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Synthesis of Glass‐like Cordierite from Metal Alkoxides and Characterization by 27 Al and 29 Si MASNMR

Ulagaraj Selvaraj、Sridhar Komarneni、Rustum Roy1990-12-01Journal of the American Ceramic Society

A sol‐gel process for the preparation of glass‐like cordierite and ceramic oxide powder is described. Metal alkoxide precursors were dissolved in 2‐methoxyethanol and the metal cations were complexed using 2,4‐pentanedione to overcome different hydrolysis rates of metal alkoxides which lead to microscopic inhomogeneit…

Glass properties and applicationsAdvanced NMR Techniques and ApplicationsX-ray Diffraction in Crystallography

Phase behavior of ternary polymer blends composed of three miscible binaries

G. R. Brannock、D. R. Paul1990-12-01Macromolecules

ADVERTISEMENT RETURN TO ISSUEPREVArticleNEXTPhase behavior of ternary polymer blends composed of three miscible binariesG. R. Brannock and D. R. PaulCite this: Macromolecules 1990, 23, 25, 5240–5250Publication Date (Print):December 1, 1990Publication History Published online1 May 2002Published inissue 1 December 1990h…

Polymer crystallization and propertiesCatalysis for Biomass ConversionBlock Copolymer Self-Assembly

Refolding and aggregation of bovine carbonic anhydrase B: quasi-elastic light scattering analysis

Jeffrey L. Cleland、Daniel I. C. Wang1990-12-01Biochemistry

Bovine carbonic anhydrase B (CAB) is chosen as the model protein to study the phenomenon of protein aggregation, which often occurs during the refolding process. Refolding of CAB from 5 M GuHCl has been observed by quasi-elastic light scattering (QLS), which confirms the formation of a molten globular protein structur…

Enzyme Structure and FunctionPolyamine Metabolism and ApplicationsEnzyme function and inhibition

Monitoring Cable Systems

R. Samm、Fernando de Cuadra García、T.J. Rodenbaugh 等 4 位作者1990-12-01IEEE Power Engineering Review

The existing underground transmission system in the United States is worth about $5 billion. To optimize the return on that investment and on further investment in the growing system, EPRI has sponsored research to develop periodic and continuous diagnostic procedures and methodologies for evaluating underground cable…

High voltage insulation and dielectric phenomenaLightning and Electromagnetic PhenomenaThermal Analysis in Power Transmission

Dependence of electrical conductivity and activation energy of lithiumzinc ferrites on sintering temperature and porosity

D. Ravinder、T. Seshagiri Rao、V. N. Muley 等 4 位作者1990-12-01Crystal Research and Technology

Abstract The electrical conductivity (σ) and thermoelectric power ( Q ) of polycrystalline lithiumzinc ferrites sintered at 1200 and 1300 °C was investigated as a function of temperature. The porosity and activation energy were calculated. It was found that the electrical conductivity is progressively increasing with…

Advancements in Battery MaterialsMagnetic Properties and Synthesis of FerritesElectromagnetic wave absorption materials

Moisture absorption by PVC plastisol components

Richard A. Marshall1990-12-01Journal of Vinyl Technology

Abstract Moisture can be absorbed from the air by PVC plastisols and by the fused product. Water in plastisols can contribute to defects in films, sheet goods and foam products, usually in the form of depressions or craters. Water absorbed by thermoformable foam PVC sheets can result in defects in the molded product,…

Material Properties and ProcessingPolymer Science and PVC

A microstructure based magnetization reversal model in sintered Fe-Nd-B magnets. II. Effect of post sintering treatments

R. Ramesh1990-12-01Journal of Applied Physics

The effect of post sintering heat treatments on the intrinsic coercivity of Fe-Nd-B magnets is studied. It is shown that the large anisotropy in thermal expansion coefficients in the a and c directions of the tetragonal unit cell as well as the anisotropy in thermal expansion properties between the matrix and the grai…

Magnetic properties of thin filmsMagnetic Properties and ApplicationsMagnetic Properties of Alloys

