Materials Literature
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Abstract The synthesis of poly[(oligoethylene glycol) methyl ether acrylate] [poly(OEGA)] brushes was achieved via reversible addition‐fragmentation chain transfer (RAFT) polymerization and used to selectively immobilize streptavidin proteins. Initially, gold surfaces were modified with a trithiocarbonate‐based RAFT c…
Scale deposition is one of the most important and serious problems that limits and sometimes blocks oil and gas production by plugging the oil producing formation matrix or fractures and perforated intervals. One of the most insoluble substances formed from formation water (brine) and one that is very difficult to rem…
The product yield of the electron-impact dissociation of methane has been studied with a combination of three theoretical methods: R-matrix theory to determine the electronically inelastic collisional excitation cross sections, high-level electronic structure methods to determine excited states energies and derivative…
Abstract The contemporary status of experimental as well as theoretical advances within the special view of structural phase transitions is reviewed. A brief outline of phase transitions and its classification is presented first. High-pressure experimental techniques developed for studying the structural phase transit…
Raman shifts of crystalline materials can reliably be evaluated at the ab initio level, provided that suitable Hamiltonians, like the hybrid Hartree–Fock/density functional theory ones, are employed in the calculation. The Raman shifts of jadeite (NaAlSi 2 O 6 ) were obtained by using the WC1LYP hybrid Hamiltonian, an…
We grew graphene by thermal decomposition of B(4)C and investigated its features by high-resolution transmission electron microscope observations. At temperatures higher than 1600 °C in a vacuum, B(4)C decomposes and graphene forms epitaxially on its surface. The number and the morphology of the graphene layers depend…
Star and hyperbranched polyacrylamides (s‐PAMs and b‐PAMs) were synthesized via semibatch RAFT copolymerization of acrylamide (AM) and N,N′‐methylenebisacrylamide (BisAM) using four monomer feeding policies. The BisAM to chain transfer agent (CTA) ratios from 1 to 40 at a constant [AM] 0 /[CTA] 0 of 600 were investiga…
Boehmite (BM) nanoplatelets were adopted to compound with fully biobased poly(propylene sebacate) (PPSe) to form the shape memory composites. The PPSe/BM composites kept excellent shape memory properties as previously reported PPSe. Compared to neat PPSe, the composites possess much higher mechanical properties above…
This paper introduces an indirect intelligent sliding mode controller (IISMC) for shape memory alloy (SMA) actuators, specifically a flexible beam deflected by a single offset SMA tendon. The controller manipulates applied voltage, which alters SMA tendon temperature to track reference bending angles. A hysteretic rec…
The spectroscopic properties of BaGd2-xO4:Eux (x = 0.0 - 0.1) phosphors were investigated. The phosphors were synthesized by conventional solid state reaction method. The samples were characterized by powder-XRD and energy dispersive spectroscopy (EDS) techniques. The photoluminescence (PL) and thermally stimulated lu…
Abstract This study elucidates the influence of the atom transfer radical polymerization initiator structure, monolayer versus disordered multilayer, on the growth kinetics and the structural transition of poly(methyl methacrylate) (PMMA) brush layers. The multilayer initiator film, prepared by acylation of the electr…
A series of quasi-one-dimensional molecular conductors (DMEDO-TTF)(2)XF(6) (X = P, As, and Sb), where DMEDO-TTF is dimethyl(ethylenedioxy)tetrathiafulvalene, undergo characteristic structural transitions in the range of 130-195 K for the PF(6) salt and 222-242 K for the AsF(6) salt. The dramatic structural transition…
DTPA chelates of various diamagnetic and paramagnetic lanthanide(III) metal ions, as well as the chemically similar DTPA chelate of Y(3+), were studied in aqueous solution by variable temperature (17)O NMR with the aim of characterizing their internal dynamics. As a consequence of poor chemical shift dispersion and fa…
A hydrodynamic continuum theory (HCT) of thermally stimulated capillary waves describing surface fluctuations of linear polystyrene melts is found to describe surface fluctuations of sufficiently thick films of unentangled cyclic polystyrene. However, for cyclic polystyrene (CPS) films thinner than 10 R g, the surface…
Abstract The solid — liquid phase equilibria for binary mixture of citric acid with tartaric acid were measured using differential scanning calorimetry. The phase diagram showed the existence a simple eutectic behavior. The thermal properties of this system as heat of mixing, entropy of fusion and excess thermodynamic…
A group of Stellite alloys are studied in consideration of temperature effects on their hardness and wear resistance. The hardness test is conducted on a micro-hardness tester with a hot stage equipped that allows heating the specimen up to 650°C. The wear resistance of each alloy is evaluated using a pin-on-disc trib…
Two-component gels formed from pseudoenantiomeric ethynylhelicene oligomers in toluene exhibited two different properties depending on difference in numbers of helicenes in the two components. The combinations (M)-5/(P)-4, (M)-6/(P)-4, and (M)-7/(P)-4, which contained oligomers with comparable numbers of helicenes, fo…
Hydrothermal synthesis and electrodeposition are low-temperature and cost-effective growth techniques of high quality nanostructured active materials for opto-electronic devices. Here we report a hydrothermal seed layer-free and rapid synthesis (15 min) of epitaxial nanorod arrays of ZnO on p -GaN(0 0 0 1). The effect…
Electrochemical Stability of Metal Electrodes for Reversible Magnesium Deposition/Dissolution in Tetrahydrofuran Dissolving Ethylmagnesium Chloride, Yagi, Shunsuke, Tanaka, Akira, Ichitsubo, Tetsu, Matsubara, Eiichiro
Si 3 N 4 fillers were added to polyethersulfone (PES) using the solution mixing and ball-mill mixing methods to increase the thermal conductivity. 3-Aminpropyltriethoxysilane was used as a coupling agent for the surface modification of the Si 3 N 4 particles. The morphology, thermal stability, mechanical properties, a…