Materials Literature
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A colorimetric sensing strategy employing gold nanoparticles and a paper assay platform has been developed for tuberculosis diagnosis. Unmodified gold nanoparticles and single-stranded detection oligonucleotides are used to achieve rapid diagnosis without complicated and time-consuming thiolated or other surface-modif…
In order to study the dynamic recrystallization (DRX) behavior of as-extruded 42CrMo high-strength steel, a series of isothermal upsetting experiments were carried out in a temperature range of 1123~1348 K and a strain rate range of 0.01~10 s-1 on Gleeble 1500. It was found that DRX softening is more recognizable at h…
The main purpose of this paper is to investigate both the columnar to equiaxed transition and primary dendritic arm spacings of Al-3wt.%Si alloy during the horizontal directional solidification. The transient heat transfer coefficient at the metal-mold interface is calculated based on comparisons between the experimen…
The infrared spectroscopy study of zeolite samples, obtained by steam treatment at 560‑960 °C of the ZSM‑5 catalyst (framework Si/Al ratio of 13), suggests an association between adsorbed molecular water and extra‑framework aluminum hydroxyls generated after treatment. Moreover, infrared spectroscopy of adsorbed pyrid…
The construction industry keeps on demanding huge quantities of natural resources, mainly minerals for mortars and concrete production. The depletion of many quarries and environmental concerns about reducing the dumping of construction and demolition waste in quarries have led to an increase in the procuring and use…
Superduplex stainless steel has been frequently employed in new sites of Brazilian Pre-Salt. In these environments, chloride concentration, temperature and carbon dioxide are normally present in higher levels than those at sea water at room temperature. In these conditions, it is expected that the passive films of sta…
This paper presents a summary of the knowledge on fibres and pulps of non wood tropical plants used as reinforcement in cementitious composites accumulated during the recent years by Guadeloupean and Brazilian teams participating in collaborative work. Vegetable fibres represent a good alternative as non-conventional…
Cathodic cage discharge was developed recently in order to eliminate phenomena as edge effect and overheating, which occurs during conventional processes. In this study, the effect of cage configuration in active species during the deposition process and optical properties of TiN film were studied. TiN compound was ch…
After a short review of electron tomography techniques for materials science, this overview will cover some recent results on different shape memory and nanostructured metallic systems obtained by various three-dimensional (3D) electron imaging techniques. In binary Ni–Ti, the 3D morphology and distribution of Ni4Ti3…
The paper presents some results of the research connected with the development of new approach based on the Adaptive Network-based Fuzzy Inference Systems (ANFIS) of predicting the Vickers microhardness of the phase constituents occurring in five steel samples after continuous cooling. The independent variables in the…
Solid-solution strengthening in six Al–X binary systems is investigated using first-principle methods. The volumetric mismatch parameter and the solubility enthalpy per solute were calculated. We derive three rules for designing solid-solution strengthened alloys: (i) the solubility enthalpy per solute is related to t…
Synthetic apatites are widely used both in the dental and the orthopaedic fields due to their similarity in composition with the inorganic phase of hard tissues. Biologic apatites are not pure hydroxyapatite (HA), but are calcium-deficient apatites with magnesium and carbonate as minor but important substituents. The…
Ni39+xMn50Sn11−x (x = 0.5, 1.0, 1.5 and 2) alloys comprise multiple martensite nanostrips of nanocrystallites when cast in small discs, for example, ~15 mm diameter and 8 mm width. A single martensite phase with a L10 tetragonal crystal structure at room temperature can be formed at a critical Sn content of 9.0 at.% (…
It has been more than four years since the discovery of β-FeSe1−x superconductors. Through the efforts of many outstanding research groups, unprecedented advances in the field have been achieved. High-quality single crystals of β-FeSe1−x and related compounds have been prepared by various techniques, allowing us to ex…
Because of its excellent biocompatibility and low allergenicity, titanium has been widely used for bone replacement and tissue engineering. To produce a desirable composite with enhanced bone response and mechanical strength, in this study bioactive calcium phosphate (CaP) and gelatin composites were coated onto titan…
For good performance of electrical steels it is necessary a high magnetic induction and a low power loss when submitted to cyclic magnetization. A fine dispersion of precipitates is a key requirement in the manufacturing process of Fe- 3%Si grain oriented electrical steel. In the production of high permeability grain…
Palygorskite is fibrous clay in which the structural tetrahedral and octahedral layers are organized in a way that structural channels are formed, leading to high surface area. However, impurities inside the channels and aggregated ones considerably reduce the available area. In order to increase the surface area, an…
The thermal conductivity of emulsion-polymerized styrene–butadiene rubber (ESBR) composites filled with carbon nanotubes (CNTs), zinc oxide (ZnO) and alumina (Al2O3) was predicted using the finite element method (FEM). Two-dimensional (2D) FEM models, which involved the effects of aspect ratio (AR), shape, orientation…
We first report the successful synthesis of porous germanium with ordered hierarchical structures, via controlled etching, and show its performance as an anode in a new metal-air battery. Our experimental results demonstrate the potential use of porous germanium in a high power density Ge-air energy conversion cell, s…
The synthesis and mesomorphic properties of novel homologous series are reported. All 11 members of the series, except the methoxy and ethoxy derivatives, are enantiotropically mesogenic. The propoxy to tetradecyloxy homologues exhibits smectognic amd nematogenic behavior, while the hexadecyloxy homologue shows only n…