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A model for a solvent-free synthetic organic research laboratory: click-mechanosynthesis and structural characterization of thioureas without bulk solvents

Vjekoslav Štrukil、Marina Diana Igrc、L. Fábián 等 10 位作者2012-01-01Green Chemistry

The mechanochemical click coupling of isothiocyanates and amines has been used as a model reaction to demonstrate that the concept of a solvent-free research laboratory, which eliminates the use of bulk solvents for either chemical synthesis or structural characterization, is applicable to the synthesis of small organ…

Crystallography and molecular interactionsAdvanced NMR Techniques and ApplicationsX-ray Diffraction in Crystallography

Large enhancement of magnetostriction due to compaction hydrostatic pressure and magnetic annealing in CoFe2O4

Muhammad Atif、Reiko Sato-Turtelli、M. Kriegisch 等 6 位作者2012-01-01Journal of Applied Physics

Polycrystalline CoFe2O4 was produced by a ceramic method. The heat-treated powder was pressed, varying the hydrostatic pressure between 87 and 278 MPa, and was heat-treated again at 1350 °C for 24 h. All magnetic parameters showed a clear dependence on this hydrostatic pressure. The saturation magnetization showed a m…

Magnetic properties of thin filmsMagnetic Properties and Synthesis of FerritesMagnetic Properties and Applications

Additives stabilize calcium sulfate hemihydrate (bassanite) in solution

Yunwei Wang、Fiona C. Meldrum2012-01-01Journal of Materials Chemistry

Recent work on the precipitation of the mineral gypsum (calcium sulfate dihydrate) has shown that contrary to long-standing opinion, this phase can precipitate from solution at room temperature via a bassanite (calcium sulfate hemihydrate, or plaster of Paris) intermediate phase. An amorphous calcium sulfate (ACS) pha…

Calcium Carbonate Crystallization and InhibitionCO2 Sequestration and Geologic InteractionsMicrobial Applications in Construction Materials

Microemulsion-mediated hydrothermal synthesis of ZnSe and Fe-doped ZnSe quantum dots with different luminescence characteristics

Lin Yang、Jianguo Zhu、Dingquan Xiao2012-01-01RSC Advances

A microemulsion-mediated hydrothermal method has been demonstrated for synthesizing ZnSe and Fe-doped ZnSe quantum dots (QDs). The properties of ZnSe QDs can be controlled by using the surfactants of polyoxyethylene lauryl ether and Triton X-100. The resulting QDs were found to be in a zinc blende crystal structure, w…

Advanced Photocatalysis TechniquesQuantum Dots Synthesis And PropertiesChalcogenide Semiconductor Thin Films

A Review on Detonation Gun Sprayed Coatings

Lakhwinder Pal Singh、Vikas Chawla、Jasmaninder Singh Grewal2012-01-01Journal of Minerals and Materials Characterization and Engineering

Materials are precious resources. Different methods are employed to protect the material from degradation. Thermal spraying is one of the most effective method to protect the material from wear, high temperature corrosion, stresses and erosion, thus increasing the life of material in use. Detonation gun spraying is on…

Diamond and Carbon-based Materials ResearchCombustion and Detonation ProcessesTribology and Wear Analysis

Engineering of lipid-coated PLGA nanoparticles with a tunable payload of diagnostically active nanocrystals for medical imaging

Aneta J. Mieszawska、Anita Gianella、David P. Cormode 等 9 位作者2012-01-01Chemical Communications

Polylactic-co-glycolic acid (PLGA) based nanoparticles are biocompatible and biodegradable and therefore have been extensively investigated as therapeutic carriers. Here, we engineered diagnostically active PLGA nanoparticles that incorporate high payloads of nanocrystals into their core for tunable bioimaging feature…

Quantum Dots Synthesis And PropertiesNanoplatforms for cancer theranosticsAdvanced Nanomaterials in Catalysis

Characterisation of surface wettability based on nanoparticles

Nan Gao、Yuying Yan2012-01-01Nanoscale

Nanoparticles are becoming frequently used in the research area of creating functional surfaces because they can be more versatile than just making dimensions smaller. Particularly, a variety of nanoparticles have been applied for the construction of superhydrophobic and superhydrophilic surfaces with micro- and nano-…