Zur Kenntnis von Unordnungsphänomenen bei Oxiden mit dem „Schmetterlingsmotiv” Über Rb2K4[O2CoOCoO2]

J. Birx、R. Hoppe1990-12-01Zeitschrift für anorganische und allgemeine Chemie

Abstract Rb 2 K 4 Co 2 O 5 wurde erstmals durch Erhitzen inniger Gemenge der binären Oxide in Form von dunkelroten Einkristallen und Pulver erhalten (vor Verreiben Rb:K:Co = 1,2:3,2:1; Ni‐Zylinder, 570°C, 20d). Die Strukturaufklärung [Vierkreisdiffraktometerdaten; PW 1100; AgK ‐Strahlung; 401 von 607 I 0 (hkl); R = 9,…

Crystal Structures and PropertiesSolid-state spectroscopy and crystallographyInorganic Chemistry and Materials

Overlooked trigonal symmetry in structures reported with monoclinic centred Bravais lattices; trigonal description of Li8Pb3, PtTe, Pt3Te4, Pt2Te3, LiFe6Ge4, LiFe6Ge5, CaGa6Te10 and La3.266Mn1.1S6

K. Cenzual、Louise Gelato、Marinella Penzo 等 4 位作者1990-12-01Zeitschrift für Kristallographie - Crystalline Materials

Article Overlooked trigonal symmetry in structures reported with monoclinic centred Bravais lattices; trigonal description of Li8Pb3, PtTe, Pt3Te4, Pt2Te3, LiFe6Ge4, LiFe6Ge5, CaGa6Te10 and La3.266Mn1.1S6 was published on December 1, 1990 in the journal Zeitschrift für Kristallographie - Crystalline Materials (volume…

Crystal Structures and PropertiesSolid-state spectroscopy and crystallographyX-ray Diffraction in Crystallography

PVC/plasticizer compatibility: Evaluation and its relation to processing

Luis Ramos‐Devalle、M. Gilbert1990-12-01Journal of Vinyl Technology

Abstract The compatibility of suspension poly(vinylchloride) [PVC] with twelve different plasticizers was determined using calculated compatibility predictors, as well as actual measurements of compatibility. Solubility parameters were capable of classifying plasticizers of a given family in terms of their compatibili…

Polymer crystallization and propertiesAdvanced Polymer Synthesis and CharacterizationPolymer Science and PVC

Preparation and fundamental physical properties of Sn2SbS2I3 and Pb2SbS2I3 compounds

Володимир Староста、J. C. Kroutil、Ludvı́k Beneš1990-12-01Crystal Research and Technology

Abstract The oriented ingots of isostructural compounds Sn 2 SbS 2 I 3 and Pb 2 SbS 2 I 3 were prepared using a modified Bridgman method. The lattice parameters of the prepared orthorhombic compounds have been determined by a X‐ray powder diffraction analysis. From the spectral response of the photoconductivity the fo…

Crystal Structures and PropertiesNuclear materials and radiation effectsX-ray Diffraction in Crystallography

Photoconductive switching in diamond under high bias field

S. T. Feng、Paul T. P. Ho、J. Goldhar1990-12-01IEEE Transactions on Electron Devices

The limits of high-power, high-repetition-rate operation of photoconductive switches utilizing diamond are explored. To evaluate diamond as a photoconductor for high-power switching applications, the following experiments were performed: (1) measurement of switch resistance as a function of the bias electric field; (2…

Diamond and Carbon-based Materials ResearchLaser Material Processing TechniquesAdvanced Surface Polishing Techniques

Release of Iodine and Noble Gas Fission Products from Defected Fuel Elements during Reactor Shutdown and Start-Up

Brent J. Lewis、R.D. MacDonald、Hugues W. Bonin1990-12-01Nuclear Technology

Data from a single defected fuel element operating in-reactor are used to develop a physically based model for describing the increased release of iodine and noble gas fission products to the primary coolant following a reactor shutdown and start-up. Iodines are only released on reactor shutdown, whereas both species…

Nuclear reactor physics and engineeringRadioactive element chemistry and processingNuclear Materials and Properties

