Materials Literature
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A comparative study of the electric field emission behaviour of vertically aligned few-layer graphene and carbon nanotubes was evaluated in a parallel plate type setup. Few-layer graphene was synthesized in the absence of any metallic catalyst by microwave plasma enhanced chemical vapour deposition with gas mixtures o…
Due to shrinking wire dimensions, higher current density, and process variations, electromigration (EM) has become a major reliability problem. The existing backend design flows use the maximum allowed current density as the only practical guidance to prevent EM. There is a need for tools capable of performing compreh…
Under 980 nm excitation, room-temperature ultraviolet (UV) upconversion (UC) emissions of Er3+ from the 4G(9/2), 2K(13/2), and 2P(3/2) states were observed in Gd2O3:Yb3+/Er3+ nanotubes, which were synthesized via a simple wet-chemical route at low temperature and ambient pressure followed by a subsequent heat treatmen…
This study describes a hydrogen embrittlement evaluation of the subsurface zone in 590DP steel by micro-Vickers hardness measurement. The 590DP steel was designed to use in high-strength thin steel sheets as automotive materials. The test specimens were fabricated to 5 series varying the chemical composition through t…
Nanocomposites of linear low-density polyethylene (LLDPE)/natural rubber (NR)/liquid natural rubber (LNR) blend denoted as TPNR with montmorillonite-based organoclay (OMMT) were prepared using melt blending method. The melt blending of LLDPE/NR/LNR with a composition of 70:20:10 formed blends. For better dispersion of…
A series of molecular-weight-controlled aromatic polyimides based on 4,4′-oxydiphthalic anhydride (ODPA), 1,4-bis(4-amino-2-trifluoromethylphenoxy)benzene (6FAPB) and 3,3′-diaminodiphenylsulfone (3,3′-DDS) were synthesized in the presence of phthalic anhydride (PA) as an end-capping agent. The effect of molecular weig…
The CAPER facility operated at the Tritium Laboratory Karlsruhe for the demonstration of the tokamak exhaust processing system comprises a PERMCAT reactor as final clean-up stage. CAPER has been upgraded to enable the production of highly tritiated water (HTW) to be detritiated with PERMCAT. A staged approach for HTW…
Experimental and analytical studies on hydrogen-tritium isotope separation by a CECE process with a LPCE column have been carried out in order to apply it to the water detritiation system for fusion reactors. Kogel catalysts and Dixon gauze rings were mixed at a certain ratio and packed in the column in a random manne…
The effect of excitation energy on the lifetimes of the charge-transfer-to-solvent (CTTS) states of small (4 ≤ n ≤ 10) iodide-doped water and alcohol clusters was explored using femtosecond time-resolved photoelectron imaging. Excitation of the CTTS state at wavelengths ranging from 272 to 238 nm leads to the formatio…
Wear debris and metal ion release generated during application of biomedical devices would cause adverse cellular response, inflammation and pain in the human body. Modifying of implant surface with rutile structure is one of the methods to reduce these problems. In the present study, an attempt was made to evaluate t…
최근, 화석연료의 고갈과 환경오염의 문제로 인해 차세대 신재생 에너지에 대한 관심이 증대되고 있다. 그 중 수소연료는 친환경, 저장의 용이, 손쉬운 제조 등과 같은 장점에 반해 가연범위가 넓고, 폭발의 위험성이 단점으로 대두되고 있다. 본 연구에서는 간편한 SP 시험법을 이용하여 고압수소가스 분위기 하에서 in-situ 수소취화거동을 평가할 수 있는 시험기법을 확립하고자 한다. 그 적용성을 평가하기 위해서 수소저장용기 재료로 사용되는 스테인리스강(SUS316L)을 사용하여 대기압, 고압 헬륨 및 수소가스 분위기에서 시험하였다. 실험결과, 고압 수소가스 분위기에서는…
Er3+-Yb3+ codoped hexagonal NaYF4 nanocrystals were prepared via a method of thermal decomposition of stearate precursor. Their crystal structure, morphologies and photoluminescence (PL) properties were characterized by XRD, SEM, and fluorescence spectra. The hexagonal NaYF4:Er3+, Yb3+ nanocrystals could be well dispe…
Intense terahertz electroluminescence from SiC structures with a miniband electron spectrum caused by the natural superlattice has been observed. The shape of the terahertz radiation line, the linear dependence of the position of its maximum on the bias voltage, the typical value of the field required to induce the ra…
In this work, thermal nanoimprint lithography (NIL) is used on full 8 in. silicon wafers to imprint a thin PS-b-PMMA block copolymer (BCP) layer. The authors show that the imprinted BCP layer can thermally self-organize after the NIL process or during the NIL process itself, depending on experimental conditions used.…
Spherical NiO nanoparticles have been synthesized by a simple and modified solvothermal method using NiCl2·6H2O and urea. After the precursor was calcined in the air, NiO could be obtained. Structural, optical, and morphological characterizations were done by x-ray powder diffraction, ultraviolet–visible (UV–vis) spec…
ZrB 2 –SiC ceramic composite was brazed by using TiZrNiCu active filler metal. The microstructure and interfacial phenomena of the joints were analysed by means of SEM, energy dispersive X-ray spectroscopy and X-ray diffraction. The joining effect was evaluated by shear strength. The results showed that the reaction p…
Metal organic decomposition (MOD) Er2O3 coating for tritium permeation barrier was fabricated on two ferritic steels with dip-coating method. The interfacial layers, which were formed by the oxidation of the substrates, were found under the coating with different compositions and thickness according to the elemental d…
Multiple photosynthetic reaction centers have successfully been constructed using a supramolecular complex of zinc porphyrin dendrimer [D(ZnP) 16 ] with pyridylnaphthalenediimide (PyNIm) in benzonitrile. The apparent formation constant determined from the fluorescence quenching of the singlet excited state of porphyri…
Hybrid nanocomposites were successfully prepared by the incorporation of polyethersulfone (PES) and organoclay into epoxy resin. They had higher fracture toughness than the prepared PES/epoxy blend and organoclay/epoxy nanocomposites. The microstructures of the hybrid nanocomposites were studied. They were comprised o…
The database system for thermophysical property data, which has been developed by the National Metrology Institute of Japan (NMIJ), is evolved to store comprehensive information on thin films. Since a thin film is identified by not only its constituent elements, phases, or compositions but also its method of synthesis…