-pressure Raman spectra of carbon onions and nanocapsules investigated by diamond anvil cell experiments. The pressure coefficient and elastic behavior of carbon onions and nanocapsules are found to be very similar to those of multiwall carbon nanotubes. Additionally, detectable structure changes, partic…
We show that the generally accepted demagnetizing field corrections are not applicable to the broad class of modern granular magnetic materials, where magnetization reversal occurs via discrete switching of the moments of individual grains, and thus the self-demagnetizing field of a given grain is proportional to the…
Abstract As majority of polyheteroarylenes based on bis(naphthalic anhydrides), are difficult to process due to their infusiblity and insolubility in common organic solvents and solubility only in strong acids, this study is concerned with the synthesis and properties of new, easily processable polyimides and copolyim…
A highly inclined CoO2 plane orientation was realized in CaxCoO2 thin films grown on sapphire single crystal substrates. The inclination angle of the CoO2 plane orientation was controlled by changing the inclination angle of the sapphire(0001) plane with respect to the substrate surface and additionally by introducing…
Chitooligosaccharides (COSs) are the biodegradation products of chitosan that have been demonstrated with neuroaffinity and/or neuroprotective actions. In this study, we investigated the possible benefits of treatment with COSs on nerve regeneration after crush injuries to peripheral nerves. The rabbits with the crush…
Corrosion inhibition efficiency of acid extract of dry Emblica officinalis leaves for mild steel in 1N HCl medium is investigated in the present study. Experimental methods include weight loss, potentiodynamic polarization and impedance studies. The results indicate Emblica officinalis leaves to be a good corrosion in…
The matrix cracking behavior of slurry cast melt‐infiltrated SiC matrix composites consisting of Sylramic‐iBN fibers with a wide variety of fiber architectures were compared. The fiber architectures included 2D woven, braided, 3D orthogonal, and angle interlock architectures. Acoustic emission was used to monitor in‐p…
A series of swallow-shaped tetrathiafulvalene (TTF)-based liquid crystal (LC) molecules (a-6TTF n, where 6 represents the number of carbon atoms in the two tails of a-6TTF n and n is the even number of carbon atoms in the alkyl chains attached to the side of the asymmetric TTF mesogen, n = 6−12) was designed and synth…
Abstract In this work, effects of coolant chemistry, including concentrations of chloride ions and ethylene glycol and addition of various ions, on corrosion of 3003 Al alloy were investigated by electrochemical impedance spectroscopy measurements and scanning electron microscopy characterization. In chloride‐free, et…
We have studied the kinetics of trans to cis isomerization under the illumination of ultraviolet light, in the Langmuir monolayer of mesogenic azobenzene dimer, bis-[5-( 4' -n-dodecyloxy benzoyloxy)-2-( 4''-methylphenylazo)phenyl] adipate, at an air-water interface. We find that the trans to cis isomerization reaction…
We present a method, polarized Raman (PR) spectroscopy combined with atomic force microscopy (AFM), to characterize in situ and nondestructively the structure and the physical properties of individual nanostructures. PR-AFM applied to individual ZnO nanobelts reveals the interplay between growth direction, point defec…
Polarized Raman spectroscopy has been performed to investigate the effects of the electric field on 0.67PbMg1/3Nb2/3O3–0.33PbTiO3 (PMN–33%PT) single crystal. The electric-field-evolution of Raman spectra differed from one microarea to another. In the crossed polarization geometry, the abrupt changes in the intensities…
CaCu 3 Ti 4 O 12 (CCTO) single-phase powder synthesized by the solid-state reaction method was used to investigate the decomposition reaction after different sintering conditions, in which copper (Cu) atoms played a key role. A secondary intergranular liquid phase (Cu-rich, especially CuO-rich), which is related to bo…
An increase in the optical absorption coefficient during illumination [photodarkening (PD)] is known to be described by a stretched exponential function (SEF) 1−exp[−(t/τ)β], where τ and β, respectively, are the effective response time and the dispersion parameter. τ and β deduced experimentally depend on the thicknes…
The fabrications of sphere-like Au nanoparticles (NPs) on sapphire, GaN, and SiO(2) substrates through the irradiation of a few pulses of 266-nm laser onto Au thin films deposited on the substrates are demonstrated. The top-view diameter, contact angle on substrate, surface population density, and surface coverage per…
We report an enhanced transmission through a single circular subwavelength aperture that is incorporated with a split ring resonator (SRR) at the microwave regime. Transmission enhancement factors as high as 530 were observed in the experiments when the SRR was located in front of the aperture in order to efficiently…
We present a combined experimental and theoretical study of molecular methanethiol $({\text{CH}}_{3}\text{SH})$ adsorption on the reconstructed Au(111) surface in the temperature range between 90 and 300 K in UHV. We find that the simplest thiol molecules form two stable self-assembled monolayer (SAM) structures that…
Serpentine carbon nanotubes (CNTs) are successfully synthesized by controlling the landing of ultralong CNTs on a quartz surface. Several experimental parameters are investigated and the growth mechanism is further clarified (see figure). It is demonstrated that the high on/off ratio of single CNTs is maintained when…
Excellent low field magnetoresistance (LFMR) properties could be achieved from the La0.7Sr0.3Mn1+dO3 (LSMO)-manganese oxide polycrystalline composites. While the improvement of LFMR properties in the perovskite maganite-oxide composites is commonly accompanied with a significant increase in their electrical resistivit…