Materials Literature
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Currently, ingenious new analytical and process experimental techniques which are environmentally benign techniques, viz., ultrasound irradiation, have become immensely popular in promoting various reactions. In this work, a novel soluble multi-site phase transfer catalyst (PTC) viz., 1,4-bis-(propylmethyleneammounium…
Variable‐angle spectroscopic ellipsometry is employed for the optical characterization of non‐stoichiometric silicon nitride thin films exhibiting inhomogeneity formed by refractive index and extinction index changes through the film thickness. For all the film samples, the best fit of the experimental data is achieve…
Large scale dynamics within the Michaelis complex mimic of Bacillus stearothermophilus thermophilic lactate dehydrogenase, bsLDH·NADH·oxamate, were studied with site specific resolution by laser-induced temperature jump relaxation spectroscopy with a time resolution of 20 ns. NADH emission and Trp emission from the wi…
The detonation of a radiological dispersion device may result in a situation where individuals inhale radioactive materials and require rapid assessment of internal contamination. The feasibility of using a 2×2-inch sodium-iodide detector to determine the committed effective dose to an individual following acute inhal…
Purpose Lightweight alloys are of major concern, due to their applicability, in transport and industry applications. The purpose of this paper is to perform a comprehensive analysis of time dependent properties of aluminum alloy by nanoindentation technique, through investigation of creep behavior. Additionally, possi…
Core-level and valence band spectra of InxGa1−xN films were measured using hard x-ray photoemission spectroscopy (HX-PES). Fine structure, caused by the coupling of the localized Ga 3d and In 4d with N 2s states, was experimentally observed in the films. Because of the large detection depth of HX-PES (∼20 nm), the spe…
In this paper, we report critical design rules for improving the sensitivity of plasmonic biosensors. We use a scalable, parallel method to fabricate Au plasmonic crystal substrates patterned with an array of pits for real-time sensing. Capture ligands printed selectively in these pits resulted in a strong response to…
The La 2 Ce 2 O 7 powder doped with Sr was synthesized by sol‐gel method in this study and its dense bulk samples were also prepared by pressureless‐sintered at 1600°C for 10 h. Its phase composition, microstructure, and thermophysical property were investigated. Results reveal that pure (La 0.95 Sr 0.05 ) 2 Ce 2 O 6.…
In this study, the release of NO during the combustion of single char particles of spruce bark was investigated. Modeled NO release rates were compared to experimentally determined NO rates from a single particle reactor of quartz glass. The operating conditions were between 1073 and 1323 K with 3–19 vol % O 2 and wit…
A simple and scalable synthetic strategy was developed for the fabrication of one-dimensional SiC nanostructures-nanorods and nanowires. Thin sheets of single-walled carbon nanotubes (SWNTs) were prepared by vacuum filtration and were washed repeatedly with sodium silicate (Na2SiO3) solution. The resulting "glassy buc…
Hydrogen peroxide is a candidate propellant for rocket-propulsion applications with the potential to replace highly toxic propellants currently used. Decomposition of hydrogen peroxide yields a high-temperature oxygen-steam mixture, which can be used as monopropellant or as oxidizer in a bipropellant configuration. Th…
The anisotropic wetting of functional organic molecules on a patterned surface and the development of a photolithography-compatible method to fabricate addressable organic structures is reported. For example, DtCDQA is grown on a SiO2 surface with a Au prepattern, achieving a high resolution cross-over organic structu…
In this paper, we demonstrate self-alignment of microchips on a simple-to-fabricate hybrid template with both water and UV-curing adhesive (EPO-TEK UVO-114). The hybrid template contains receptor sites with solid edges for droplet confinement and large wetting contrast between the receptor sites and the substrate for…
A series of novel mono‐ethylenically unsaturated polycarbosiloxanes macromonomers as compatibilizer materials for soft silicon hydrogels were prepared from the anionic ring‐opening polymerization (AROP) of 2,2,5,5‐tetramethyl‐2,5‐disila‐1‐oxacyclopentane followed by methacrylation. The characterization was performed b…
This study investigated the influence of high pressure processing on the thermal and mechanical properties of low-density polyethylene (LDPE) films used for food packaging. This was carried out by monitoring the thermal and mechanical properties of the materials before and after the pressure treatments. Pouches made f…
New hybrid cryogels comprising natural polymers (free atelocollagen or atelocollagen mixed with a hyaluronic acid derivative) and a synthetic polyester--poly(ε-caprolactone)--were successfully developed by a cryogenic treatment and a subsequent freeze-drying step. Systematic studies on the effect of preparation condit…
Nanoencapsulation of thiamine dilauryl sulfate (TDS), a vitamin B1 derivative, was proved to effectively inhibit the spore germination of Fusarium oxysporum f. sp. raphani (F. oxysporum), as well as mycelial growth. The average diameter of nanoparticles was measured as 136 nm by being encapsulated with an edible encap…
BACKGROUND: Imatinib mesylate is an effective treatment for metastatic gastrointestinal stromal tumor (GIST). However, most patients eventually develop resistance and there are few other treatment options. Immunotherapy using genetically modified or designer T cells (dTc) has gained increased attention for several mal…
As ultra-high-voltage direct current (UHVDC) projects are constructed in China, the electromagnetic environment problem is widely concerned. One of the most important problems is the ion-flow field including the human body under the UHVDC lines. But it has not been analyzed sufficiently. In this paper, the 3-D upstrea…
Hydrogen peroxide is a major component of oxygen metabolism in biological systems that, when present in high concentrations, can lead to oxidative stress in cells. Noninvasive molecular imaging of H(2)O(2) using fluorogenic systems represents an effective way to detect and measure the accumulation of this metabolite.…