Materials Literature
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Abstract In the stereocomplex between enantiomeric poly( l ‐lactide) ( l ‐PLA) and poly( d ‐lactide), crystallites formed as a result of stereocomplexation, equimolar l ‐ and d ‐lactide unit sequences are packed side by side. The stereocomplex exhibits a melting temperature higher by about 50 °C than that of each homo…
In this experiment, when the strontium chloride–citrate acid extractant (0.02 M SrCl2–0.05 M citrate) was used for extraction of calcareous soils with calcium carbonate greater than 70 g kg−1, the filtrate was turbid. Furthermore, white precipitation appeared when this extract was used for phosphorus determination wit…
In this paper we report a systematic study of low-frequency 1∕fα resistance fluctuation in a metal film at different stages of electromigration. The resistance fluctuation (noise) measurement was carried out in presence of a dc electromigration stressing current. We observe that in addition to the increase in the spec…
This paper deals with partial discharge measurement on three phase construction. It was shown that the measurement must be conducted on all phases simultaneously to obtain measurement result of partial discharge occurring in whole region of three phase construction with high sensitivity and to obtain information of th…
In recent experiments we observed bistable switching in devices made with long pitch square gratings on one surface. It was also discovered that the switching in these devices was localized mainly at isolated edges of the square grating profile. In this paper we present an initial study of surface‐induced director con…
At high temperatures, oxidative ageing affects only the rubber near the surface, as essentially all the oxygen is consumed by reaction with antioxidant or rubber before it can diffuse into the bulk. A resinous oxidized layer is formed and in the center of large components is essentially anaerobic. The inhomogeneous na…
Carbon nanotube (CNT) is an ideal candidate for future nanoelectronics because of its small diameter, high current-carrying capability, and high conductance in a one-dimensional nanoscale channel. The most challenging part in fabricating nanosystems could be the formation of CNT connections. Existing techniques in for…
Abstract A convenient preparative method of the synthesis of dithienylethenes based on maleimides was proposed. Previously, difficult accessible dithienylethene derivatives, in which 2-thienyl substituents are attached to the double bond of maleimide, have been synthesized. The spectral properties of the dithienylmale…
The process of dyeing poly(ethylene terephthalate) - PET films at 50, 60 and 65ºC and poly(hydroxybutyrate) - PHB granules at 60, 70 and 80ºC using supercritical carbon dioxide (scCO2) as solvent and ethanol as cosolvent was studied by DSC, TGA analysis and measurements of shrinkage to determine the morphological modi…
Carbon fiber-reinforced PMR-type polyimide composites were prepared from T-300 carbon fibers and polyimide matrix resin derived from 4,4′-methylenediamine (MDA), p-phenylenediamine ( p-PDA), diethyl ester of 3,3′,4,4′-oxydiphthalic acid (ODPE) and monoethyl ester of cis-5-norbornene-endo- 2,3-dicarboxylic acid (NE). T…
Electroluminescence (EL) emission has been observed under AC field excitation in chemically deposited (dipping technique) films of (Zn-Cd)S:Cu,F using substrates of conducting glass plates. Results of XRD, SEM, absorption spectra, transmission spectra, EL emission spectra, voltage, frequency and temperature dependence…
Abstract The prismatic variety of fluoro-edenite, a new amphibole found in lavas from Mt Etna in Biancavilla (Catania Province, Sicily, Italy), has been characterized by μ-Raman and μ-FTIR spectroscopy. The wavenumbers at which the bands are detected in the μ-Raman and μ-FTIR spectra are compared with tremolite, asbes…
Mechanical performance of hydroentangled nonwovens is determined by the degree of the fiber entanglement, which depends on parameters of the fibers, fiberweb, forming surface, water jet and the process speed. This paper develops a computational fluid dynamics model of the hydroentanglement process. Extensive compariso…
Our contribution will describe the basic fundamentals of shape memory alloys. Emphasis will be given to specific characteristics for the use of shape memory wires in actuators. The investigation of shape memory wires in actuators includes qualitative and quantitative benchmarking based on measurements at different tes…
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Abstract Ge‐filled carbon nanotubes (CNTs) with an average diameter of 15–100 nm, and Ge‐filled carbon microtubes (CMTs) with an average diameter of 100‐8000 nm, with diamondlike structures have been prepared by metal‐organic (MO)CVD from organogermanium precursors [(C 2 H 5 ) 4 Ge and (n‐C 4 H 9 ) 4 Ge]. These new co…
Liquidus temperatures (TL) were measured for the following float glass-type composition region (in mass%): 72?7 to 74?0 SiO2, 13?1 to 14?2 Na2O, 7?95 to 8?95 CaO, 2?97 to 3?97 MgO, 0?10 to 0?45 Al2O3, and 0?03 to 0?10 K2O. Glasses also contained constant minor fractions of Fe2O3 (0?71) and TiO2 (0?01). Fractions of si…
Films of polypropylene (PP) were grafted with glycidil methacrylate (GMA) using supercritical CO2 as swelling agent and solvent. Different pressures and temperatures were used to study their effects on the soaking and grafting process. FTIR results showed signals at 1726 and 1640 cm-1, assigned to C=O and C=C (after t…
The compound of single-component filled polypropylene (PP) (consists of either talc or CaCO 3 ) and multicomponent filled PP (talc/CaCO 3 /PP) are prepared by melt mixing using Brabender Plasticorder internal mixer. All systems exhibit good stability and normal flow in the molten state. The multicomponent filled PP ha…
Stable crystalline Lead Selenide nanoparticles (PbSe NPs) were prepared with a cubic (sphalerite) phase in polyvinyl alcohol (PVA) matrix. Moreover, XRD was used to characterize the PbSe NPs in PVA. The size were controlled by Pb:Se ions ratio in which the particle size was found to be inversely proportional to this r…