Surface Modification and SuperhydrophobicityNanomaterials and Printing TechnologiesElectrohydrodynamics and Fluid Dynamics

Size-based cytotoxicity of silver nanoparticles in bovine retinal endothelial cells

Muthu Irulappan Sriram、Kalimuthu Kalishwaralal、Selvaraj BarathManiKanth 等 4 位作者2012-01-01Nanoscience Methods

Biologically synthesised nanoparticles with distinct shapes and sizes have found tremendous breakthroughs and fondness in various fields of therapeutic and diagnostic applications. In this study, size-controlled green synthesis of silver nanoparticles (Ag-NPs) was performed using Bacillus licheniformis kk2 by response…

Nanoparticles: synthesis and applicationsGold and Silver Nanoparticles Synthesis and ApplicationsAdvanced Nanomaterials in Catalysis

Mechanical Properties of Kenaf/Fiberglass Polyester Hybrid Composite

M.A.A. Ghani、Z. Salleh、Koay Mei Hyie 等 6 位作者2012-01-01Procedia Engineering

In a view to reduce the cost of production and the harmful destruction in normal environment, there's a lot of research have been conducted or still ongoing for the possibility of using natural fibers which are wholly degradable in the combination of biodegradable thermoplastic materials. This research will focus on K…

Natural Fiber Reinforced CompositesMechanical Engineering and Vibrations Research

Extracellular biosynthesis of silver nanoparticles by culture supernatant of Pseudomonas aeruginosa

P. Jeevan、K Ramya、A Edith Rena2012-01-01OpenAlex

The development of reliable, eco-friendly processes for the synthesis of nanoscale materials is an important aspect of nanotechnology. Silver bionanoparticles have been known to have inhibitory and bactericidal effects. In the present study, authors report the extracellular synthesis of nanoparticles of silver by redu…

Nanoparticles: synthesis and applicationsGraphene and Nanomaterials ApplicationsNanotechnology research and applications

Facile synthesis of vertically aligned hexagonal boron nitride nanosheets hybridized with graphitic domains

Amir Pakdel、Xuebin Wang、Chunyi Zhi 等 8 位作者2012-01-01Journal of Materials Chemistry

Motivated by the recent quest for producing novel two dimensional nanomaterials, we developed a facile synthetic method for growing boron nitride–carbon (BN–C) phase-separated composite nanosheet coatings on silicon/silicon dioxide (Si/SiO2) substrates. The coatings were composed of compact partially vertically aligne…

Graphene research and applicationsBoron and Carbon Nanomaterials ResearchMXene and MAX Phase Materials

Fatty acid derived renewable polyamides via thiol–ene additions

Oğuz Türünç、Maulidan Firdaus、Gregor Klein 等 4 位作者2012-01-01Green Chemistry

The syntheses of new fatty acid-derived amine functional monomers via the thiol–ene addition reaction as well as the thereof derived renewable polyamides were investigated. The thiol–ene addition of cysteamine hydrochloride to the double bonds of methyl 10-undecenoate, methyl oleate, and methyl erucate yielded heterod…

Advanced Polymer Synthesis and Characterizationbiodegradable polymer synthesis and propertiesCarbon dioxide utilization in catalysis

Recent Trends in the Microwave‐Assisted Synthesis of Metal Oxide Nanoparticles Supported on Carbon Nanotubes and Their Applications

Sarah Constance Motshekga、Sreejarani Kesavan Pillai、Suprakas Sinha Ray 等 5 位作者2012-01-01Journal of Nanomaterials

The study of coating carbon nanotubes with metal/oxides nanoparticles is now becoming a promising and challenging area of research. To optimize the use of carbon nanotubes in various applications, it is necessary to attach functional groups or other nanostructures to their surface. The combination of the distinctive p…

Carbon Nanotubes in CompositesTransition Metal Oxide NanomaterialsNanomaterials for catalytic reactions

