Materials Literature
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The metastable garnet lattice of Gd3Al5O12 is stabilized by doping with smaller Lu3+, which then allows an effective incorporation of larger Eu3+ activators. The [(Gd1−xLux)1−yEuy]3Al5O12 (x = 0.1–0.5, y = 0.01–0.09) garnet solid solutions, calcined from their precursors synthesized via carbonate coprecipitation, exhi…
The spark plasma sintering (SPS) process is known for its rapid densification of metals and ceramics. The mechanism behind this rapid densification has been discussed during the last few decades and is yet uncertain. During our SPS experiments we noticed oscillations in the applied pressure, related to a change in ele…
Microstructure evolution of electron beam physical vapour deposited (EB-PVD) Ni‑23.5Cr‑2.66Co‑1.44Al superalloy sheet during annealing at 600 °C was investigated. The results showed that the as-deposited alloy was composed of only g phase. After annealing at 600 °C, the locations of diffraction peaks were still the sa…
Water-soluble carbon dots (C-dots) were prepared through microwave-assisted pyrolysis of an aqueous solution of dextrin in the presence of sulfuric acid. The C-dots produced showed multicolor luminescence in the entire visible range, without adding any surface-passivating agent. X-ray diffraction and Fourier transform…
Zeolite A was synthesized using the coal ash from Siderópolis/RS - Brazil. The synthesis was based on a standard IZA synthesis using coal ash as the Si and Al source. XRF analysis showed that the coal ash has a Si/Al ratio of 1.52, which is close to the Si/Al ratio required to produce zeolite A (1.0). The synthesized…
The proper healing of bone defects requires a bone graft or bone substitute and synthetic materials have been developed as alternatives to autografts and allografts. Poly(DL-lactic-co-glycolic acid) (PLGA) is a synthetic polymer widely used for bone healing because of its biocompatibility and biodegradability. PLGA sc…
We developed a mathematical analysis method of reflectometry data and used it to characterize the internal structure of TiO2/SiO2/Si and Ti/SiO2/Si stacks. Atomic concentration profiles of all the chemical elements composing the samples were reconstructed from the analysis of the reflectivity curves measured versus th…
The photoluminescence (PL) and PL excitation (PLE) spectra of Si6−zAlzOzN8−z (β-sialon):Eu2+ phosphors with small z values (z=0.025–0.24) were studied at room temperature and 6 K. The PL and PLE spectra exhibit fine structure with the PL lines being as sharp as 45–55 nm even at room temperature; this fine structure wa…
This paper aimed to study the removal of zinc using bentonite clay from the Northeastern Brazil, as an adsorbent. A study of the clay subjected to thermal and chemical treatment was performed in order to evaluate the optimization of the adsorption capacity of this material. For the evaluation of the kinetic equilibriu…
In order to perform the numerical simulations of forging response and establish the processing parameters for as-extruded 7075 aluminum alloy, the compressive deformation behavior of as-extruded 7075 aluminum alloy were investigated at the temperatures of 573 K, 623 K, 673 K and 723 K and the strain rates of 0.01 s-1,…
Rheological and micro-Raman time-series characterizations were used to investigate the chemical evolutionary changes of silica sol–gel mixtures for electrospinning fibers to immobilize an enzyme (tyrosinase). Results of dynamic rheological measurements agreed with the expected structural transitions associated with re…
The aim of this study was to obtain and evaluate the electrical, thermal and mechanical properties of iron oxide-filled castor oil polyurethane (PU/Fe2O3). The iron oxide used in this study was a residue derived from the steel pickling process of a Brazilian steel rolling industry. Polymeric composites with different…
This paper reports the effects of annealing and age hardening heat treatments on the microstructural morphology and mechanical properties of 7075 Al alloy. The material was cast in the form of round cylindrical rods inside green sand mould from where some samples were rapidly cooled by early knockout and others gradua…
Nanoporous silica cryogels with a high specific surface area of 1095 m2 g−1 were fabricated using tert-butyl alcohol as a reaction solvent, via a cost-effective sol–gel process followed by vacuum freeze drying. The total time of cryogel production was reduced markedly to one day. The molar ratio of solvent/precursor,…
In this work two very simple apparatuses, namely the ball crater (or ball-on-plate) and the linear reciprocating (or pin-on-plate) tests, were used in order to investigate the wear mechanisms of TPH Spectrum® and Resilab Master® dental composite resins. Loads in the range of 100 g to 1 kg and a total number of up to 2…
We report TiO2 patterns obtained by a soft-lithographic technique called 'micromolding in capillaries' using sol–gel and dispersion solutions. A comparison between patterning with a sol–gel and dispersion solutions has been performed. The patterns obtained from sol–gel solutions showed good adhesion to the substrate a…
NiFe2O4@BaTiO3 multiferroic composite particles were produced by a simple hydrothermal method in two steps: preparing NiFe2O4 nanoparticles and then synthesizing core-shell nanocomposites. Multiferroic composite ceramics were sintered from these powders. X-ray diffraction, Raman scattering and energy dispersive x-ray…
A detailed study is given on the synthesis of a hierarchical porous carbon, possessing both meso- and macropores, using a mesophase pitch (MP) as the carbon precursor. This carbon material is prepared by the nanocasting approach involving the replication of a porous silica monolith (hard templating). While this carbon…
In this article we review the fundamental properties and applications of sidewall GaAs tunnel junctions. Heavily impurity-doped GaAs epitaxial layers were prepared using molecular layer epitaxy (MLE), in which intermittent injections of precursors in ultrahigh vacuum were applied, and sidewall tunnel junctions were fa…
Gelatins were crosslinked with organic acids and treated with alkali to impart to them endothelialization and anti-thrombogenic properties. These matrices were characterized by biochemical and physicochemical techniques. The amounts of residual amino groups in the matrices decreased with increasing crosslinker concent…