Materials Literature
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Abstract Two monomers, ethylenediamine (EDA) and diaminocyclohexane (DACH), were plasma‐polymerized in continuous‐wave (CW) and pulse modes. The influence of different plasma parameters on the deposition rate and film composition were investigated in detail and the changes in aminofunctionalization with varying pulse…
Solute-induced quenching of sonoluminescence (SL) is reported for aqueous solutions of two homologous series of methyl esters and ketones using low (20 kHz) and high (515 kHz) ultrasound frequencies. SL data at 20 kHz from aqueous solutions containing alcohols and carboxylic acids are also presented to compare with pr…
We present measurements on simple foam structures flowing through a narrow channel. Driving pressure and bubble velocity are found to be related by a power law with exponent 2/3, thus extending this relationship from single bubble trains (see Bretherton F. P., J. Fluid Mech. 10 (1961) 166) to more complicated foam str…
AC electric field alignment (see Figure) offers a route to composite films with unusual physical properties, in numerous geometries and applicable to a wide range of organically modified layered silicates. Exchangeable organic cations on the aluminosilicate surface are suspected to cause the induced dipole. Orientatio…
Titanium dioxide nanoparticles were produced by the controlled hydrolysis of titanium tetraisopropoxide (TTIP) in the presence of reverse micelles formed in CO2 with the surfactants ammonium carboxylate perfluoropolyether (PFPECOO-+NH4) (Mw = 587) and poly(dimethyl amino ethyl methacrylate-block-1H,1H,2H,2H-perfluoroo…
The surfactant-free synthesis of vinyl polymer-silica nanocomposite particles has been achieved in aqueous alcoholic media at ambient temperature in the absence of auxiliary comonomers. Styrene, methyl methacrylate, methyl acrylate, n-butyl acrylate, and 2-hydroxypropyl methacrylate were homopolymerized in turn in the…
The influence of polyanilines (PANIs) as hole conductors on the photovoltaic behaviors of dye-sensitized solar cells is studied. The current-voltage (I-V) characteristics and the incident photon to current conversion efficiency (IPCE) curves of the devices are determined as the function of different conductivities and…
Abstract Thermoplastic olefin (TPO)/clay nanocomposites were made with clay loadings of 0.6–6.7 wt %. The morphology of these TPO/clay nanocomposites was investigated with atomic force microscopy, transmission electron microscopy (TEM), and X‐ray diffraction. The ethylene–propylene rubber (EPR) particle morphology in…
Because of a large difference in storage modulus below and above the glass transition temperature, poly(acrylic acid- co -methyl methacrylate)/poly(ethylene glycol) (P(AA- co -MMA)/PEG) complexes show shape memory properties with a recovery ratio of nearly reach 99%. Before the shape memory testing, it was necessary t…
Using a simple low‐temperature chemical‐solution method , multi‐walled carbon nanotubes (MWCNTs) coated with crystalline multi‐walled europium oxide nanotubes have been successfully synthesized (see Figure). The studies conducted show that such MWCNTs provide an opportunity for synthesising various rare earth oxide na…
We report on the synthesis of single-walled carbon nanohorns (SWNHs) by arc discharge between two graphite electrodes submerged in liquid nitrogen. The product in its powder form was found to consist of spherical aggregates with sizes in the range of 50–100 nm. The nanohorns are characterized by transmission electron…
Gold nanoparticles are organized into a three‐dimensional network structure using a newly designed thiol‐terminated organic gelator. Gold nanoparticles have been covalently linked with supramolecular nanoscopic fibers, in which the gelators have been assembled by intermolecular hydrogen bonding. The Figure shows fibro…
We present the fabrication of vertically aligned cobalt nanowire arrays on planar surfaces as well as preliminary field-emission (FE) experiments using them as cold electron cathodes. These arrays are obtained by electrodeposition into nanoporous templates on Au/Ti/Si substrates at very low temperature (<100 °C). Afte…
Copper, titanium, and iron with grain sizes of the order of 100 nm were prepared by severe plastic deformation. At 77 K these materials offer very high yield strength coupled with high ductility, uniform tensile strains, and long‐term stability. These properties demonstrate a nanomaterials advantage for science and en…
We individuated a method to distinguish a glass phase from a highly viscous liquid phase in a lattice of vortices, established in type-two superconductors. Our analysis is based on the study of the temperature dependence of numerically obtained 1st and 3rd harmonics curves of the AC magnetic susceptibility, by changin…
The magnetization reversal of Cu/NiFe and Nb/NiFe composite wires carrying AC current is studied. The frequency spectrum of a voltage induced in a pick-up coil wound around the wire is analyzed. The frequency spectrum is shown to consist of even harmonics within a wide range of AC current amplitudes and longitudinal D…
We report the first demonstration that carbon nanotubes can be trapped and manipulated by optical tweezers. This observation is surprising because individual nanotubes are substantially smaller than the wavelength of light, and thus should not be amenable to optical trapping. Even so, nanotube bundles, and perhaps eve…
Polymer-grafted magnetite (Fe 3 O 4 ) nanoparticles (diameter about 10 nm) were prepared through a direct polymer grafting reaction from their surfaces. The chemisorbed initiator (TEMPO-based alkoxyamine) for nitroxide-mediated radical polymerization with a phosphoric acid group gave controlled polystyrene (PS) and po…
The control objectives of batch crystallization processes are often defined in terms of particle size distribution (PSD), or properties related to the PSD, viz. average particle size, product filterability, dry solids flow properties, etc. To achieve these control objectives, a constrained nonlinear model-based optimi…
A super‐amphiphobic polymeric coating , i.e., one that shows both water‐ and oil‐repellent properties, produced by a simple, one‐step casting process from two common polymers, is described. The micro–nano binary structure of the film has similarities to that of a lotus leaf. The Figure shows a water droplet on the coa…