Aptamer carbon nanodot sandwich used for fluorescent detection of protein

Bailu Xu、Chuanqi Zhao、Weili Wei 等 7 位作者2012-01-01The Analyst

Carbon nanodots (C-Dots) have attracted growing interest in recent years due to their low cost, ready scalability, excellent chemical stability, biocompatibility, colloidal stability, and resilience of photoluminescence. They have been employed as novel, ideal fluorescent probes for bio-imaging and smart sensing. In a…

Advanced biosensing and bioanalysis techniquesElectrochemical sensors and biosensorsCarbon and Quantum Dots Applications

Composite Oxygen Electrode Based on LSCM for Steam Electrolysis in a Proton Conducting Solid Oxide Electrolyzer

Yun Gan、Jun Zhang、Yuan‐Xin Li 等 6 位作者2012-01-01Journal of The Electrochemical Society

This paper presents a ceramic composite oxygen electrode (La 0.75 Sr 0.25 ) 0.95 Mn 0.5 Cr 0.5 O 3-δ (LSCM) – BaCe 0.5 Zr 0.3 Y 0.16 Zn 0.04 O 3-δ (BCZYZ) for steam electrolysis in a proton-conducting Solid Oxide Electrolyzer (SOE) with proton conducting electrolyte BCZYZ and fuel electrode BCZYZ/Ni at 700°C. AC imped…

Advancements in Solid Oxide Fuel CellsAdvanced battery technologies researchChemical Looping and Thermochemical Processes

Swelling-induced mesoporous block copolymer membranes with intrinsically active surfaces for size-selective separation

Zhaogen Wang、Xueping Yao、Yong Wang2012-01-01Journal of Materials Chemistry

Block copolymers (BCPs) are receiving growing interest in the preparation of advanced membranes with regular pores due to their capability to form highly ordered, mesoscopic structures via microphase separation. We report on the fabrication of composite membranes with mesoporous amphiphilic BCPs as the size-selective…

Membrane Separation and Gas TransportBlock Copolymer Self-AssemblyDielectric materials and actuators

Atomic layer deposition for nanofabrication and interface engineering

Monan Liu、Xianglin Li、Siva Krishna Karuturi 等 5 位作者2012-01-01Nanoscale

Atomic layer deposition (ALD) provides a tool for conformal coating on high aspect-ratio nanostructures with excellent uniformity. It has become a technique for both template-directed nanofabrications and engineering of surface properties. This Feature Article highlights the application of ALD in selected fields inclu…

Semiconductor materials and devicesCopper-based nanomaterials and applicationsElectronic and Structural Properties of Oxides

Synergic catalytic effects in confined spaces

Chenguang Yu、Jing He2012-01-01Chemical Communications

Combining the merits of confined effects and synergic effects is a promising way to build efficient and versatile heterogeneous catalytic systems. Recently, heterogeneous bifunctional and even trifunctional catalysts have attracted more and more attention because the synergic catalysis between the multifunctional grou…

Mesoporous Materials and CatalysisCovalent Organic Framework ApplicationsSurface Chemistry and Catalysis

Structural and Electrical Conductivity Studies in Nickel-Zinc Ferrite

K. Rama Krishna、K. Vijaya Kumar、D. Ravinder2012-01-01Advances in Materials Physics and Chemistry

The magnetic particles of nickel-zinc ferrite with chemical composition Ni1-xZnxFe2O4 were synthesized successfully by citrate precursor auto-combustion method using high purity nitrates and citric acid as chelating agent. The prepared powder of nickel-zinc ferrites was sintered at 1000℃ for 1 hr to obtain good crysta…

Multiferroics and related materialsMagnetic Properties and Synthesis of FerritesMagneto-Optical Properties and Applications

A novel flame-retardant-free copolyester: cross-linking towards self extinguishing and non-dripping

Haibo Zhao、Li Chen、Jun-Chi Yang 等 5 位作者2012-01-01Journal of Materials Chemistry

In this manuscript, contradiction between the non-flammability and non-dripping of polyesters could be solved by copolymerizing terephthalic acid and ethylene glycol together with a pendent phenylethynyl-based monomer named 4-(phenylethynyl) di(ethylene glycol) phthalate (PEPE), which exhibited a cross-linkable nature…

biodegradable polymer synthesis and propertiesFlame retardant materials and propertiesSynthesis and properties of polymers