Materials Literature
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Magnetic bimetallic Fe–Bi composites, synthesized by decomposition of organometallic precursors under amine borane and dihydrogen, formed regular nanospheres with mean diameter of 150 ± 30 nm. The nanospheres display a core–shell like chemical distribution in which bismuth is mainly concentrated in the core, as demons…
Copper(I) and silver(I) ionic compounds [(L)M{(μ(3)-NH)(3)Ti(3)(η(5)-C(5)Me(5))(3)(μ(3)-N)}][O(3)SCF(3)] containing [MTi(3)N(4)] cube-type cations have been prepared by reaction of [(CF(3)SO(2)O)M{(μ(3)-NH)(3)Ti(3)(η(5)-C(5)Me(5))(3)(μ(3)-N)}] (M = Cu (2), Ag (3)) with a variety of donor molecules L. Treatment of comp…
The thermal decomposition of Perilla frutescens polysaccharide was examined by thermogravimetry, differential thermogravimetry, and differential thermal analysis. The results showed that the mass loss of the substance proceeded in three steps. The first stage can be attributed to the expulsion of the water from ambien…
We generate percolating fullerene-polymer bulk heterostructures that are consistent with the experimental characterization of a nanostructure, in particular neutron reflectometry and small-angle neutron scattering data from as-cast and annealed poly(3-hexylthiophene) (P3HT) and [6,6]-phenyl C61-butyric acid methyl est…
The crystalline and electronic structures of lithium insertion/extractions in trirutile LixFeF3 as well as the intercalation/deintercalation average voltages have been investigated using the density functional theory within the DFT+U framework. Our calculations give a good prediction of the average voltages with the r…
There is considerable interest in determining amide-(15)N chemical shift anisotropy (CSA) tensors from biomolecules and understanding their variation for structural and dynamics studies using solution and solid-state NMR spectroscopy and also by quantum chemical calculations. Due to the difficulties associated with th…
Macroscopic and colloidal silica surfaces were readily modified with alkoxysilaneboronate, IV, yielding silica surfaces with covalently bonded phenylboronic acid groups. XPS and neutron activation confirmed the presence of boron. The ability of these surfaces to specifically interact with polyols was demonstrated with…
Rod-shaped manganese dioxide (MnO2) nanoparticles with three different crystallographic phases, namely α-, β-, and γ-MnO2, were hydrothermally prepared. The products were characterized by X-ray diffraction (XRD), field-emission scanning electron microscopy (FE-SEM), Brunaure-Emmett-Teller (BET) method, and electrochem…
AIM: To elucidate whether warming may reduce the viscosity of miriplatin-lipiodol suspension (MPT/LPD) and also the injection pressure through microcatheters, for potential use as a chemotherapeutic agent of transarterial chemoembolization (TACE) for hepatocellular carcinoma (HCC). METHODS: Viscosity of MPT/LPD prepar…
The performance of Ni/SiO 2 catalyst for glycerol reforming has been investigated in fixed-bed reactor using careful tailoring of the operational conditions. In this paper, a commercial Engelhard catalyst has been sized and compared to gas product distribution versus catalyst size, water-to-carbon ratio, and stability…
The work carried out in this paper is to deal with a proposed conductor temperature rise computation algorithm. This simple algorithm gives more accurate calculation, making use of the load current and the weather data parameters, particularly the amount of solar incidental radiation upon the conductor and the conduct…
Plasma-assisted cleaning by metastable atomic neutralization (PACMAN) is a process that can clean hydrocarbon from extreme ultraviolet photo masks and dissolve hydrocarbon particles. It was developed with semiconductor manufacturing and cleaning in mind. The PACMAN process works by utilizing helium metastable atoms to…
The canonical Monte Carlo computer simulations and integral equation theory were applied to examine the structural and thermodynamic properties of a mixture of ions and a core-softened fluid molecules. The positive and negative ions forming a +1:-1 salt were modeled as charged hard spheres, immersed in the dielectric…
Nanocomposite hydrogels (NC gels) have been prepared based on poly(N-isopropylacrylamide) (PNIPAM) containing 0.25-15 wt% of the expandable synthetic hectorite Laponite XLS (Clay-S) by reversible addition fragmentation chain transfer (RAFT) polymerization. The swelling behaviors were investigated and the hydrogels by…
Abstract Resistive‐switching memories based on copolyimides (coPIs), PI‐NTCDIX and PI‐BTCDIX, with different compositions of 4,4′‐diamino‐4″‐methyltriphenylamine (AMTPA), 4,4′‐(hexafluoroisopropylidene)diphthalic anhydride, and N,N′‐bis‐(4‐aminophenyl)‐1,8:4,5‐naphthalenetetracarboxydiimide (NTCDI) or N,N′‐bis‐(4‐amin…
We adopt fringe counting from classical moiré interferometry on moiré patterns observed in scanning tunneling microscopy of strained thin films on single crystalline substrates. We analyze inhomogeneous strain distribution in islands of CeO2(111) on Cu(111) and identify a generic source of strain in heteroepitaxy--a t…
The role of interparticle interactions and the morphology in the magnetic behavior of dense assemblies of Fe nanoparticles with concentration well above the percolation threshold has been studied using the Monte Carlo simulations technique. The initial and temperature-dependent magnetization curves have been calculate…
Polymer (XAD7HP)/Ti 4+ nanocomposites were prepared through the swelling of polymer in titanium (IV) ethoxide as a titanium dioxide precursor. The nanocomposite beads exhibit relatively high porosity different than the porosity of the initial polymer. Thermal treatment of composite particles up to 200 °C in vacuum cau…
A new synthetic strategy to prepare dendrimers using a single, inexpensive monomer is described. Divergent growth relies on a highly efficient, metal-free Click cycloaddition of azides to alkynes. Functional dendrimers are obtained with minimal purification in high yields, with no by-product but a water soluble salt,…
Small lithium ammonia clusters are model systems for the dissociation of metals into solvated cations and electrons in ammonia. Metal-ammonia solutions display a complex behavior with increasing metal concentration including a phase change from a paramagnetic to a metallic diamagnetic phase, and small clusters should…