Materials Literature
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For manganese oxides with low manganese oxidation states, such as MnO or Mn3O4, the electrochemical oxidation during potential cycling is critical to achieve high supercapacitor performance. In this work, dense Mn3O4 thin films are prepared by pulsed laser deposition. An electrochemical lithiation/delithiation process…
Nano-silver composites with a thermoplastic polyurethane as the matrix were prepared by two different routes. Using the so-called in situ preparation, silver nanoparticles were obtained by a thermal reduction of silver acetate during melt mixing. In addition, a more sophisticated ex situpreparation method was develope…
The self-assembly of inorganic nanoparticles is a research area of great interest aiming at the fabrication of unique mesostructured materials with intrinsic properties. Although many assembly strategies have been reported over the years, chemically induced self-assembly remains one of the dominant approaches to achie…
Due to the dangerous nature of anthrax, the development of a cost-effective, sensitive and field-portable sensor for the anthrax biomarker--calcium dipicolinate (CaDPA)--is of exceptional significance for both military and civilian use. Herein, a flexible polymer-film-based ratiometric sensor for detecting CaDPA was d…
Herein we report a novel green chemical route for the simultaneous reduction and exfoliation of metal salt–graphite oxide composites for the synthesis of metal/metal oxide nanoparticles dispersed over graphene using focused solar radiation. The one-step energy efficient technique resulted in an excellent dispersion of…
A split Hopkinson pressure bar is used to investigate the dynamic mechanical properties of biomedical 316L stainless steel under strain rates ranging from 1 × 10(3) s(-1) to 5 × 10(3) s(-1) and temperatures between 25°C and 800°C. The results indicate that the flow stress, work-hardening rate, strain rate sensitivity,…
In an era where the requirement for greener chemical processes is so exigent, the growing need for developing novel routes to environmentally benign and sustainable catalytic procedures is highly desirable. Heterogenising bio-inspired transition-metal complexes on a diverse range of porous supports provides a viable a…
In this short review we are discussing the creation of two dimensional nanostructures based on self-assembly of latex particles. Furthermore we are showing that optical properties of these structures can be controlled with their morphology and materials used for their preparation. Two representative structures, namely…
Pure palladium thorn clusters were synthesized using the electrodeposition method. The clusters were composed of several thorns growing on one basis. Each thorn was composed of hexahedral units with decreasing sizes. The whole thorn was a single crystal along the <220> direction. The cluster was synthesized by square…
We have synthesized polyurethane (PU)-g-poly(ethylene glycol) (PEG) copolymers for protein resistance. A macroiniferter consisting of polyurethane (PU) with tetraphenylethane groups is synthesized by the reaction of 1,1,2,2-tetraphenyl-1,2-ethanediol and isocyanate-terminated prepolymer with poly(tetramethylene glycol…
The increase in hydrogen back pressure unexpectedly enhances the overall dehydrogenation reaction rate of the 4LiBH(4) + YH(3) composite significantly. Also, argon back pressure has a similar influence on the composite. Gas back pressure seems to enhance the dehydrogenation reaction by kinetically suppressing the form…
Graphene-based nanocomposites have recently received rising interest owing to their outstanding performance. Crosslinkers, such as a divalent ion based coordinative complex, have been proved to significantly improve load transfer between adjacent graphene sheets, which subsequently defines the overall mechanical prope…
A series of open-framework aluminoborates (ABOs), [CH(3)NH(3)][(CH(3)CH(2))(2)NH(2)][Al(B(5)O(10))] (1), [CH(3)CH(2)NH(3)][(CH(3)CH(2))(2)NH(2)][Al(B(5)O(10))] (2), [CH(3)CH(2)NH(3)][(CH(3))(2)NH(2)](H(2)O)(0.5)[Al(B(5)O(10))] (3) and [CH(3)NH(3)][CH(3)CH(2)NH(3)](H(2)O)(2)[Al(B(5)O(10))] (4) have been made co-templat…
Co-dispersion of native cellulose and single walled carbon nanotubes in water is demonstrated. The pH of the water should be between 6 and 10 for better dispersion. Raman spectra confirm debundling of nanotubes in water and FTIR spectra reveal that the co-solubility is likely caused through disruption of intramolecula…
The biointegration of implants affects their function, stability and safety. Although most research on this topic has focused on bone and other hard tissues, biointegration with soft tissues is important in numerous applications, such as in prosthetic corneas. Here, we have adapted polydopamine-based adhesive surface…
A class of potential multi-chromic (19)F imaging tracers is made by pairing metal ions with a fluorinated chelator. All fluorinated metal chelates emit a single (19)F signal. Paramagnetic metal ions shifted the (19)F signal frequency and made the (19)F relaxation rates insensitive toward local chemical environment.
The results of the DC magnetron sputtering of copper thin films with different parameters of deposition are presented. The main aim of studies was to determine the influence of current value, time of deposition and target-substrate distance on morphology and grain size of obtained copper thin films. The effects of fil…
Structure-guided re-design of the acceptor binding site of D-fructose-6-phosphate aldolase from E. coli leads to the construction of FSA A129S/A165G double mutant with an activity between 5- to >900-fold higher than that of wild-type towards N-Cbz-aminoaldehyde derivatives.
Thin films of tin (Sn), aluminum (Al), gold (Au), ruthenium (Ru), tungsten (W), ruthenium dioxide (RuO2), tin dioxide (SnO2), and tungsten trioxide (WO3) were grown by glancing angle deposition (GLAD) to determine the nanostructuring temperature threshold, ΘT, above which adatom surface diffusion becomes large enough…
A comprehensive survey of electronic structure and optical properties of rare-earth ions-doped semiconductor is of vital importance for their potential applications. In this work, Eu(3+)-doped β-Ga(2)O(3) nanocrystals were synthesized via a combustion method. The evolution of the optical properties of nanophosphors wi…