Materials Literature
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Bath mixtures of ethanol and ethylene glycol in dry ice produce sustainable constant temperatures over the range from -12 to -78 °C, which show a linear relationship between the bath temperature and the volume fraction of ethylene glycol. Our bath is less toxic than previously reported mixtures of ortho - and meta -xy…
A real-time in situ study of the initial stages of the interaction of oxygen with Ni(111) in a high temperature scanning tunneling microscope (STM) at temperatures between 400 and 470 K is presented. Oxygen adsorption features, in particular the Ni(111)-p(2×2)O reconstruction, were identified in room temperature STM i…
The radioluminescence and thermoluminescence spectra of synthetic zircon crystals doped with individual trivalent rare earth element (REE) ions (Pr, Sm, Eu, Gd, Dy, Ho Er, and Yb) and P are reported in the temperature range 25 to 673 K. Although there is some intrinsic UV/blue emission from the host lattice, the domin…
The dependence of the pressure threshold of martensitic transformations on the disordering degree of starting structures is considered for graphite-like BN into diamond-like BN modifications transitions. The effect of loading conditions on transformation mechanisms of rhombohedral BN into zinc blende or wurtzite modif…
A constant deflection device designed for use within a transmission electron microscope (TEM) was used to study the change in dislocation configuration ahead of a crack tip during stress corrosion cracking (SCC) of brass in water, Ti-24% Al-11% Nb alloy in methanol (CH3OH), and the initiation of SCC. In-situ tensile t…
Metal-bonded cobalt ferrite composites are promising candidates for torque sensors and other magnetostrictive sensing and actuating applications. In the present study, the temperature dependence of the magnetomechanical effect in a ring-shape cobalt ferrite composite under torsional strain has been investigated in the…
It is demonstrated through the comparison of analytical, numerical, and experimental results that the existence of excess eddy current losses can be explained by the peculiar nature of the nonlinear diffusion of electromagnetic fields in magnetically nonlinear laminations. The essence of this peculiar nature is that n…
A bis(ether amine) containing the ortho-substituted phenylene unit and pendant tert-butyl group, 1,2-bis(4-aminophenoxy)-4-tert-butylbenzene, was synthesized and used as a monomer to prepare polyimides with six commercial dianhydrides via a conventional two-stage procedure. The intermediate poly(amic acid)s had inhere…
By linking C2 type axial ligands such as 2,2‘-biphenoxy or 2,2‘-binaphthyloxy to the metal of a metallophthalocyanine (MtPc) as axial ligands, the effective symmetry of the chromophore was lowered, as manifested in the splitting of the Q00 band, which is reasonally explained by an excitonic interaction between the axi…
BaFe 11.9 Mn 0.1 O 19 powders were prepared by a sol–gel method. Magnetic and structural properties of the powders were characterized by Mössbauer spectroscopy, x-ray diffractometry, and vibrating sample magnetometry. X-ray diffraction and Mössbauer measurements showed that the BaFe11.9Mn0.1O19 had an M-type hexagonal…
Abstract A simple theoretical model of network degradation around ultrasonically pulsating cavities is considered. The model is based on the concept of overstressed chains and provides a simple tool to estimate a number of chains which should be involved in mechanochemical degradation at a given amplitude of ultrasoni…
Anisotropic magnetoresistance (AMR) in strained Pr0.67Sr0.33MnO3 thin films has been studied by measuring the resistance as a function of the angle between the applied magnetic field direction and the film normal with the current always perpendicular to the magnetic field. The results show that both compressive- and t…
Although phosphate sorption is a well‐understood phenomenon in soils, less is known of its effect on electrophoretic mobility (EM), isoelectric point (IEP), and clay particle dispersion in Oxisols. High phosphate sorption and high stability of aggregates are characteristic of Oxisols. Phosphate sorbed as inner‐sphere…
The power loss (Pcv) was analyzed by combining two methods. The first, Pcv, is divided into hysteresis loss (Ph) and residual loss (Pr) from the frequency dependence of the power loss according to the method of Otsuki et al., and, second, the loss factors are attributed to domain wall motion (Pw) and the rotation magn…
Water solubility in silica melts was determined at 100-600 MPa, 1200-1350 °C, and at each temperature (T) was found to increase with pressure (P). At P ≤ 250 MPa, the effect of T on water solubility in silica melts is small and within analytical precision (±0.15 wt% H 2 O). A positive correlation with T was observed a…
peer reviewed
A Σ = 11, {332} nickel bicrystal was grown by solidification. The aim of this paper is to show the evolution of the grain-boundary (GB) structure depending upon the position in the bicrystal of the extracted sample. Conventional transmission electron microscopy and high-resolution transmission electron microscopy (HRT…
A comprehensive model has been developed for the computation of corrosion rates of carbon steels in the presence of lithium bromide (LiBr)-based brines that are used as working fluids for absorption refrigeration cycles. The model combines a thermophysical module that provides realistic speciation of aqueous systems w…
Several banana-shaped liquid crystal materials with perfluorinated terminal chains have been synthesized. A dimorphism SmA-B2 was proved by X-ray studies and electro-optical measurements. The unusual ratio d/L (d = layer spacing, L = molecular length) and the unexpected behaviour of the layer spacing at the phase tran…
In this article a study on the melting behavior and microstructure of semicrystalline poly(ethylene naphthalene-2,6-dicarboxylate) (PEN) prepared by crystallization from the glass under different annealing conditions is presented. The influence of the annealing temperature (Ta), annealing time (ta), and the heating ra…