Materials Literature
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Recent developments in producing large single crystal CVD diamond plates are reviewed. The developments consist of synthesis of large single crystal diamond and production of single crystal diamond plates from the bulk diamond by the lift-off process. Combining these developments, half-inch single crystal CVD diamond…
Amorphous InGaZnO4 (a-IGZO) films doped with various concentrations of Mn have been fabricated by using pulsed-laser deposition technique. Optical, electrical, and magnetic properties of the prepared Mn-doped a-IGZO films were investigated. The resistivity, carrier concentration, and carrier mobility of the a-IGZO fil…
We fabricated 20 nm thick PbTiO3 films via reactive magnetron sputtering and studied the domain switching phenomena and retention properties using piezoresponse force microscopy. We found that multistep deposited PbTiO3 thin films showed 29% smaller rms roughness (2.5 versus 3.5 nm), 28% smaller coercive voltage (1.68…
Polypropylene (PP)/ethylene-octene copolymer (POE) blends with 10–50wt% POE composition were prepared using a twin-screw extruder in the melt state. Mechanical properties of PP and PP/POE blends were tested and the effect of POE content on the crystalline morphology and structure, melting and crystallization behavior,…
Abstract Distribution of fabric softeners on cotton terry cloth was studied using scanning electron microscopy and energy dispersive X‐ray analysis. The unsaturated groups in the quaternary fabric softeners were tagged with osmium tetroxide to provide contrast in the microscopy. Longitudinal specimens showed the fabri…
Triphenylphosphine oxide (TPPO) was characterized by a differential scanning calorimeter (DSC) and nuclear magnetic resonance ( 1 H NMR and 31 P NMR). Using a static analytical method, the solubilities of TPPO were measured in benzene, toluene, ethyl acetate, and binary solvent mixtures: benzene + ethyl acetate (volum…
Intraconnects, as-grown single-walled carbon nanotubes bridging two metal electrodes, were investigated as gated structures. We show that even with a seemingly "ohmic" contact at zero gate voltage one observes negative differential resistance (NDR) at nonzero gate bias. Large differential photo conductance (DPC) was a…
Solubilities of nonanedioic acid in binary ethanol + water solvent mixtures have been determined by the dynamic method using a laser monitoring observation technique over a temperature range from (292.35 to 345.52) K and a solvent composition, mole fraction of ethanol of solute-free x 2 0, range from 0.0 to 1.0. The e…
The present study was to examine influence of epichlorohydrin (ECH) modification on structure and properties of glycerol-plasticized wheat gliadin films casting from ethanol/water (70/30 v/v) solution. The modified films were characterized using proton nuclear magnetic resonance ((1)H NMR), Fourier transformation infr…
Abstract BACKGROUND: Poly(1‐amino‐2‐naphthol‐4‐sulfonic acid) and its copolymers with aniline are a new class of conducting polymers which can acquire intrinsic protonic doping ability, leading to the formation of highly soluble self‐doped homopolymers and copolymers. Free OH and NH 2 groups in the polymer chain can…
Embossing or embedding of nanoparticles into a polymeric film is realized by an electromagnetic field. Upon laser light illumination nanoparticles absorb energy, convert it to heat, and sink into a locally softened polymer film as probed by atomic force microscope. The polymeric matrix forms a characteristic rim and s…
In this paper, some technological problems (e.g. low drawability, high susceptibility to galling, spring-back) occurring in the sheet-titanium forming process are discussed. A numerical simulation of the stamping process was carried out with the Adina System v.8.3 based on the finite element method. The effects of fri…
Ga 1− x Mn x As nanowires were synthesized with finely controlled Mn contents ( x = 0, 0.01, 0.02, 0.03, and 0.05) by the vapor transport method. They consisted of single-crystalline GaAs nanocrystals (avg. diameter = 60 nm) grown along the [111] direction. The Mn doping decreases the lattice constant, most significan…
Biaxial ZnO−ZnS heterostructure nanoribbons (NRs) have been synthesized using the vapor−liquid−solid technique by the thermal evaporation of ZnS powder in the presence of a Au nanoparticles catalyst, a limited supply of oxygen and an inert carrier gas under controlled temperature and pressure. High resolution transmis…
Poly(L-lactic acid)-block-poly(poly(ethylene glycol) monomethacrylate) (PLLA-b-PPEGMA) has been prepared by the ring-opening polymerization of lactide with a double-headed initiator, 2-hydroxyethyl 2'-methyl-2'-bromopropionate (HMBP), followed by atom transfer radical polymerization (ATRP) of poly(ethylene glycol) mon…
Abstract BACKGROUND: The aim of this work was to study, using differential scanning calorimetry, the effect of carboxylic functionalization of multi‐walled carbon nanotubes (MWCNTs) on the cure reaction of MWCNTs/diglycidyl ether of bisphenol A/2‐ethyl‐4‐methylimidazole (MWCNTs/DGEBA/EMI‐2,4) nanocomposites. This is i…
We present an approach where biomolecular self-assembly is used in combination with lithography to produce patterns of metallic nanoparticles on a silicon substrate. This is achieved through a two-step method, resulting in attachment of nanoparticles on desired sites on the sample surfaces, which allowed a detailed ch…
The electronic structure of radially deformed single walled carbon nanotubes under transverse external electric fields is studied by self-consistent density functional theory methods. The energy band structure modifications are analyzed, revealing that the admixture of the different states and increased σ−π hybridizat…
Abstract In this paper, a semi‐classical one‐dimensional (1D) electron fluid model is built that is based on a classical two‐dimensional electron fluid theory taking into account electron–electron repulsive forces, which are significant in 1D system. We have used 1D fluid model to characterize the carbon nanotube (CNT…
We show that the S(N)(H) approach opens up new possibilities in the synthesis of hetaryl-substituted nitronyl nitroxides. The reaction of 4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazole-3-oxide-1-oxyl lithium salt with pyridine-, pyrimidine-, pyrazine-, isoquinoline-, phthalazine-, quinoxaline-, and 1,2,4-triazine-N-oxid…