Materials Literature
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The corona pattern from porcelain insulator strings on high voltage (HV) transmission lines has been investigated for inspecting faulty insulators on-line. Corona patterns from HV conductive line, metal accessory, and discharge patterns from bad connection, power stations, have also been studied for background pulse n…
MgO is an important inorganic material, which can be used in many aspects, such as catalyst, toxic-waste remediation agent, adsorbent, and others. In order to make use of MgO, nano-MgO was prepared by ultrasonic method using Mg (CH3COO)2.2H2O as precursor, NaOH aqueous solution as precipitant in this paper. Effect fac…
Orthorhombic HoMnO3 films with well-aligned crystallographic orientations were deposited on LaAlO3(110) single crystal substrates by using pulsed laser deposition. The nearly perfect b-axis-oriented films provide the opportunity of investigating the orientation-dependent physical property of this material. The tempera…
Abstract A new type of polymeric hybrid coating is created by layer‐by‐layer deposition of polyelectrolyte multilayers (PEM) onto nano‐patterned polymer brushes (NPB). The PEM is a hydrogen‐bonded multilayer consisting of poly(acrylic acid) and poly(acrylamide) and the NPB is derived from a surface reactive rod‐coil b…
Abstract In the present study, an icosahedral single phase bulk quasicrystalline material based on Al 62 Cu 25.5 Fe 12.5 has been synthesised by a spray forming route. Microstructural characterization showed an average grain size of 10 μm. The oversprayed fine powder showed the presence of β - and λ -phases, whereas,…
Abstract A simple 5‐chloro‐7‐iodo‐8‐quinolinolato‐manganese(III) complex with the feature of pH‐regulated molecular switches was conveniently synthesized and found to be a novel and highly efficient catalyst for the epoxidation of olefins with aqueous hydrogen peroxide in water‐acetone media containing ammonium acetat…
A method is proposed to modulate phase using variant square holes in a metallic film based on a fundamental mode approximation model. Phase retardation through square holes in a subwavelength scale in a thin metal film has been analyzed and calculated. Based on the model, a structured lens with a numerical aperture of…
Abstract A water‐soluble chitosan derivative namely, N ‐(2‐hydroxy) propyl‐3‐trimethylammonium chitosan chloride (HTCC) was synthesized by the reaction of chitosan with glycidyltrimethyl ammonium chloride in a neutral aqueous condition and solution blended with polyacrylonitrile (PAN) in an organic solvent. Polymeric…
Monitoring the kinetics of hydrolysis and condensation of γ-glycidoxypropyltrimethoxy-silane (γ-GPS) was carried out by NMR spectroscopy (29Si–, 13C–, and 1H–). The course of these reactions was followed in 2 wt% aqueous dilution conditions (26% D2O/74% H2O), pH 5.4, and temperatures of 26, 50, and 70°C. At ambient te…
Abstract The present work provides a critical review of polymer crystallization studies using SALS; experimental methods, analysis techniques, observations and their relations with respect to other techniques are discussed. Furthermore, the fact that nucleation might be accompanied by large scale density fluctuations…
We herein report an anomalous thermal hysteresis in dielectric permittivity in CaCu3Ti4O12. The anomalous behavior was well explained in terms of the low-temperature Maxwell–Wagner relaxation induced by frozen carriers. A multirelaxation mechanism, i.e., the coupling of the dipole relaxation to the frozen carrier-indu…
The stress evolution in nanocrystalline diamond (NCD) films deposited at different temperatures (from 800to400°C) was investigated. Results showed that the intrinsic stress gradually changed from tensile to compressive with decreasing deposition temperature. Most importantly, the intrinsic stress can be tailored to ze…
We studied photoluminescence (PL) and energy transfer dynamics in CdSe nanocrystal (NC) assembled monolayers on Au surfaces. The close-packed CdSe NC monolayers were fabricated using the Langmuir–Blodgett method on spin-coated inert polymer films on rough-surface Au substrates. The PL intensity and PL decay time were…
The influence of the A-site ionic radii $(⟨{r}_{\mathrm{A}}⟩)$ on the magnetic structure has been investigated in ${\mathrm{La}}_{0.5}{\mathrm{Ca}}_{0.5\ensuremath{-}x}{\mathrm{Sr}}_{x}\mathrm{Mn}{\mathrm{O}}_{3}$ compounds $(0\ensuremath{\leqslant}x\ensuremath{\leqslant}0.5)$ using neutron diffraction, magnetization,…
The fabrication of nanoporous sputtered CaCu3Ti4O12 thin films with high gas sensitivity is reported in this work. The porous microstructure and the nanocrystalline nature of the material promoted the diffusion of the atmosphere into the film, shortening the response time of the samples. Behaving as p-type semiconduct…
Abstract Raman spectroscopy combined with infrared spectroscopy has been used to study the minerals, nullaginite and zaratite. Raman bands are observed at 3650, 3556 and 3309 cm −1 for nullaginite and 3609, 3516 and 3336 cm −1 for zaratite. By using a Libowitzky‐type empirical function, estimation of the hydrogen‐bond…
2,6-Di-O-methylcellulose was prepared from natural and synthetic celluloses. Natural cellulose was converted to 2,6-di-O-thexyldimethylsilylcellulose, then to 3-mono-O-allyl-2,6-di-O-methylcellulose, and finally into 2,6-di-O-methylcellulose. Alternatively, 2,6 di-O-methylcellulose was synthesized from the synthetic c…
Abstract Mesostructured forms of silica (denoted MSU‐J) and aminopropyl‐functionalized silica (denoted AP‐MSU‐J) with wormhole framework structures are effective reinforcing agents for a rubbery epoxy polymer. At loadings of 2.0–10 wt %, MSU‐J silica with an average framework pore size of 14 nm (65 °C assembly tempera…
Surface finish has a vital influence on most functional properties of a component like fatigue life, wear resistance, corrosion resistance, etc. This has given birth to processes such as lapping, honing, burnishing, etc. Burnishing is a fine finishing operation involving the cold working plastic deformation of surface…
First- and second-generation dendrimers with an isocyanide group as the focal functional point (CN-G(n); n: 1,2) and their corresponding organometallic complexes [MCl(CN-G(n))] (M: Au, Cu), [{CuCl(CN-G(n))2}2], and trans-[MI2(CN-G(n))2] (M: Pd, Pt) have been synthesized. The free ligands and the first-generation compl…