Materials Literature
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The Troika II beamline at the European Synchrotron Radiation Facility was conceived as a versatile beamline for the study of liquid and solid interfaces, combining grazing-incidence diffraction, X-ray reflectivity and grazing-incidence small-angle scattering in a single instrument. Scattering experiments can be perfor…
By hydrolysis of an ethanolic gallium nitrate solution, gamma-Ga2O3 was prepared as a single-phase polymorph having a specific surface area of 160 m2 g(-1). Surface acidity and basicity of this material was studied by IR spectroscopy, using pyridine, 2,6-dimethylpyridine, acetonitrile, and carbon dioxide as spectrosco…
Thin films obtained from a layer-by-layer deposition of a weak polycarboxylic acid and a positively charged globular protein were studied by in situ ATR-FTIR. The system was chicken egg lysozyme (Lys), bovine pancrease ribonuclease A (RNase), or bovine gamma-globulin (IgG) self-assembled with polycarboxylic acids. Whe…
The distortions in the square tellurium nets long known to exist in the structures of the charge-density wave materials, RETe3, have been elucidated. The (Te2)1- nets contain polytelluride oligomers which propagate in a fashion incommensurate from the adjacent (RETe)+ sublattice. The new information sets the stage for…
The excitation spectrum of a model magnetic system, LiHoF4, was studied with the use of neutron spectroscopy as the system was tuned to its quantum critical point by an applied magnetic field. The electronic mode softening expected for a quantum phase transition was forestalled by hyperfine coupling to the nuclear spi…
A series of copper catalysts supported on TiO2-ZrO2 with copper loading varying from 1.0 to 21.6 wt % were prepared by a wet impregnation method. The catalysts were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), UV-vis diffuse reflectance spectroscopy, electron spin resonance (ESR),…
A novel laser molecular beam epitaxy (LMBE) system for the fabrication of atomically controlled oxides superlattices and an x-ray diffractometer that measures spatially-resolved x-ray diffraction spectra have been developed based on the concept of combinatorial methodology. The LMBE chamber has two moving masks, an au…
Electronic structures, exchange interaction mechanism between magnetic ions and Curie temperature of Vanadium - doped Nitrides (AlN, GaN, and InN) are studied within KKR-LSDA-CPA. It is found that the ferromagnetic super-exchange interaction mechanism is dominant at low concentrations of Vanadium, but the anti-ferroma…
Substances such as the ``telephone number compound'' Sr14Cu24O41 are intrinsically hole-doped. The involved interplay of spin and charge dynamics is a challenge for theory. In this article we propose to describe hole-doped Heisenberg spin rings by means of complete numerical diagonalization of a Heisenberg Hamiltonian…
The strip projection method is the most important way to generate quasiperiodic patterns with predefined local structure. We have obtained a very efficient algorithm for this method which allows one to use it in superspaces of very high dimension. A version of this algorithm for two-dimensional clusters and an applica…
We develop a theory of the linear optical spectrum of excitons in quantum dot molecules, including the effect of exciton-phonon coupling beyond the Markov limit. The model reproduces the general trend of the zero-phonon line broadening as a function of interdot distance, that were recently measured. The unexpectedly b…
Electron spin resonance spectra of copper phthalocyanine doped with alkaline metals (AxCuPc) have been investigated. The temperature dependence of ESR spectra indicates the ferromagnetic behavior. The Curie-Weiss temperature varies from 30K to 115K depending on the stoichiometry x of samples. Some particles of polycry…
The spin-orbit split white line, synchrotron X-ray spectra at the respective Cu and Ba L2,3 and Ba M4,5 edges in YBa2Cu3O7 crystal, powders, films and derivatives are compared to those for standard BaBr2 and CuO powders. The white line absorption integrated intensity, I ratios: r3,2 = I(L3)/I(L2) and r5,4 = I(M5)/I(M4…
Disguise tactics: Peptide–polymer hybrid nanotubes are constructed in which self-assembled cyclic peptides govern the structure, and a synthetic polymer coating determines the surface chemistry. Formation of the latter is initiated in situ from preorganized peptide building blocks. The picture shows an AFM image of na…
There is considerable interest in hydrogen adsorption on carbon nanotubes and porous carbons as a method of storage for transport and related energy applications. This investigation has involved a systematic investigation of the role of functional groups and porous structure characteristics in determining the hydrogen…
We compute analytically and numerically the four-point correlation function that characterizes nontrivial cooperative dynamics in glassy systems within several models of glasses: elastoplastic deformations, mode-coupling theory (MCT), collectively rearranging regions (CRR's), diffusing defects, and kinetically constra…
The paper reports the study of the effect of Zr contents on the dielectric, ferroelectric, leakage current and fatigue properties of Ba (Zr x Ti1 − x ) O3 films. All these films exhibited high dielectric constant, which tends to be maximum for 5 at % (BZT5) Zr doped BaTiO3 film. The dielectric properties at the sub-sw…
This study has demonstrated that acetylshikonin (ACS), the isolated ingredient from Lithospermum canescens Lehm. roots, in a daily dose of 200 microg for 3 days, inhibited cutaneous angiogenesis induced by L-1 sarcoma cells in Balb/c mice.
Composites of palm fiber and polypropylene were compounded using a mixing equipment connected to an extruder. The composites were then injection molded into standard tensile specimens for mechanical characterization. The fracture morphology of the specimens was also analyzed by Scanning electron microscopy. It was obs…
It is demonstrated that Fe3+ in one solution can be reduced to Fe2+ by ascorbic acid in another solution when both aqueous solutions are separated by polyaniline membrane. This transmembrane redox process is possible due to electron/anion coupled counter transport through polyaniline membrane. It was demonstrated that…