A Fragmentation Model for Cylindrical Warheads

John Pearson1990-12-01Defense Technical Information Center (DTIC)

This report presents a descriptive model for the expansion and fragmentation behavior for the case of a single-point, end-initiated cylindrical warhead. This model divides the overall behavioral process of the warhead case into four distinct zones of behavior which occur between initial case motion and fragment impact…

High-Velocity Impact and Material BehaviorStructural Response to Dynamic Loads

Apophyllite group: effects of chemical substitutions on dehydration behaviour, recrystallization products and cell parameters

Giselle F. Marriner、J. Tarney、J. I. Langford1990-12-01Mineralogical Magazine

Abstract The effects of (OH)/F substitutions on thermally induced reactions in the apophyllite group have been investigated using TGA and DTA methods, supplemented by X-ray diffraction, infra-red and other techniques to identify the products of reaction. The samples studied cover the range between fluorapophyllite and…

Glass properties and applicationsBuilding materials and conservationClay minerals and soil interactions

Network formation and properties: Rate theory description of effects of ring formation on elastic shear modulus of RA2 + RB3 networks

H. Rolfes、R. F. T. Stepto1990-12-01Makromolekulare Chemie Macromolecular Symposia

Abstract The rate theory of RA 2 +RB 3 polymerization has been developed to enable the concentrations of the smallest inelastic loops and the resulting reductions in elastic shear modulus at complete reaction to be evaluated. Reduction in modulus is expressed as M c /M° c , the effective molar mass of chains between e…

Polymer Nanocomposites and PropertiesConducting polymers and applicationsPolymer composites and self-healing

Native Oxide Growth on Silicon Surface in Ultrapure Water and Hydrogen Peroxide

Mizuho Morita、Tadahiro Ohmi、Eiji HASEGAWA 等 4 位作者1990-12-01Japanese Journal of Applied Physics

The effects of n-type dopant (P, As) concentration in silicon (100), temperature, and oxidizing species on native oxide growth in liquid water are described. The oxide growth on phosphorus (P)- and arsenic (As)-doped n + -Si surfaces (10 20 cm -3 ) in ultrapure water exhibits saturation of oxide thickness, suggesting…

Semiconductor materials and devicesSilicon Nanostructures and PhotoluminescenceIon-surface interactions and analysis

Surface studies on scandate cathodes and synthesized scandates

Gary G. Lesny、R. Forman1990-12-01IEEE Transactions on Electron Devices

Auger, ESCA, electron emission, evaporation, and desorption measurements were made on three different types of scandate surfaces. They are: (a) an impregnated top layer scandate cathode, (b) an unimpregnated top layer scandate cathode with a deposited barium or barium oxide adsorbate surface layer, and (c) a synthesiz…

Advancements in Battery MaterialsCatalytic Processes in Materials ScienceSemiconductor materials and devices

Structure-activity relationship of antiestrogens. Phenolic analogs of 2,3-diaryl-2H-1-benzopyrans

Arun P. Sharma、Ayesha Saeed、S. Durani 等 4 位作者1990-12-01Journal of Medicinal Chemistry

Phenolic analogues of 2-[4-(2-piperidinoethoxy)phenyl]-3-phenyl-2H-1-benzopyran (1), a novel antiestrogen, were synthesized and evaluated for their structure-activity relationship. Incorporation of OH at position 7 was found to improve receptor affinity of the benzopyran while having no effect on its action as an anta…

Estrogen and related hormone effectsPhotochromic and Fluorescence ChemistrySynthesis of Organic Compounds

Tetrahedrite and tennantite; evaluation of thermodynamic data and phase equilibria

Robert R. Seal、Eric J. Essene、William C. Kelly1990-12-01OpenAlex

Tetrahedrite and tennantite are extremely common in a variety of ore deposits, but the genetic information they record is difficult to decipher because of the limited understanding of their phase relations in multicomponent systems. Most natural compositions can be described by the general formula (Cu,Ag)1e@e,Zn,Cu)2(…

Metallurgical Processes and ThermodynamicsMetallurgical and Alloy ProcessesRailway Systems and Materials Science