Materials Literature
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We investigate the effects of inertia on the hydrodynamics in the microscopic vicinity of moving contact lines. These hydrodynamics control the macroscopic shape and spreading of fluid bodies across solid surfaces. We perform experiments at low capillary number (Ca<0.1) and negligible (10−4) to moderate (Re∼1)…
The photoluminescence (PL) of hydrogenated amorphous carbon nitride films and its behaviors due to ultraviolet (UV) light irradiation and thermal annealing have been investigated. The films were produced using an electron cyclotron resonance plasma with various mixtures of N2 and CH4 gases. The broad PL spectra center…
Abstract Stable carboxylate-functionalized silver nanoparticles (1.4 - 5.7 nm in diameter) which can be separated as pure water-redispersible powder are synthesized by the reduction of silver nitrate with sodium borohydride in the presence of mercaptosuccinic acid (MSA) in methanol. The results show that the particle…
Article Experimental Investigations and Thermodynamic Calculation in the Al-Mg-Sc System was published on November 1, 1999 in the journal International Journal of Materials Research (volume 90, issue 11).
Dissolution kinetics for pits and crevices in aluminum and the effect of dichromate ions on the dissolution kinetics were investigated by using artificial crevice electrodes. The aluminum artificial crevice electrodes were potentiostatically polarized over a range of potential in 0.1 M NaCl solution with and without d…
Polarization tunability and analysis of X-rays is one of the most advancing features of third-generation synchrotron radiation sources. In order to apply such developments to the observation of magnetic effects, a diffractometer for X-ray magnetic absorption and scattering experiments was constructed on BL39XU at SPri…
In process industries coking is an annoying phenomenon, the carbon deposition causes decrease of heat transfer and hinders gas flow. Coking in a process may indicate metal dusting, i.e. the disintegration of metals and alloys in carbonaceous atmospheres under formation of graphite and fine metal particles. The metal p…
The efficiency of imidazole and its derivatives (4-methylimidazole, 4-methyl-5-hydroxymethylimidazole, 1 phenyl-4-methylimidazole, 1-[p-tolyl]-4-methylimidazole) for corrosion inhibition of copper in 0.5 M hydrochloric acid (HCl) was investigated. Corrosion inhibition was studied using impedance spectroscopy and poten…
The hydrolytic degradation under physiological conditions of a series of poly(ester amide)s prepared from 1, n -amino alcohols and aliphatic dicarboxylic acids including succinic, glutaric, and tartaric acids was examined. Degradability was observed to increase with the content in ester groups. Poly(ester amide)s cont…
Elastic and inelastic neutron scattering has been used to study static and dynamic magnetic properties in Ca-doped ${\mathrm{LaMnO}}_{3}$ perovskites in the region of low doping (5% and 8%) and to determine the phase diagram. In addition to the spin-wave branch related to the superexchange coupling between Mn ions (fe…
Oxygen bulk diffusion rates were experimentally determined in a natural ultramylonite sample ( c . 5 μ m grain size; 15–20% biotite, 20% quartz, 60–65% feldspars, and minor Fe‐oxides) from the Gerrish Island shear zone, SE Maine, USA. The diffusion experiments were performed at 250–550 °C and 100 MPa water pressure. O…
Gadolinium-based contrast agents in angiography and interventional radiology.D J Spinosa, A H Matsumoto, K D Hagspiel, J F Angle and G D HartwellAudio Available | Share
Protein aggregation plays an important role in biotechnology and also causes numerous diseases. Human carbonic anhydrase II is a suitable model protein for studying the mechanism of aggregation. We found that a molten globule state of the enzyme formed aggregates. The intermolecular interactions involved in aggregate…
The mechanism of the heat-induced charge transfer observed in Prussian-blue compounds ${\mathrm{K}}_{1\ensuremath{-}2x}{\mathrm{Co}}_{1+x}\mathrm{Fe}(\mathrm{CN}{)}_{6}$ is studied theoretically in connection with photoinduced magnetism. In the case of $x=0,$ our first-principles band calculation confirms that the ban…
Highly oriented perovskite films of PbMg1/3Nb2/3–PbTiO3 and PbSc1/2Nb1/2O3–PbTiO3 with compositions near the morphotropic phase boundary were formed by pulsed laser deposition on La0.5Sr0.5CoO3/MgO (100). The dielectric properties of the films were studied over the frequency range of 100 Hz–1 MHz in the temperature ra…
A spectrum-inversion approach to extract information from MQ-MAS NMR spectra in glasses is presented. This allows the reconstruction of the underlying two-dimensional distribution of the isotropic chemical shift correlated to the quadrupolar interaction. The dependency upon the quadrupolar interaction and the RF field…
Both selenomethionine (SeMet) based multiwavelength anomalous diffraction (MAD) phasing and protein production in baculovirus expression vector systems have greatly enhanced the scope and speed of macromolecular crystallography, but the apparent incompatibility of these two powerful techniques presents an obstacle to…
Optical reflectivity spectra were measured on cleaved surfaces of ${\mathrm{La}}_{0.825}{\mathrm{Sr}}_{0.175}{\mathrm{MnO}}_{3}$ single crystals ${(T}_{\mathrm{C}}=283$ K) over a temperature range 10--295 K. The optical conductivity $\ensuremath{\sigma}(\ensuremath{\omega})$ shows incoherent-to-coherent crossover with…
The fracture behavior of an oxide/oxide ceramic‐matrix composite, alumina/alumina‐silica (Nextel610/AS), was investigated at 23° and 950°C using a single edge notched specimen geometry with clamped ends. Crack growth and damage progression were monitored during the tests using optical microscopy, ultrasonic C‐scans, a…
Stable organic biradical crystals PNNNO, ${\mathrm{F}}_{2}\mathrm{PNNNO},$ and PIMNO of the PNNNO family were synthesized. ${\mathrm{PNNNO}=2\ensuremath{-}[{4}^{\ensuremath{'}}\ensuremath{-}$ $(N\ensuremath{-}\mathit{tert}\ensuremath{-}\mathrm{butyl}\ensuremath{-}N\ensuremath{-}\mathrm{oxyamino})\mathrm{phenyl}]\ensur…